scholarly journals Hollow Channel Formation inside Sodium Aluminoborate Glass by Femtosecond Laser Writing and Distilled Water Etching

Materials ◽  
2021 ◽  
Vol 14 (19) ◽  
pp. 5495
Author(s):  
Sergey Fedotov ◽  
Alexey Lipatiev ◽  
Tatiana Lipateva ◽  
Sergey Lotarev ◽  
Vladimir Sigaev

Recently, the effect of nanograting formation was demonstrated for binary sodium borate glass with the possibility of data storage with an enhanced level of security. The obvious disadvantage of such glass is poor chemical stability, which limits real applications. In this paper, we show that the introduction of Al2O3 allows preserving the possibility of nanograting formation with a significant increase of chemical resistance and thus to preserve optical memory applications. On the other hand, the possibility of selective etching of laser-written tracks by means of distilled water is revealed, which was not demonstrated for other types of glasses. The dependence of retardance of nanogratings form birefringence on laser writing parameters is established and discussed. Structural features of laser-modified microdomains are studied via Raman spectroscopy which revealed an increase of three-coordinated boron content. A possible mechanism of selective etching is discussed.

Author(s):  
P. S. Kotval ◽  
C. J. Dewit

The structure of Ta2O5 has been described in the literature in several different crystallographic forms with varying unit cell lattice parameters. Earlier studies on films of Ta2O5 produced by anodization of tantalum have revealed structural features which are not consistent with the parameters of “bulk” Ta2O5 crystalsFilms of Ta2O5 were prepared by anodizing a well-polished surface of pure tantalum sheet. The anodic films were floated off in distilled water, collected on grids, dried and directly examined in the electron microscope. In all cases the films were found to exhibit diffraction patterns representative of an amorphous structure. Using beam heating in the electron microscope, recrystallization of the amorphous films can be accomplished as shown in Fig. 1. As suggested by earlier work, the recrystallized regions exhibit diffraction patterns which consist of hexagonal arrays of main spots together with subsidiary rows of super lattice spots which develop as recrystallization progresses (Figs. 2a and b).


Author(s):  
K. Chien ◽  
R.C. Heusser ◽  
M.L. Jones ◽  
R.L. Van de Velde

Silver impregnation techniques have been used for the demonstration of the complex carbohydrates in electron microscopy. However, the silver stains were believed to be technically sensitive and time consumming to perform. Currently, due to the need to more specifically evaluate immune complex for localization in certain renal diseases, a simplified procedure in conjunction with the use of the microwave has been developed and applied to renal and other biopsies. The procedure is as follows:Preparation of silver methenamine solution:1. 15ml graduated, clear polystyrene centrifuge tube (Falcon, No. 2099) was rinsed once with distilled water.2. 3% hexamethylene tetramine (methenamine) was added into the centrifuge tube to the 6ml mark.3. 3% silver nitrate was added slowly to the methenamine to the 7ml mark while agitating. (Solution will instantly turn milky in color and then clear rapidly by mixing. No precipitate should be formed).4. 2% sodium borate was added to the solution to the 8ml mark, mixed and centrifuged before use.


1995 ◽  
Vol 392 ◽  
Author(s):  
Larry R. Dalton ◽  
Aaron W. Harper ◽  
Zhiyong Liang ◽  
Jingsong Zhu ◽  
Uzi Efron ◽  
...  

AbstractChromophores capable of undergoing conformational changes when exposed to ultraviolet or visible light have been synthesized with functional groups permitting attachment to polymer matrices. One class of such chromophores, containing reactive functionalities at both ends of the chromophore, are referred to as double-end crosslinkable (DEC) chromophores. These chromophores are used in the synthesis of hardened nonlinear optically active lattices and in the fabrication of buried channel nonlinear optical waveguides by photoprocessing; development of such waveguides represents a critical step in the production of polymeric electro-optic modulators. Such chromophores are also crucial to the phenomena of laser-assisted poling (also known as photochemically-induced poling). Finally, these chromophores are attached to the surface of polystyrene beads permitting the realization of room temperature spectral hole burning exploiting morphology-dependent resonances. Such resonances provide the basis of wavelength coding for the development of high density optical memories.


2021 ◽  
Author(s):  
A. S. Lipatiev ◽  
S. S. Fedotov ◽  
S. V. Lotarev ◽  
T. O. Lipateva ◽  
V. N. Sigaev

Nanomaterials ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 1335
Author(s):  
Lorenzo Bigiani ◽  
Chiara Maccato ◽  
Alberto Gasparotto ◽  
Cinzia Sada ◽  
Elza Bontempi ◽  
...  

MnO2 nanostructures were fabricated by plasma assisted-chemical vapor deposition (PA-CVD) using a fluorinated diketonate diamine manganese complex, acting as single-source precursor for both Mn and F. The syntheses were performed from Ar/O2 plasmas on MgAl2O4(100), YAlO3(010), and Y3Al5O12(100) single crystals at a growth temperature of 300 °C, in order to investigate the substrate influence on material chemico-physical properties. A detailed characterization through complementary analytical techniques highlighted the formation of highly pure and oriented F-doped systems, comprising the sole β-MnO2 polymorph and exhibiting an inherent oxygen deficiency. Optical absorption spectroscopy revealed the presence of an appreciable Vis-light harvesting, of interest in view of possible photocatalytic applications in pollutant degradation and hydrogen production. The used substrates directly affected the system structural features, as well as the resulting magnetic characteristics. In particular, magnetic force microscopy (MFM) measurements, sensitive to the out-of-plane magnetization component, highlighted the formation of spin domains and long-range magnetic ordering in the developed materials, with features dependent on the system morphology. These results open the door to future engineering of the present nanostructures as possible magnetic media for integration in data storage devices.


Author(s):  
Jang Hyun Kim ◽  
Wooyoung Jeong ◽  
Hyunseok Yang

Today many media of information storage device are formed as disks. Hence, next generation removable data storage media are shaped as disk types too. The holographic data storage system also uses a disk type photopolymer media. And then, holographic data storage system is most advanced optical memory system. Tracking servo and tilt servo control are very important research in holographic data storage system. In this paper, we propose intelligent servo control by fuzzy rules in holographic data storage system. Hence, we have found pattern of tilt servo control in holographic data storage system through fuzzy system. Fuzzy rules were generated by Genetic algorithm for controlling tilt servo. Therefore, we control tilt servo using fuzzy rules in holographic data storage system. Consequently, practical pattern of tilt servo control was found by intelligence algorithm in holographic data storage system.[1]


2009 ◽  
Author(s):  
Sergei V. Zhukovsky ◽  
Dmitry N. Chigrin ◽  
Dmitry N. Chigrin

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