scholarly journals Dynamic Precipitation in Mg–8.08Gd–2.41Sm–0.30Zr Alloy during Hot Compression

Materials ◽  
2018 ◽  
Vol 11 (11) ◽  
pp. 2147
Author(s):  
Limin Zhu ◽  
Quanan Li ◽  
Qing Zhang ◽  
Xiaoya Chen
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Hot Compression ◽  
Strain Rates ◽  
Dynamic Precipitation ◽  
Compression Tests ◽  
Effects Of Temperature ◽  
Compression Temperature

Dynamic precipitation of Mg–8.08Gd–2.41Sm–0.30Zr (wt %) alloy during hot compression was studied in the present work. The effects of temperature and strain rate on dynamic precipitation, and the effects of dynamic precipitation on dynamic recrystallization (DRX) and microhardness, were systematically analyzed. For this purpose, hot compression tests were conducted at the strain rates of 0.002~1 s−1 and temperatures of 350~500 °C, with the compaction strain of 70% (εmax = 0.7). The obtained results revealed that dynamic precipitation occurred during hot compression at 350~400 °C, but did not occur for T ≥ 450 °C. The precipitates were demonstrated to be β-Mg5Gd with a size of 200~400 nm, and they were distributed in the DRXed region. Dynamic precipitation occurred at strain rates in the 0.002~0.01 s−1 range, but did not occur when the strain rates were in the 0.1~1 s−1 range for the hot compression temperature of 350 °C. The relationships between the hot compression temperature (T) and DRXed grain size (lnd), microhardness (Hv), and DRXed grain size (d−1/2) of Mg–8.08Gd–2.41Sm–0.30Zr alloy were obtained.

Compressing Deformation and Microstructure of AZ61 Magnesium Alloy

2014 ◽  
Vol 1015 ◽  
pp. 203-206
Author(s):  
Quan Li ◽  
Jin Yang ◽  
Wen Jun Liu ◽  
Su Qin Luo ◽  
Ren Ju Cheng ◽  
...  
Keyword(s):  
Grain Size ◽  
Flow Stress ◽  
Magnesium Alloy ◽  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Deformation Temperature ◽  
Hot Compression ◽  
Compression Tests ◽  
Az61 Magnesium Alloy

Hot compression tests of AZ61 magnesium alloy were performed on gleeble1500D at strain rate ranged in 0.01~1s-1 and deformation temperature 350~400°C.The results show that the flow stress and microstructures strongly depend on the deformation temperature and the strain rate. When the temperature was reduced and the strain rate was enhanced, the area after dynamic recrystallization was enhanced, and the average dynamically recrystallied grain size reduce. But the dynamically recrystallied grain size was not well-proportioned. In this paper the 350°C×1s-1 was suggested.

The effects of temperature and strain rate on the hot deformation behavior of AISI H10 tool steel

2020 ◽  
Vol 118 (1) ◽  
pp. 107
Author(s):  
Maryam Kamali Ardakani ◽  
Maryam Morakabati
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Tool Steel ◽  
Hot Deformation ◽  
Deformation Behavior ◽  
Strain Rates ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
Temperature Range

The hot deformation behavior of a H10 hot work tool steel was studied by performing hot compression tests over the temperature range of 900 to 1200 °C and strain rates of 0.001–1 s−1 and total strain of 0.7. At temperatures below 1100 °C, the grain size is fine and below 20 μm. In this temperature range, grain size increase with temperature due to dissolution of carbides. Then by increasing temperature to 1150 and 1200 °C, the grain size is increased significantly due to growth of grains. The study on the effect of strain rate showed that at constant temperature of 1000 °C, the grain size increased from 4.8 to 6 μm with increasing strain rate from 0.001 to 1 s−1. Also, this increase in the strain rate at temperature of 1100 °C lead to increase the grain size from 5.9 to 17 μm, due to the occurrence of dynamic recrystallization. At 1200 °C growth of grains causes to decrease grain size from 112 to 87 μm by increasing strain rate. According to the microstructural investigations, at the temperatures of 1000 and 1100 °C and strain rates of 0.01 and 0.1 s−1 dynamic recrystallization was the main softening mechanism. As a result, the most suitable range for hot deformation was obtained at the temperature range of 1000–1100 °C and strain rates of 0.01–0.1 s−1.

scholarly journals Hot Deformation Behavior of a Ni-Based Superalloy with Suppressed Precipitation

Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 605
Author(s):  
Franco Lizzi ◽  
Kashyap Pradeep ◽  
Aleksandar Stanojevic ◽  
Silvana Sommadossi ◽  
Maria Cecilia Poletti
Keyword(s):  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Hot Deformation ◽  
Strain Rates ◽  
Compression Tests ◽  
Deformation Bands ◽  
Stress Softening ◽  
Relative Stress ◽  
The Matrix ◽  
Thermomechanical Processes

Inconel®718 is a well-known nickel-based super-alloy used for high-temperature applications after thermomechanical processes followed by heat treatments. This work describes the evolution of the microstructure and the stresses during hot deformation of a prototype alloy named IN718WP produced by powder metallurgy with similar chemical composition to the matrix of Inconel®718. Compression tests were performed by the thermomechanical simulator Gleeble®3800 in a temperature range from 900 to 1025 °C, and strain rates scaled from 0.001 to 10 s−1. Flow curves of IN718WP showed similar features to those of Inconel®718. The relative stress softening of the IN718WP was comparable to standard alloy Inconel®718 for the highest strain rates. Large stress softening at low strain rates may be related to two phenomena: the fast recrystallization rate, and the coarsening of micropores driven by diffusion. Dynamic recrystallization grade and grain size were quantified using metallography. The recrystallization grade increased as the strain rate decreased, although showed less dependency on the temperature. Dynamic recrystallization occurred after the formation of deformation bands at strain rates above 0.1 s−1 and after the formation of subgrains when deforming at low strain rates. Recrystallized grains had a large number of sigma 3 boundaries, and their percentage increased with strain rate and temperature. The calculated apparent activation energy and strain rate exponent value were similar to those found for Inconel®718 when deforming above the solvus temperature.

scholarly journals Study of Static Recrystallization Kinetics and the Evolution of Austenite Grain Size by Dynamic Recrystallization Refinement of an Eutectoid Steel

Metals ◽  
2019 ◽  
Vol 9 (12) ◽  
pp. 1289
Author(s):  
Cesar Facusseh ◽  
Armando Salinas ◽  
Alfredo Flores ◽  
Gerardo Altamirano
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Static Recrystallization ◽  
Controlled Rolling ◽  
Strain Rates ◽  
Peak Strain ◽  
Compression Tests ◽  
Eutectoid Steel ◽  
Austenite Grain Size ◽  
Austenite Grain

Interrupted and continuous hot compression tests were performed for eutectoid steel over the temperature range of 850 to 1050 °C and while using strain rates of 0.001, 0.01, 0.1, and 1 s−1. The interrupted tests were carried out to characterize the kinetics of static recrystallization(SRX) and determinate the interpass time conditions that are required for initiation and propagation of dynamic recrystallization (DRX), while considering that the material does not contain microalloying elements additions for the recrystallization delay. Continuous testing was used to investigate the evolution of the austenite grain size that results from DRX. The results indicate that carbon content accelerates the SRX rate. This effect was observed when the retardation of recrystallization due to a decrease in deformation temperature from 1050 to 850 °C was only about one order of magnitude. The expected decelerate effect on the SRX rate when the initial grain size increases from 86 to 387 µm was not significant for this material. Although the strain parameter has a strong influence on SRX rate, in contrast to a lesser degree of strain rate, both of the effects are nearly independent of the chemical composition. The calculated maximum interpass times that are compatible with DRCR (Dynamic Recrystallization Controlled Rolling), for relatively low strain rates, suggest that the onset and maintaining of the DRX is possible. However, while using the empirical equations that were developed in the present work to estimate the maximum times for high strain rates, such as those observed in the wire and rod mills, indicate that the DRX start is feasible, but maintaining this mechanism for 5% softening in each pass after peak strain is not possible.

High Temperature Deformation Behavior and Dynamic Recrystallization Law of 33Mn2V Steel for Oil Well Tube

2014 ◽  
Vol 511-512 ◽  
pp. 63-69
Author(s):  
Rui Jia ◽  
Fu Zhong Wang
Keyword(s):  
Dynamic Recrystallization ◽  
Deformation Behavior ◽  
Hot Compression ◽  
High Temperature Deformation ◽  
Temperature Deformation ◽  
Oil Well ◽  
Strain Rates ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
Activation Energy Of Deformation

Deformation behavior of steel 33Μn2v for oil well tube was studied by hot compression tests conducted at various temperatures and strain rates.The Kumar model was developed to predict the hot deformation behavior of steel 33Mn2V for oil well tube.In this regard,the hot compression tests were carried out at the temperatures from 750°C to 1200°C and at the strain rates of 0.02s1 to 0.16 s1.The experimental data were then used to determine the constants of developed constitutive equations. The Kumar model can be represented by ZenerHollomon parameter in a hyperbolic sinusoidal equation form.The apparent activation energy of deformation is calculated to be 342.1481kJ/Mol.Dynamic recrystallization of steel 33Mn2V occur and the completion of the critical deformation is small,termination error and the initial deformation is smaller.Therefore,its easy for the steel 33Mn2V to the occurrence and completion of dynamic recrystallization.

Deformation Behavior and Microstructure Evolution of 6063 Alloy during Hot Compression

2018 ◽  
Vol 913 ◽  
pp. 63-68 ◽  
Author(s):  
Zhu Hua Yu ◽  
Da Tong Zhang ◽  
Wen Zhang ◽  
Cheng Qiu
Keyword(s):  
Flow Stress ◽  
Strain Rate ◽  
Shear Bands ◽  
Hot Compression ◽  
Al Alloy ◽  
Strain Rates ◽  
Compression Tests ◽  
Softening Effect ◽  
6063 Al Alloy ◽  
Gleeble 3500

Hot compression tests of homogenized 6063 Al alloy were carried out in the temperatures range from 390°C to 510°C and strain rates from 1s-1 to 20s-1 on a Gleeble-3500 thermal simulation machine. The results showed that the flow stress decreased with increasing deformation temperature or decreasing strain rate. The dynamic softening effect was more obvious when the alloy was deformed at strain rate of 20 s-1. The Arrhenius-type constitutive equation with strain compensation can accurately describe the flow stress of 6063 aluminum alloy during hot compression. Shear bands appeared in grains interior when the alloy deformed at high strain rates, corresponding to high Zenner-Hollomon (Z) parameters. When deformed under the conditions with low Z parameters, the dynamic recrystallization started occurred.

Effect of Deformation Conditions on Dynamic Recrystallization of As-Cast GH625 Alloy

2015 ◽  
Vol 816 ◽  
pp. 620-627
Author(s):  
Hao Yu Wang ◽  
Jian Xin Dong ◽  
Mai Cang Zhang ◽  
Lei Zheng ◽  
Zhi Hao Yao ◽  
...  
Keyword(s):  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Process Design ◽  
Deformation Process ◽  
Strain Rates ◽  
Recrystallization Behavior ◽  
Compression Tests ◽  
Volume Percent ◽  
Dynamic Recrystallization Behavior ◽  
Continuous Recrystallization

High temperature compression tests at a deformation temperature range of 1273K~1473K with various strain rates of 0.01s-1~0.1s-1 on as-cast GH625 alloy were carried out, aiming at the current research status that the deformation process of cogging and the recrystallization behavior of ingot are still in the study. The results indicated that the recrystallization nuclei of ingot formed not only along the original grain boundaries, but also in the interdendrite. Dynamic recrystallization volume percent increased with the increase of temperature and the decrease of strain rate. When the temperature was high and strain rate was low, the dynamic recrystallization behavior of as-cast GH625 alloy was dominated by discontinuous recrystallization. However, when the temperature was low and strain rate was high, continuous recrystallization also existed. These results can provide some reliable experimental support for the cogging process design.

Grain Size and the Compressive Strength of Ice

1985 ◽  
Vol 107 (3) ◽  
pp. 369-374 ◽  
Author(s):  
D. M. Cole
Keyword(s):  
Grain Size ◽  
Size Effect ◽  
Strain Rate ◽  
Peak Stress ◽  
Applied Strain ◽  
Test Material ◽  
Strain Rates ◽  
Grain Size Effect ◽  
Compression Tests ◽  
Polycrystalline Ice

This work presents the results of uniaxial compression tests on freshwater polycrystalline ice. Grain size of the test material ranged from 1.5 to 5 mm, strain rate ranged from 10−6 to 10−2 s−1 and the temperature was −5°C. The grain size effect emerged clearly as the strain rate increased to 10−5 s−1 and persisted to the highest applied strain rates. On average, the stated increase in grain size brought about a decrease in peak stress of approximately 31 percent. The occurrence of the grain size effect coincided with the onset of visible cracking. The strength of the material increased to a maximum at a strain rate of 10−3 s−1, and then dropped somewhat as the strain rate increased further to 10−2 s−1. Strain at peak stress generally tended to decrease with both increasing grain size and increasing strain rate. The results are discussed in terms of the deformational mechanisms which lead to the observed behavior.

Hot Deformation and Processing Map of C919 Aluminum Alloy

2015 ◽  
Vol 816 ◽  
pp. 810-817
Author(s):  
Yong Biao Yang ◽  
Zhi Min Zhang ◽  
Xing Zhang
Keyword(s):  
Aluminum Alloy ◽  
Flow Stress ◽  
Strain Rate ◽  
Hot Deformation ◽  
Testing Machine ◽  
Strain Rate Range ◽  
Hot Compression ◽  
Strain Rates ◽  
Processing Maps ◽  
Compression Tests

The hot deformation behaviors of Aluminum alloy C919 were studied in the present investigation. The hot compression tests for C919 were carried out in the temperature range of 350°C~470°C and strain rates range of 0.001s-1~1s-1 using GLEEBLE-1500 thermal simulate testing machine. Optical microscopy (OM) was used for the microstructure characterization. The experimental results showed that the flow stress of C919 aluminum alloy decreased with increasing temperature and decreasing strain rates and the flow stress curves tended to increase at a strain rate of 1s-1 with increasing strain, while the flow stresses kept with increasing strain at lower strain rate. The alloys were more prone to dynamic recrystallization with decreasing strain rates during hot deformation. The hot compression behavior of C919 aluminum alloy can be described as hyperbolic sine function corrected Arrhenius relation. The processing maps for the alloy were built at a strain of 0.6. The instability deformation domain occurred at temperatures range from 350°C and 380°C and at a strain rate of 0.1-1s-1. Based on the processing maps and microstructure observations, the optimum hot-working parameters were determined to be at a temperature of 470°C in the strain rate range from 0.1-0.01s−1 for the C919 aluminum alloy.

scholarly journals Evolution of Dynamic Recrystallization in 5CrNiMoV Steel during Hot Forming

2020 ◽  
Vol 2020 ◽  
pp. 1-13
Author(s):  
Zhiqiang Hu ◽  
Kaikun Wang
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Volume Fraction ◽  
True Strain ◽  
True Stress ◽  
Hot Forming ◽  
Strain Rates ◽  
Stress Strain ◽  
Lower Strain

The dynamic recrystallization (DRX) behavior of 5CrNiMoV steel was investigated through hot compression at temperatures of 830–1230°C and strain rates of 0.001–10 s−1. From the experimental results, most true stress-strain curves showed the typical nature of DRX that a single peak was reached at low strains followed by a decrease of stress and a steady state finally at relatively high strains. The constitutive behavior of 5CrNiMoV steel was analyzed to deduce the operative deformation mechanisms, and the correlation between flow stress, temperature, and strain rate was expressed as a sine hyperbolic type constitutive equation. Based on the study of characteristic stresses and strains on the true stress-strain curves, a DRX kinetics model was constructed to characterize the influence of true strain, temperature, and strain rate on DRX evolution, which revealed that higher temperatures and lower strain rates had a favorable influence on improving the DRX volume fraction at the same true strain. Microstructure observations indicated that DRX was the main mechanism and austenite grains could be greatly refined by reducing the temperature of hot deformation or increasing the strain rate when complete recrystallization occurred. Furthermore, a DRX grain size model of 5CrNiMoV was obtained to predict the average DRX grain size during hot forming.

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