Transformation of expanded austenite to an amorphous ferromagnetic surface layer during laser carburization of austenitic stainless steel

2009 ◽  
Vol 64 (4) ◽  
pp. 242-248 ◽  
Author(s):  
P. Schaaf ◽  
H. Binczycka ◽  
M. Kahle ◽  
S. Cusenza ◽  
D. Höche ◽  
...  
2017 ◽  
Vol 701 ◽  
pp. 167-173 ◽  
Author(s):  
Frederico A.P. Fernandes ◽  
Thomas L. Christiansen ◽  
Grethe Winther ◽  
Marcel A.J. Somers

Coatings ◽  
2020 ◽  
Vol 10 (12) ◽  
pp. 1250
Author(s):  
Darina Manova ◽  
Patrick Schlenz ◽  
Jürgen W. Gerlach ◽  
Stephan Mändl

Expanded austenite γN formed after nitrogen insertion into austenitic stainless steel and CoCr alloys is known as a hard and very wear resistant phase. Nevertheless, no single composition and lattice expansion can describe this phase with nitrogen in solid solution. Using in situ X-ray diffraction (XRD) during ion beam sputtering of expanded austenite allows a detailed depth-dependent phase analysis, correlated with the nitrogen depth profiles obtained by time-of-flight secondary ion mass spectrometry (ToF-SIMS) or glow discharge optical emission spectroscopy (GDOES). Additionally, in-plane XRD measurements at selected depths were performed for strain analysis. Surprisingly, an anomalous peak splitting for the (200) expanded peak was observed for some samples during nitriding and sputter etching, indicating a layered structure only for {200} oriented grains. The strain analysis as a function of depth and orientation of scattering vector (parallel/perpendicular to the surface) is inconclusive.


2013 ◽  
Vol 634-638 ◽  
pp. 2955-2959 ◽  
Author(s):  
Lie Shen ◽  
Liang Wang ◽  
Jiu Jun Xu ◽  
Ying Chun Shan

The fine grains and strain-induced martensite were fabricated in the surface layer of AISI 304 austenitic stainless steel by shot peening treatment. The shot peening effects on the microstructure evolution and nitrogen diffusion kinetics in the plasma nitriding process were investigated by optical microscopy and X-ray diffraction. The results indicated that when nitriding treatments carried out at 450°C for times ranging from 0 to 36h, the strain-induced martensite transformed to supersaturated nitrogen solid solution (expanded austenite), and slip bands and grain boundaries induced by shot peening in the surface layer lowered the activation energy for nitrogen diffusion and evidently enhanced the nitriding efficiency of austenitic stainless steel.


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