scholarly journals Nanoscale electrochemical 3D deposition of cobalt with nanosecond voltage pulses in an STM

Author(s):  
Alain Reiser ◽  
Rolf Schuster ◽  
Ralph Spolenak

To explore a minimal feature size of <100 nm with electrochemical additive manufacturing, we use a strategy originally applied to microscale electrochemical machining for the nanoscale deposition of Co on Au. The concept’s essence is the localization of electrochemical reactions below a probe during polarization with ns-long voltage pulses. As shown, a confinement that exceeds that predicted by a simple model based on the time constant for one-dimensional double layer charging enables a feature size of <50 nm for 2D patterning. We further indirectly verify the potential for out-of-plane deposition by tracking growth curves of high-aspect-ratio deposits. Importantly, we report a lack of anodic stability of Au tips used for patterning. As an inert probe is the prerequisite for controlled structuring, we experimentally verify an increased resistance of Pt probes against degradation. Consequently, the developed setup and processes show a path towards reproducible direct 2D and 3D patterning of metals at the nanoscale.

2020 ◽  
Vol 117 (24) ◽  
pp. 13339-13349 ◽  
Author(s):  
Sahil K. Rastogi ◽  
Raghav Garg ◽  
Matteo Giuseppe Scopelliti ◽  
Bernardo I. Pinto ◽  
Jane E. Hartung ◽  
...  

The ability to modulate cellular electrophysiology is fundamental to the investigation of development, function, and disease. Currently, there is a need for remote, nongenetic, light-induced control of cellular activity in two-dimensional (2D) and three-dimensional (3D) platforms. Here, we report a breakthrough hybrid nanomaterial for remote, nongenetic, photothermal stimulation of 2D and 3D neural cellular systems. We combine one-dimensional (1D) nanowires (NWs) and 2D graphene flakes grown out-of-plane for highly controlled photothermal stimulation at subcellular precision without the need for genetic modification, with laser energies lower than a hundred nanojoules, one to two orders of magnitude lower than Au-, C-, and Si-based nanomaterials. Photothermal stimulation using NW-templated 3D fuzzy graphene (NT-3DFG) is flexible due to its broadband absorption and does not generate cellular stress. Therefore, it serves as a powerful toolset for studies of cell signaling within and between tissues and can enable therapeutic interventions.


2013 ◽  
Vol 38 (12) ◽  
pp. 2005 ◽  
Author(s):  
Feng Tian ◽  
Guangya Zhou ◽  
Yu Du ◽  
Fook Siong Chau ◽  
Jie Deng ◽  
...  

2018 ◽  
Vol 203 ◽  
pp. 04011
Author(s):  
Ong Yin Hoe ◽  
Hisham Mohamad

There is a trend in Malaysia and Singapore, engineers tend to model the effect of TBM tunneling or deep excavation to the adjacent piles in 2D model. In the 2D model, the pile is modelled using embedded row pile element which is a 1-D element. The user is allowed to input the pile spacing in out-of-plane direction. This gives an impression to engineers the embedded pile row element is able to model the pile which virtually is a 3D problem. It is reported by Sluis (2014) that the application of embedded pile row element is limited to 8D of pile length. It is also reported that the 2D model overestimates the axial load in pile and the shear force and bending moment at pile top and it is not realistic in comparison to 3D model. In this paper, the centrifuge results of single pile and 6-pile group - tunneling problem carried out in NUS (National University of Singapore) are back-analysed with Midas GTS 3D and a 2D program. In a separate case study, pile groups adjacent to a deep excavation is modelled by 3D and 2D program. This paper compares the deflection and forces in piles in 2D and 3D models.


2016 ◽  
Author(s):  
E. R. Méndez ◽  
G. D. Jiménez ◽  
A. A. Maradudin

Author(s):  
Yuqing Zhou ◽  
Tsuyoshi Nomura ◽  
Kazuhiro Saitou

This paper presents a gradient-based multi-component topology optimization (MTO) method for structures assembled from components made by powder bed additive manufacturing. It is built upon our previous work on the continuously-relaxed MTO framework utilizing the concept of fractional component membership. The previous attempt on the integration of the relaxed MTO framework with additive manufacturing constraints, however, suffered from numerical instability for larger size problems, limiting its application to 2D low-resolution examples. To overcome this difficulty, this paper proposes an improved MTO formulation based on a design field regularization and a nonlinear projection of component membership variables, with a focus on powder bed additive manufacturing. For each component, constraints on the maximum allowable build volume (i.e., length, width, and height), the elimination of enclosed voids, and the minimum printable feature size are imposed during the simultaneous optimization of the overall base topology and component partitioning. The scalability of the new MTO formulation is demonstrated by a few 2D examples with much higher resolution than previously reported, and the first reported 3D example of MTO.


2011 ◽  
Vol 121-126 ◽  
pp. 3945-3949 ◽  
Author(s):  
Shih Heng Tung ◽  
Jui Chao Kuo ◽  
Ming Hsiang Shih ◽  
Wen Pei Sung

In recent years, 2D digital image correlation method (DIC) has been widely used in the measurement of plane strain. However, out-of-plane displacement could be induced during the loading and it would affect the measurement accuracy. Thus, a 3D measurement is necessary. This study utilizes a simplified 3D DIC to measure the geometry of an object before and after deformation. Then the finite element concept is involved to determine the strain after deformation. A flat plate specimen with in-plane and out-of-plane displacement is observed. Both 2D and 3D DIC are used to analyze the strain. The results show that using 3D DIC to measure strain is feasible and with a very good accuracy.


2018 ◽  
Vol 45 (2) ◽  
pp. 253-278 ◽  
Author(s):  
Meraj Alam ◽  
Bibaswan Dey ◽  
Sekhar Raja

In this article, we present a biphasic mixture theory based mathematical model for the hydrodynamics of interstitial fluid motion and mechanical behavior of the solid phase inside a solid tumor. The tumor tissue considered here is an isolated deformable biological medium. The solid phase of the tumor is constituted by vasculature, tumor cells, and extracellular matrix, which are wet by a physiological extracellular fluid. Since the tumor is deformable in nature, the mass and momentum equations for both the phases are presented. The momentum equations are coupled due to the interaction (or drag) force term. These governing equations reduce to a one-way coupled system under the assumption of infinitesimal deformation of the solid phase. The well-posedness of this model is shown in the weak sense by using the inf-sup (Babuska?Brezzi) condition and Lax?Milgram theorem in 2D and 3D. Further, we discuss a one-dimensional spherical symmetry model and present some results on the stress fields and energy of the system based on ??2 and Sobolev norms. We discuss the so-called phenomena of ?necrosis? inside a solid tumor using the energy of the system.


Author(s):  
H Hardisty ◽  
A R Mileham ◽  
H Shirvani

A theoretical and computational investigation into the electrochemical machining (ECM) process for the case of a moving stepped tool eroding an initially flat surface is presented. Five parametric variations of the basic geometry of the stepped tool machining process are possible, depending on the relative distance between the moving tool and eroded work. For each of the five cases, and based on one-dimensional theory, formulae have been developed to predict the minimum depth of working material that must initially be provided to enable a particular step size to be machined to a specified tolerance. The computer simulation of the ECM process which has been developed is based on the finite element method (FEM). The geometry of tool, electrolyte and work is simulated by means of a two-dimensional mesh of square elements. A system of macros has been developed which interact internally with an FE package to move component boundaries systematically to simulate both tool movement and surface erosion. Such boundary movements are accomplished automatically and continuously without user intervention during a simulation run. The algorithms employed to achieve characteristically different erosion rates are described. Results both from one-dimensional ECM theory and from the computer simulations of the characteristic cases are presented. Comparisons show that there is good agreement between computer predictions and theory. The differential erosion process is fundamental to all ECM processes. Complex shapes evolve because of spatial differences in erosion rates. Thus the one-dimensional results presented here for the formation of a step should provide a basis for comparisons between spatially separated regions of one-dimensional differential erosion on bodies of arbitrary shape.


1. Introduction .—Gamow's elegant deduction by general arguments of the law of radioactive decay by α-particle emission and his subsequent investigations on artificial disintegration suggested to us the desirability of investigating as closely as possible any simple model of a decaying nucleus as a verification of his general approximations. For the model chosen the exact investigation of the decay process is almost trivial. Since we obtained this, now some time ago, Dr. Gamow informed us that he had also obtained equivalent detailed results. Still more recently such results have been published by Kudar. We shall not therefore dwell upon them here. The application of the same ideals, however, to the reverse process of penetration presents points of very definite interest, which we think are well worth discussion. The main point that arises is that the chance of penetration α-particle is or is not equal to a characteristic energy of the nucleus itself. This is a point which is not dealt with by Gamow in his paper. We have discussed it with him, and now put forward the results we have obtained. Since the solution of the decay problem is required in the main discussion of the penetration of α-particles into the nucleus it is included here in 2 for reference. We must emphasise that we claim no novelty, except of detail, for the work of 2; the general lines by now are a matter of fairly common knowledge.


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