scholarly journals A MICRO-PRECONCENTRATOR/FOCUSER FOR A MICRO-GAS CHROMATOGRAPH: DEVICE AND MATERIALS CHARACTERIZATION

2008 ◽  
Author(s):  
R.A. Veeneman ◽  
E.T. Zellers
Keyword(s):  
Materials Characterization ◽  
Gas Chromatograph

Elemental Distribution in Pt-Re:Al2O3 Naphtha Reforming Catalysts

1980 ◽  
Vol 38 ◽  
pp. 200-201
Author(s):  
R. L. Freed ◽  
M. J. Kelley
Keyword(s):  
Bimetallic Catalyst ◽  
Supported Catalysts ◽  
Coke Formation ◽  
Materials Characterization ◽  
Metal Catalyst ◽  
Elemental Distribution ◽  
Exact Nature ◽  
Naphtha Reforming ◽  
Reforming Catalysts ◽  
Commercial Introduction

The commercial introduction of Pt-Re supported catalysts to replace Pt alone on Al2O3 has brought improvements to naphtha reforming. The bimetallic catalyst can be operated continuously under conditions which lead to deactivation of the single metal catalyst by coke formation. Much disagreement still exists as to the exact nature of the bimetallic catalyst at a microscopic level and how it functions in the process so successfully. The overall purpose of this study was to develop the materials characterization tools necessary to study supported catalysts. Specifically with the Pt-Re:Al2O3 catalyst, we sought to elucidate the elemental distribution on the catalyst.

Optimization of the time the chromatograph thermostats exit to a given temperature

2020 ◽  
pp. 40-45
Author(s):  
Nadezhda O. Vzduleva ◽  
Valery B. Gitlin
Keyword(s):  
Heating Rate ◽  
Entire Range ◽  
Gas Chromatograph ◽  
Heating And Cooling ◽  
Operating Temperatures ◽  
The Stability

The problems of ensuring the stability of the temperature of the chromatographic experiment carried out using a serial gas chromatograph LGH-3000 are considered. Limiting the permissible heating rate of the chromatograph thermostats does not allow a quick transition to the new conditions of the chromatographic experiment in accordance with the requirements of the technical conditions. The processes of heating and cooling the thermostat are analyzed. It is shown that the ratio of the duration of the interval equal to the sum of the durations of the heating and cooling intervals to the duration of the heating interval is inversely proportional to the temperature of the chromatographic experiment. Based on this situation, an empirical algorithm is proposed for heating the thermostat to a given temperature, which made it possible to reduce the time it takes to reach a given temperature in the entire range of operating temperatures.

Methods to Determine Phytopharmaceuticals in Tobacco and Tobacco Products. 4th Report: A Procedure to Determine Vamidothion and its Metabolites/Methoden zur Bestimmung von Phytopharmaka in Tabak und Tabakerzeugnissen: IV. Mitteilung: Ein Bestimmungsverfahren fuer Vamidothion und seine Metaboliten

1977 ◽  
Vol 9 (2) ◽  
Author(s):  
A.N. Sagredos ◽  
R. Moser
Keyword(s):  
Mass Spectrometry ◽  
Nuclear Magnetic Resonance ◽  
Acetic Acid ◽  
Magnetic Resonance ◽  
Aluminium Oxide ◽  
Nuclear Magnetic Resonance Data ◽  
Gas Chromatograph ◽  
Tobacco Products ◽  
Magnetic Resonance Data ◽  
Resonance Data

AbstractBased on previous work (7) a method to simultaneously determine vamidothion [I], vamidothion-sulfoxide [II] and vamidothion sulfone [III] in tobacco has been developed. The compounds are extracted with water/acetone/acetic acid from the tobacco, cleansed over an aluminium oxide column and then determined on the gas chromatograph with the specific sulphur detector. Rates of recovery are 70 % - 92 %, the determination level is 0.1 ppm. Mass spectrometry and nuclear magnetic resonance data of vamidothion [I], vamidothion-sulfoxide [ II ] and vamidothion-sulfone [III] are given.

Nanomechanical Characterization in the FIB

2005 ◽  
Author(s):  
Thomas M. Moore
Keyword(s):  
Focused Ion Beam ◽  
Ion Beam ◽  
Materials Characterization ◽  
Depth Of Focus ◽  
Ion Milling ◽  
Nano Technology ◽  
Physical Behavior ◽  
Nanomechanical Testing ◽  
Load Cells ◽  
Scanning Electron

Abstract The availability of the focused ion beam (FIB) microscope with its excellent imaging resolution, depth of focus and ion milling capability has made it an appealing platform for materials characterization at the sub-micron, or "nano" level. This article focuses on nanomechanical characterization in the FIB, which is an extension of the FIB capabilities into the realm of nano-technology. It presents examples that demonstrate the power and flexibility of nanomechanical testing in the FIB or scanning electron microscope with a probe shaft that includes a built-in strain gauge. Loads that range from grams to micrograms are achievable. Calibration is limited only by the availability of calibrated load cells in the smallest load ranges. Deflections in the range of a few nanometers range can be accurately applied. Simultaneous electrical, mechanical, and visual data can be combined to provide a revealing study of physical behavior of complex and dynamic nanostructures.

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