scholarly journals Large-Scale Coaxial Magnetron Discharge Containing Magnets at Extremely High Vacuum and Its Application to Sputter Ion Pump.

Shinku ◽  
1995 ◽  
Vol 38 (1) ◽  
pp. 17-21 ◽  
Author(s):  
Tastuo ASAMAKI ◽  
Takemichi TANIGUCHI ◽  
Toshihiro FUKAYA ◽  
Atsuo KUDOH ◽  
Kenichi YAMAMOTO
2019 ◽  
Vol 223 ◽  
pp. 379-385 ◽  
Author(s):  
Qinglong Xie ◽  
Li Cai ◽  
Fan Xia ◽  
Xiaojiang Liang ◽  
Zhenyu Wu ◽  
...  

Nanomaterials ◽  
2019 ◽  
Vol 9 (4) ◽  
pp. 540 ◽  
Author(s):  
Huanchun Wang ◽  
Junping Ding ◽  
Haomin Xu ◽  
Lina Qiao ◽  
Xuanjun Wang ◽  
...  

Cuprous based chalcogenides have attracted intensive research interest due to the potential applications in solar energy conversion. However, typical fabrications of these compounds are often carried out under severe conditions, such as inert gas protection, high vacuum, and/or extreme high temperature. Here we reported a one-pot process for cuprous based chalcogenides synthesis in aqueous solution. A strategy for BiCuSO nanosheets fabrication without toxic chemicals or rigorous reagents at pretty low temperatures under an ambient atmosphere was established, with the practicality of morphology controlling and the compatibility of multifarious precursors. Platelike BiCuSO with a thickness range from several to hundreds nanometers are fabricated by adjusting the alkali concentration, reaction time, and temperature. The positive effect of alkali hydroxide concentration is proposed cautiously based on the experimental results. The photocatalytic activities of BiCuSO nanosheet under UV, visible, and near-infrared irradiation were also investigated. BiCuSO obtained at room temperature with a thickness of 4.5 nm showed the most impressive efficiency to decompose organic contaminants. Our research presented a new way for cuprous sulfides fabrication, and might open up a new vista for large-scale synthesis of cuprous based materials as promising broadband spectrum light-absorbing materials.


2018 ◽  
Vol 930 ◽  
pp. 609-612
Author(s):  
Quezia Cardoso ◽  
Franks Martins Silva ◽  
Ligia Silverio Vieira ◽  
Julio Cesar Serafim Casini ◽  
Solange Kazume Sakata ◽  
...  

Graphene has attracted significant interest because of its excellent electrical properties. However, a practical method for producing graphene on a large scale is yet to be developed. Graphene oxide (GO) can be partially reduced to graphene-like sheets by removing the oxygen-containing groups and recovering the conjugated structure. GO can be produced using inexpensive graphite as the raw material via cost-effective chemical methods. High vacuum and temperature (10−7 mbar and 1100°C, respectively) conditions are well-known to enable the preparation of reduced powder at the laboratory scale. However, a large-scale high vacuum reduction system that can be routinely operated at 10−7 mbar requires considerable initial capital as well as substantial operational and maintenance costs. The current study aims at developing an inexpensive method for the large-scale reduction of graphene oxide. A stainless steel vessel was evacuated to backing-pump pressure (10−2 mbar) and used to process GO at a range of temperatures. The reduction of GO powder at low vacuum pressures was attempted and investigated by X-ray diffraction and Fourier transform infrared spectroscopy. The experimental results of processing GO powder at various temperatures (200–1000°C) at relatively low pressures are reported. The microstructures of the processed materials were investigated using scanning electron microscopy and chemical microanalyses via energy dispersive X-ray analysis.


1997 ◽  
Vol 36 (Part 1, No. 2) ◽  
pp. 787-791 ◽  
Author(s):  
Tsutomu Miura ◽  
Tatsuo Asakaki

Shinku ◽  
1992 ◽  
Vol 35 (2) ◽  
pp. 70-75 ◽  
Author(s):  
Tatsuo ASAMAKI ◽  
Tsutomu MIURA ◽  
Gen NAKAMURA ◽  
Koichi HOTATE ◽  
Shingo YONAIYAMA ◽  
...  

2016 ◽  
Vol 2016 (1) ◽  
pp. 000469-000474 ◽  
Author(s):  
Xiao Liu ◽  
Qi Wu ◽  
Dongshun Bai ◽  
Trevor Stanley ◽  
Alvin Lee ◽  
...  

Abstract Advanced wafer-level packaging (WLP) techniques, mainly driven by high performance applications in memory and mobile market, have been adopted for large-scale manufacturing in recent years. Temporary wafer bonding and debonding technology has been widely studied and developed over the last decade for use in various WLP technologies, such as package-on-package (PoP), fan-out integration, and 2.5-D and 3-D integration using through-silicon-via (TSV). Temporary bonding technology enables handling of thinned substrates (<100 μm), which can no longer self-support during backside processing and packaging. Moreover, some applications require the temporary bonding materials to withstand temperatures up to 250°C in high-vacuum conditions, and even up to 350°C or higher during the dopant activation step required for manufacturing power devices. Therefore, a simple yet effective temporary bonding process and material that can survive all the backside processes is highly desired. In this study, a series of formulations based on polar thermoplastics were developed for temporary wafer bonding applications. These materials target high temperature survivability and improved adhesion to prevent the premature delamination during downstream wafer processing. All of these materials provide high thermal stability up to 250°C or higher, and are able to be bonded to carrier wafers treated with release layers, which can be selectively debonded by either mechanical or laser release after backside processing. The material left on device wafer after debonding can be easily cleaned using common industrial solvents. Wafers bonded with these materials demonstrate lower overall stack total thickness variation (TTV < 5 μm) after grinding and have successfully passed a 200°C PECVD process without any delamination during grinding and PECVD processes.


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