scholarly journals Determination of Optimum Operating Conditions of Different Types of Intercooler Designs in Supercharged Engines

Author(s):  
Cengiz ÖNER ◽  
Ali ÖZ
2012 ◽  
Vol 31 (1) ◽  
pp. 29
Author(s):  
Violeta Mitić ◽  
Snežana Nikolić-Mandić ◽  
Vesna Stankov-Jovanović

The present paper describes a simple, selective and sensitive kinetic method for the determination of trace amounts of Sb(III) in the presence of Sb(V) based on its inhibition effect on the redox reaction between bromate and Victoria blue 4R (V.B. 4-R) in hydrochloric acid media. The reaction was followed spectrophotometrically by measuring the decrease in the absorbance of V.B. 4-R at 596.3 nm. Optimum operating conditions regarding reagent concentrations were established. The optimized conditions yielded a theoretical detection limit of 1.30·10‒8 g cm–3 Sb(III) based on the 3S0 criterion. The method allows the determination of Sb(III) in the range of 5·10‒8 ‒ 1.1·10‒6 g cm–3. The effects of certain foreign ions the reaction rate were determined for an assessment of the selectivity of the method. The kinetic parameters of the reaction were reported, and the rate equations were suggested. The results were validated statistically and through recovery studies. The proposed method has been successfully applied to the determination of Sb(III) in various model and real samples.


2008 ◽  
Vol 73 (8-9) ◽  
pp. 879-890 ◽  
Author(s):  
Snezana Mitic ◽  
Gordana Miletic ◽  
Aleksandra Pavlovic ◽  
Biljana Arsic ◽  
Valentina Zivanovic

The aim of this work was to develop a new kinetic spectrophotometric method for the determination of ibuprofen in pharmaceutical formulations. Ibuprofen was determined in an acidic ethanolic medium by monitoring the rate of appearance of 1-nitroso-2-naphthol, resulting from the displacement by ibuprofen of Co(III) from the tris(1-nitroso-2-naptholato)cobalt(III) complex. The optimum operating conditions regarding reagent concentrations and temperature were established. The tangent method was adopted for constructing the calibration curve, which was found to be linear over the concentration range 0.21-1.44 and 1.44-2.06 ?g ml-1. The optimized conditions yielded a theoretical detection limit of 0.03 ?g ml-1 based on the 3.3 S0 criterion. The interference effects of the usual excipients of powdery drugs, foreign ions and amino acids on the reaction rate were studied in order to assess the selectivity of the method. The developed procedure was successfully applied for the rapid determination of ibuprofen in commercial pharmaceutical formulations and human control serum. The unique features of this procedure are that the determination can be performed at room temperature and the analysis time is short. The newly developed method is simple, inexpensive and efficient for use in the analysis of a large number of samples.


2019 ◽  
pp. 19-23
Author(s):  
Erika Montero ◽  
David Contreras-López ◽  
Rosalba Fuentes ◽  
María Del Rosario Galindo

The production of artificial polymers is, today, one of themost important activities of the chemical industry, polymersare widely used in everyday life, as, there are different types of polymers, they can be used for different uses. These polymeric materials have unique mechanical, physical and chemical properties, which most other materials do not possess, not to mention that its cost is lower than the other materials. The present research work focuses on the determination of optimal operating conditions for the polymerization of styrene and methyl methacrylate in a Batch reactor, as well as the influence of inorganic salt in this case NaCl in the performance of reaction and in the size of the material polymer, through the process of suspension using a synthetic route of polymerization by radical free conventional (FRP), where viscometry to the polymeric material testing was performed for this way characterize it, and to determine factors of interest such as the molecular weight, etc.


2018 ◽  
Vol 42 (10) ◽  
pp. 3339-3350 ◽  
Author(s):  
Yuhao Huang ◽  
Li Shui ◽  
Saeed Asghari ◽  
Paweena Prapainainar ◽  
Akhil Garg ◽  
...  

1976 ◽  
Vol 49 (4) ◽  
pp. 1060-1067 ◽  
Author(s):  
R. Pautrat ◽  
B. Metivier ◽  
J. Marteau

Abstract It has been verified that, in a number of cases, thermogravimetric analysis permits quantitative determination and identification of carbon blacks in the free state or in vulcanized compounds. The proper operating conditions can give sufficiently good repeatability and adequate precision for most routine analyses. As is the case in other methods for determining the loading, numerous difficulties were encountered with elastomers which graphitize on heating. However, quantitative analysis of black in nitrile rubbers remains possible, but the identification of different types of black is very difficult. The authors propose to continue this study, particularly into the new families of blacks, primarily into the function of the diameter of their elementary particles and their degree of structure.


Author(s):  
Ümit Karadoğan ◽  
Gökhan Çevikbilen ◽  
Sevde Korkut ◽  
Mehmet Emin Pasaoglu ◽  
Berrak Teymur

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