scholarly journals Hot Deformation Behaviors and Intrinsic Hot Workability Map of Ti-12Mo-4Zr-5Sn Alloy Based on Physical Model and Polar Reciprocity Model

Metals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 956
Author(s):  
Peng Wan ◽  
Hang Zou ◽  
Kelu Wang ◽  
Zhengzhi Zhao ◽  
Shiqiang Lu ◽  
...  

The hot compression tests of Ti-12Mo-4Zr-5Sn alloy were tested on the thermo-mechanical simulator of Gleeble-3500 under isothermal and constant strain rate. We studied this alloy’s behavior during thermal deformation at the conditions of T = 670~820 °C, ε ˙ = 0.001~10 s−1, and deformation degree 70%. The rheological stress curves of the alloy were modified, the characteristics of the rheological stress curves were analyzed, and the activation energy map of hot deformation was established. A physical constitutive model of the alloy based on strain compensation was established, which has taken the relationship between Young’s modulus and self-diffusion coefficient and temperature into account. Moreover, the intrinsic hot workability ξ map of the alloy was established based on the polar reciprocity model. The results show that this alloy’s rheological stress will descend when the temperature of deformation rises and grow when the strain rate increases, and has negative sensitivity of temperature and positive sensitivity of strain rate. According to the error calculation, the physical constitutive model’s correlation coefficient is 0.9910 and the average relative error is 3.97%, which has good accuracy. Through the analysis of the microstructures of the instability zone and the stability zone, it was found that the instability mode of the instability zone was dominated by the local flow, and the deformation mechanism of the stability zone was dominated by the dynamic recrystallization. The optimum processing parameters of the alloy known from ξ map and metallographic structure are the following: T = 790~820 °C and ε ˙ = 0.001~0.01 s−1.

2014 ◽  
Vol 1058 ◽  
pp. 165-169 ◽  
Author(s):  
Shi Ming Hao ◽  
Jing Pei Xie

The hot deformation behaviors of 30%SiCp/2024 aluminum alloy composites was studied by hot compression tests using Gleeble-1500 thermomechanical simulator at temperatures ranging from 350-500°C under strain rates of 0.01-10 s-1. The true stress-true strain curves were obtained in the tests. Constitutive equation and processing map were established. The results show that the flow stress decreases with the increase of deformation temperature at a constant strain rate, and increases with the increase of strain rate at constant temperature, indicating that composite is a positive strain rate sensitive material. The flow stress behavior of composite during hot compression deformation can be represented by a Zener-Hollomon parameter in the hyperbolic sine form. Its activation energy for hot deformation Q is 183.251 kJ/mol. The optimum hot working conditions for this material are suggested.


Metals ◽  
2019 ◽  
Vol 9 (12) ◽  
pp. 1262 ◽  
Author(s):  
Yuhang Guo ◽  
Yaodong Xuanyuan ◽  
Chunnan Lia ◽  
Sen Yang

The dynamic microstructure evolution of Mg-3Sn-2Al-1Zn-5Li magnesium alloy during hot deformation is studied by hot compression tests over the temperature range of 200–350 °C under the strain rate of 0.001–1 s−1, whereafter constitutive equations and processing maps are developed and constructed. In most of cases, the material shows typical dynamic recrystallization (DRX) features, with a signal peak value followed by a gradual decrease. The value of Q (deformation activation energy) is 138.89414 kJ/mol, and the instability domains occur at high strain rate but the stability domains are opposite, and the optimum hot working parameter for the studied alloy is determined to be 350 °C/0.001 s−1 according to the processing maps. Within 200–350 °C, the operating mechanism of dynamic recrystallization (DRX) of Mg-3Sn-2Al-1Zn-5Li alloy during hot deformation is mainly affected by strain rate. Dynamic recrystallization (DRX) structures are observed from the samples at 300 °C/0.001 s−1 and 350 °C/0.001 s−1, which consist of continuous DRX (CDRX) and discontinuous DRX (DDRX). However, dynamic recovery (DRV) still dominates the softening mechanism. At the grain boundaries, mass dislocation pile-ups and dislocation tangle provide sites for potential nucleation. Meanwhile, flow localization bands are observed from the samples at 200 °C/1 s−1 and 250 °C/0.1 s−1 as the main instability mechanism.


2013 ◽  
Vol 833 ◽  
pp. 271-275
Author(s):  
Shi Ming Hao ◽  
Jing Pei Xie

The hot deformation behaviors of 30%SiCp/2024 aluminum alloy composites was studied by hot compression tests using Gleeble-1500 thermomechanical simulator at temperatures ranging from 350-500 °C under strain rates of 0.01-10 s-1. The true stress-true strain curves were obtained in the tests. Constitutive equation and processing map were established. The results show that the flow stress decreases with the increase of deformation temperature at a constant strain rate, and increases with the increase of strain rate at constant temperature, indicating that composite is a positive strain rate sensitive material. The flow stress behavior of composite during hot compression deformation can be represented by a Zener-Hollomon parameter in the hyperbolic sine form. Its activation energy for hot deformation Q is 153.251 kJ/mol. The optimum hot working conditions for this material are suggested.


2010 ◽  
Vol 654-656 ◽  
pp. 835-838 ◽  
Author(s):  
Wei Jie Lu ◽  
Jun Qiang Lu ◽  
Di Zhang ◽  
Hong Liang Hou

Ti-6Al-4V matrix composite (TMC) reinforced with TiB plus TiC was prepared and hydrogenated. Isothermal compression tests and high temperature tensile tests were carried out to study the effect of the hydrogen on hot deformation and superplastic deformation. The flow behaviour and microstructure evaluation of hot deformation was investigated. The results show hydrogen can reduce the flow stress and decrease the deformation temperature or increase the strain rate at the same flow stress level in hot deformation. Hydrogen increasing β phase and promoting dynamic recrystallizaiton (DRX) was considered as the main reasons for hydrogen-induced plasticity in hot deformation. The results of superplastic deformation indicate hydrogen can decrease the superplastic temperature 100°C or increase strain rate one order of magnitude at the same elongation level in superplastic deformation. Hydrogen promoting DRX were considered as the main reason for improvement of superplastic elongation.


Metals ◽  
2019 ◽  
Vol 9 (8) ◽  
pp. 880 ◽  
Author(s):  
Rongchuang Chen ◽  
Haifeng Xiao ◽  
Min Wang ◽  
Jianjun Li

In this work, hot compression experiments of 300M steel were performed at 900–1150 °C and 0.01–10 s−1. The relation of flow stress and microstructure evolution was analyzed. The intriguing finding was that at a lower strain rate (0.01 s−1), the flow stress curves were single-peaked, while at a higher strain rate (10 s−1), no peak occurred. Metallographic observation results revealed the phenomenon was because dynamic recrystallization was more complete at a lower strain rate. In situ compression tests were carried out to compare with the results by ex situ compression tests. Hot working maps representing the influences of strains, strain rates, and temperatures were established. It was found that the power dissipation coefficient was not only related to the recrystallized grain size but was also related to the volume fraction of recrystallized grains. The optimal hot working parameters were suggested. This work provides comprehensive understanding of the hot workability of 300M steel in thermal compression.


Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 605
Author(s):  
Franco Lizzi ◽  
Kashyap Pradeep ◽  
Aleksandar Stanojevic ◽  
Silvana Sommadossi ◽  
Maria Cecilia Poletti

Inconel®718 is a well-known nickel-based super-alloy used for high-temperature applications after thermomechanical processes followed by heat treatments. This work describes the evolution of the microstructure and the stresses during hot deformation of a prototype alloy named IN718WP produced by powder metallurgy with similar chemical composition to the matrix of Inconel®718. Compression tests were performed by the thermomechanical simulator Gleeble®3800 in a temperature range from 900 to 1025 °C, and strain rates scaled from 0.001 to 10 s−1. Flow curves of IN718WP showed similar features to those of Inconel®718. The relative stress softening of the IN718WP was comparable to standard alloy Inconel®718 for the highest strain rates. Large stress softening at low strain rates may be related to two phenomena: the fast recrystallization rate, and the coarsening of micropores driven by diffusion. Dynamic recrystallization grade and grain size were quantified using metallography. The recrystallization grade increased as the strain rate decreased, although showed less dependency on the temperature. Dynamic recrystallization occurred after the formation of deformation bands at strain rates above 0.1 s−1 and after the formation of subgrains when deforming at low strain rates. Recrystallized grains had a large number of sigma 3 boundaries, and their percentage increased with strain rate and temperature. The calculated apparent activation energy and strain rate exponent value were similar to those found for Inconel®718 when deforming above the solvus temperature.


2013 ◽  
Vol 554-557 ◽  
pp. 1224-1231 ◽  
Author(s):  
Cecilia Poletti ◽  
Martina Dikovits ◽  
Javier Ruete

Low alloyed steels produced by continuous casting are thermomechanically treated to achieve final high mechanical properties, meaning a good combination of strength and toughness. The hot deformation mechanisms of a micro-alloyed steel containing up to 0.1wt% of V is studied by means of hot compression tests using a Gleeble®3800 device. Austenitization of samples is carried out at 1150°C during 2 minutes followed by cooling to the deformation temperature at 1Ks-1in the range of 750 – 1150°C. The studied strain rate range is from 0.01 to 80 s-1and the total true strain achieved is of 0.7. In situ water quenching is applied after the deformation to freeze the microstructure and avoid any post dynamic effect. The Ar3temperature is determined by dilatometry experiments to be 725°C for the used cooling rate. The stress values obtained from the compression tests are evaluated at different strains to determine the strain rate sensitivity and flow instability maps and thus, to predict the formability of the material in the range of studied deformation parameters. These maps are correlated to the microstructure at specific deformation parameters.


2018 ◽  
Vol 920 ◽  
pp. 244-249 ◽  
Author(s):  
Yaroslav Erisov ◽  
Sergey Surudin ◽  
Fedor Grechnikov

The results of physical simulation of hot compression of semi-finished products, selected from a cast ingot and hot-rolled plate from aluminum-lithium alloy V-1461, in the temperature range of 400-460°C and strain rates of 1-60 s-1are presented. It is established that at a constant strain rate the flow stresses decrease with increasing test temperature, an increase in the strain rate leads to an increase in flow stresses at a constant temperature. The parameters of the hot deformation rheological model, including the Zener-Hollomon parameter and the hyperbolic sine law, are determined. It is established that the parameters of the rheological model for the cast and hot-rolled state differ insignificantly.


Author(s):  
Amir Hosein Sheikhali ◽  
Maryam Morakkabati

Abstract In this study, hot deformation behavior of SP-700 titanium alloy was investigated by hot compression tests in the temperature range of 700-9508C and at strain rates of 0.001, 0.1, and 1 s-1. Final mechanical properties of the alloy (hot compressed at different strain rates and temperatures) were investigated using a shear punch testing method at room temperature. The flow curves of the alloy indicated that the yield point phenomenon occurs in the temperature range of 800- 9508C and strain rates of 0.1 and 1 s-1. The microstructural analysis showed that dynamic globularization of the lamellar α phase starts at 7008C and completes at 8008C. The alpha phase was completely eliminated from b matrix due to deformation- induced transformation at 8508C. The microstructure of specimens compressed at 8508C and strain rates of 0.001 and 0.1 s-1showed the serration of beta grain boundaries, whereas partial dynamic recrystallization caused a necklace structure by increasing strain rate up to 1 s-1. The specimen deformed at 7008C and strain rate of 1 s-1was located in the instability region and localized shear bands formed due to the low thermal conductivity of the alloy. The processing map of the alloy exhibited a peak efficiency domain of 54% in the temperature range of 780-8108C and strain rates of 0.001- 0.008 s-1. The hot deformation activation energy of the alloy in the α/β region (305.5 kJ mol-1) was higher than that in the single-phase β region (165.2 kJ mol-1) due to the dynamic globularization of the lamellar a phase.


1980 ◽  
Vol 26 (94) ◽  
pp. 519 ◽  
Author(s):  
H. Singh ◽  
F.W. Smith

Abstract In conducting tension and compression tests on snow samples, strains and strain-rates are usually determined from the displacements of the ends of the samples. In this work, a strain-gage which mounts directly onto the snow sample during testing, was developed and was found to give accurate and direct measurements of strain and strain-rates. A commercially available 0-28 pF variable capacitor was modified to perform the required strain measurements. It is a polished metallic plunger sliding inside a metal-coated glass tube. The plunger and tube were each soldered to the end of a spring-steel wire arm. To the other end of these arms were soldered to 10 mm square pads made of thin brass shim stock. The whole device weighs 2.5 g and the low coefficient of friction in the capacitor resulted in a very low actuation force. To mount the strain gage, the pads are wetted and frozen onto the snow sample. A high degree of sensitivity was achieved through the use of “phase-lock-loop” electronic circuitry. The capacitance change caused by the strain in the sample, changes the frequency of output signal from an oscillator and thus causes the change in output from the system. In the locked state, to which the system is constantly driven by a feed-back loop, the system output is almost ripple free. The strain gages were calibrated in the field in order to take into account the effects of very low field temperatures. The calibration curves were almost linear over the travel of 15 mm, the maximum limit. The sensitivity of the system is 4 mV per strain unit, but this could be increased by an order of magnitude by minor adjustments in the circuit. Constant strain-rate tensile tests were performed on natural snow at Berthoud Pass, Colorado, U.S.A., in the density range of 140-290 kg m-3. Four strain gages were mounted onto the samples to sense any non-uniform deformation which otherwise would have gone unnoticed or caused scatter in the data. The average indication of these gages was used to construct stress—strain curves for various types of snow at different strain-rates. The effect of strain-rate on the behavior of snow was studied. “Ratcheting” in the stress-strain curve in the region where the snow becomes plastic was observed first by Kinosita in his compression tests. A similar phenomenon was observed in these tension tests. It was found that directly measured strain is quite different from that which would be calculated from sample end movement. Strain softening was not observed in these tests up to total strains of 8%. The strain-rate effects found were comparable to the results of other investigators.


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