ANALYSIS OF THE TEMPERATURE FIELD FOR CHARACTERIZATION OF THE CONCENTRATION OF THE WATER-ALCOHOL MIXTURE

Author(s):  
Pedro Gonçalves ◽  
dhiego veloso ◽  
MARCIO ROCHA ◽  
Jobson SIlva ◽  
Carlos Antonio Cabral Santos
2000 ◽  
Vol 71 (6) ◽  
pp. 675 ◽  
Author(s):  
Shafiqul D.-M. Islam ◽  
Toshifumi Konishi ◽  
Mamoru Fujitsuka ◽  
Osamu Ito ◽  
Yuko Nakamura ◽  
...  

1986 ◽  
Vol 32 (4) ◽  
pp. 4573-4580 ◽  
Author(s):  
Fumio Suzuki ◽  
Hiroshi Kimura ◽  
Kenji Onozato ◽  
Syuko Kuroda

2009 ◽  
Vol 495 (1-2) ◽  
pp. 90-94 ◽  
Author(s):  
Valeriy I. Smirnov ◽  
Valentin G. Badelin

FLORESTA ◽  
2021 ◽  
Vol 51 (4) ◽  
pp. 893
Author(s):  
Thiago Cardoso Silva ◽  
Rafael Leite Braz ◽  
Emmanoella Costa Guaraná Araujo ◽  
Gisely Alves da Silva ◽  
Maria de Los Angeles Perez Fernandez Palha

This study aimed to chemically characterize the bark extracts from three tree species: Anacardium occidentale L., Ziziphus joazeiro Mart. and Mimosa caesalpiniaefolia Benth., in addition to obtaining the soluble extract content in water, alcohol and hexane from the bark of these species. The bark was collected from branches of the three species and subsequently pre-dried and milled. The extract content was then determined using the Sohxlet method aiming to quantify the total extractives in the samples, and determine the extract content soluble in water, ethyl alcohol and hexane. The extracts were further analyzed by Near Infrared Spectroscopy (NIRS) analysis to determine their chemical composition. The extract contents in the three species behaved in a similar way, with hexane being the solvent which extracted more compounds and juazeiro the species that displayed the highest total extract content. With the chemical characterization of the extracts, it was possible to identify the presence of functional groups characteristic of carbohydrates and proteins in the aqueous extracts; the presence of characteristic hydroxyl group, for example in alcohols, aldehydes, ketones and ethers in the ethanolic extracts; and the presence of fatty acids and aromatic compounds (essential oils) in hexanolic extracts. The essential oils were the compounds which presented larger quantities, and can be exploited by the pharmaco-chemical industry.


Author(s):  
HRABOVSKA Olena ◽  
VITRIAK Oksana ◽  
AVRAMENKO Alina

Background. Taking into consideration the intense rhythm of life, the development of technologies for instant food products of increased nutritional value is urgent. Typically, food concentrates for desserts include fruit or fruit and berry fillings and require cooking to prepare ready-made meals. In this case, heat treatment of the mixture (boiling) negatively affects the thermolabile biologically active compounds. The aim of the work was to develop a recipe for instant food jelly concentrates of increased nutritional value based on encapsulated powdery hibiscus extract. Materials and methods. To encapsulate the aqueous-alcoholic extract of hibiscus and obtain a powdered semi-finished product, swelling potato starch was used. Rheological studies were carried out using a "REOTEST-2" rotational viscometer. Results. In order to enrich food concentrates of instant kissel with biologically active substances, we studied a method for extracting dry hibiscus flowers with aqueous-alcoholic solutions of various concentrations. It was found that the extractivity and the transfer of polyphenolic compounds, including anthocyanins, to the extract are improved when a water-alcohol mixture with an ethyl alcohol concentration of 30 % is used as an extractant. For the preparation of a powdery hibiscus extract, modified swelling starch was used, which has the property of swelling in cold water, which makes it possible not to subject the mixture to prolonged heat treatment for preparing a ready-made dish and to preserve the biologically active substances of the hibiscus extract. In addition, this starch is an effective solid carrier that plays a protective role for thermolabile vitamins and bioflavonoids. On the basis of experimental studies, formulations of instant jelly have been developed, which include fructose, powdered hibiscus extract, apple pectin and ascorbic acid. The study of the rheological properties of semi-finished products based on hibiscus extract, as well as ready-made jelly, testifies to the receipt of a finished dessert with a delicate creamy consistency. Conclusion. A method for obtaining a powdery encapsulated hibiscus extract based on swelling potato starch and a composition of a food jelly concentrate using this semi-finished product have been developed. It was found that for the extraction of raw materials it is better to use a water-alcohol mixture with an ethanol content of 30 %, since most of the anthocyanins are converted into the extract under these conditions. The developed semi-finished product of dry hibiscus extract can be used as a thickener, acidifier and colorant in recipes for food concentrates for instant dessert dishes. Due to the use of swelling starch, food concentrates of jelly do not need to be boiled, and the presence of vitamins, organic acids, flavonoids and especially anthocyanins in the hibiscus extract increases the nutritional value of the finished product.


2010 ◽  
Vol 663-665 ◽  
pp. 1089-1092
Author(s):  
Ya Ling Li ◽  
Jia Ning Ning ◽  
Yuan Mei Chen ◽  
Guang Fei Liu ◽  
Guo Qing Zhang

Silver myristate/AgBr composite particles were prepared by using silver nitrate, sodium hydroxide, myristic acid, and sodium bromide as raw materials and PVP as surfactant in water-alcohol system and characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRD), ultraviolet-visible spectroscopy (UV) and differential scanning calorimetry (DSC). The results showed that silver myristate/AgBr composite particles are composed of rod-like silver myristate grains with a layer structure and small silver bromide particles formed on the surface of silver myristate. Silver bromide can extend the ultraviolet absorbance range of silver myristate. The size of silver myristate is about 260nm and the average size of silver bromide is about 44nm. TG and DSC analysis showed that the reaction was carried out completely. The composite particles start to decompose at about 210oC. Silver bromide of the composite particles melts at 418.2oC.


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