The Onset and Solidification Path of a Basaltic Melt by in situ Differential Scanning Calorimetry (DSC) and ex situ Investigations

Polyethylene/montmorillonite (PE/MMT) nanocomposites were prepared by in situ polymerization. The crystallization behavior of PE/MMT nanocomposites at different MMT concentrations (from 0.1 to 1.2 wt %) were investigated by differential scanning calorimetry (DSC). The equilibrium melting points increase by the addition of MMT. The crystallization rates of PE/MMT nanocomposites are faster than those of pure PE. The addition of MMT facilitated the crystallization of PE, with the MMT functioning as a heterogeneous nucleating agent at lower content; at higher concentrations, however, the physical hindrance of the MMT layers to the motion of PE chains retarded the crystallization process.

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Experimental Investigation of Rice Straw and Model Compound Oxidative Pyrolysis by in Situ Diffuse Reflectance Infrared Fourier Transform and Coupled Thermogravimetry–Differential Scanning Calorimetry/Mass Spectrometry Method

Energy & Fuels ◽

10.1021/acs.energyfuels.5b00583 ◽

2015 ◽

Vol 29 (7) ◽

pp. 4361-4372 ◽

Cited By ~ 7

Author(s):

Shanhui Zhao ◽

Yonghao Luo ◽

Yunliang Zhang ◽

Yufeng Long

Keyword(s):

Mass Spectrometry ◽

Differential Scanning Calorimetry ◽

Experimental Investigation ◽

Diffuse Reflectance ◽

Model Compound ◽

Scanning Calorimetry ◽

Spectrometry Method ◽

Oxidative Pyrolysis ◽

Diffuse Reflectance Infrared

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In-situ investigations of thermal processes in polymers by simultaneous differential scanning calorimetry and infrared spectroscopy

Journal of Molecular Structure ◽

10.1016/0022-2860(95)08687-q ◽

1995 ◽

Vol 348 ◽

pp. 457-460 ◽

Cited By ~ 6

Author(s):

B. Ziegler ◽

K. Herzog ◽

R. Salzer

Keyword(s):

Differential Scanning Calorimetry ◽

Infrared Spectroscopy ◽

Thermal Processes ◽

Scanning Calorimetry

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Reactions in Metal-Metalloid Multilayers

MRS Proceedings ◽

10.1557/proc-311-3 ◽

1993 ◽

Vol 311 ◽

Cited By ~ 3

Author(s):

Robert Sinclair ◽

Toyohiko J. Konno

Keyword(s):

Electron Microscopy ◽

Transmission Electron Microscopy ◽

Differential Scanning Calorimetry ◽

Reactive Systems ◽

Nucleation And Growth ◽

In Situ Observation ◽

Scanning Calorimetry ◽

Compound Formation ◽

Transmission Electron

ABSTRACTWe have studied the reactions at metal-metalloid interfaces using high resolution transmission electron microscopy, including in situ observation, and differential scanning calorimetry. There is contrasting behavior depending on the affinity for interaction or segregation. For reactive systems, compound formation ultimately results, but this can be preceded by solidstate amorphization. For non-reactive systems, crystallization of the metalloid is often achieved with nucleation and growth mediated by the metal phase.

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Crystal formation in vanadium-doped zirconia ceramics

CrystEngComm ◽

10.1039/c8ce00538a ◽

2018 ◽

Vol 20 (22) ◽

pp. 3105-3116 ◽

Cited By ~ 5

Author(s):

Roman Svoboda ◽

Roman Bulánek ◽

Dušan Galusek ◽

Roghayeh Hadidimasouleh ◽

Yadolah Ganjkhanlou

Keyword(s):

Differential Scanning Calorimetry ◽

Diffraction Analysis ◽

Crystal Formation ◽

X Ray Diffraction ◽

Zirconia Ceramics ◽

Scanning Calorimetry ◽

X Ray

Differential scanning calorimetry and in situ X-ray diffraction analysis were used to study the products and mechanism of crystal formation in VOx–ZrO2 ceramics.

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