A technical assessment of a new continuous ion exchange decolourisation plant at the Tongaat-Hulett Rossburg refinery

2019 ◽  
pp. 529-539
Author(s):  
Vincent Ndinisa ◽  
Craig Jensen ◽  
Cebisile Maharaj

The Tongaat Hulett sugar refinery in Durban has recently commissioned a continuous ion-exchange (CIX) plant which has become a third ion-exchange stage in its sugar refining process following the existing two fixed bed (FB) batch ion-exchange stages. The plant will initially be evaluated and optimised as a third polishing stage using styrenic resin but the design is such that the plant can be operated as any stage with either acrylic or styrenic resin. The installed CIX plant consists of 30 resin vessels containing 1.3 m3 of resin each and has been designed to process up to 180 m3/h of refinery liquor. At the heart of the CIX plant is the Tongaat Hulett / IONEX Separations RDA technology, which has several advantages over the conventional carousel-based continuous ion exchange systems. The plant was commissioned in November 2018 and has operated with time efficiency to date above 98%. The CIX plant has 61% less resin inventory than the Fixed Bed plant. The colour removal efficiency is comparable for both systems. The CIX plant is using 71% less water per day than the FB plant and consumes 65% less chemicals. The CIX plant is producing on average 67% less effluent and 85% less sweetwater than the FB plant per day. Part of this remarkable performance is linked to water recovery design that was incorporated into the CIX plant. Modelling of the CIX plant operating as a first ion exchange stage, showed that there would be 31% reduction in water usage compared to the current first stage and about 11% reduction in effluent generation.

2011 ◽  
pp. 718-725 ◽  
Author(s):  
Laura Diego ◽  
Fernando Martín ◽  
Marta G de Quevedo ◽  
Jaime Sagristá

The main factor affecting the raw sugar refining process is certainly “colour”. The higher colour removal, the higher is the obtained sugar yield. Therefore, colour removal is the main goal throughout the process. In a conventional sugar refinery colour is removed in the purification and decolorisation steps – the second one is normally done using ion-exchange resins – but there are some other ways of colour removal such as adding some colour removing agents (powdered carbon, sodium bisulphite, PCC [precipitated calcium carbonate]). In this article the pilot plant results of experiments of increasing colour removal in the refining process are described, such as PCC addition, 3rd carbonatation (re-purification), hydrogen peroxide addition, powdered carbon addition, sodium bisulphite addition and crystallization improvements. The good results achieved in some of these trials led to perform some industrial trials, the results of wich are summarized in this article as well.


2021 ◽  
Vol 22 (23) ◽  
pp. 12904
Author(s):  
David Tichý ◽  
Zdeněk Slouka

Electrodialysis is an electric-field-mediated process separating ions exploiting selective properties of ion-exchange membranes. The ion-exchange membranes create an ion-depleted zone in an electrolyte solution adjacent to the membrane under DC polarization. We constructed a microfluidic system that uses the ion-depleted zone to separate ions from the processed water solution. We tested the separation performance by desalting a model KCl solution spiked with fluorescein for direct observation. We showed both visually and by measuring the conductivity of the output solutions that the system can work in three modes of operation referred to as continuous desalination, desalination by accumulation, and unsuccessful desalination. The mode of operation can easily be set by changing the control parameters. The desalination factors for the model KCl solution reached values from 80 to 100%, depending on the mode of operation. The concentration factor, given as a ratio of concentrate-to-feed concentrations, reached zero for desalination by accumulation when only diluate was produced. The water recovery, therefore, was infinite at these conditions. Independent control of the diluate and concentrate flow rates and the DC voltage turned our system into a versatile platform, enabling us to set proper conditions to process various samples.


2013 ◽  
Vol 31 (7) ◽  
pp. 763-781 ◽  
Author(s):  
Ana María López Fernández ◽  
Manuel Rendueles ◽  
Mario Díaz
Keyword(s):  

1999 ◽  
Vol 40 (9) ◽  
pp. 183-190 ◽  
Author(s):  
S. G. J. Heijman ◽  
A. M. van Paassen ◽  
W. G. J. van der Meer ◽  
R. Hopman

For the removal of DOC (and colour) several treatment steps are suggested. If it is also necessary to remove hardness nanofiltration is probably the first choice. For colour removal without softening a number of adsorbents are suggested in the literature. In order to estimate the costs of these treatment steps a dynamic column model based on batch experiments was used to predict the service time of the columns filled with different adsorbents. Also the (on site) regeneration of the different adsorbents was investigated in batch experiments. Especially the ion exchange resin was very promising. The costs of the treatment of one m3 water with a column filled with an ion exchange resin was estimated for the investigated case at 0.05 Euro.


2019 ◽  
Vol 3 (1) ◽  
pp. 31 ◽  
Author(s):  
Abhishek Nambiar ◽  
Ponnivalavan Babu ◽  
Praveen Linga

Water is a key resource for sustainable development and plays a crucial role in human development. Desalination is one of the most promising technologies to mitigate the emerging water crisis. Thermal desalination and reverse osmosis are two of the most widely employed desalination technologies in the world. However, these technologies are energy intensive. Clathrate-hydrate-based desalination (HyDesal) is a potential energy-efficient desalination technology to strengthen the energy–water nexus. In our previous study, we proposed a ColdEn-HyDesal process utilizing waste Liquefied Natural Gas (LNG) cold energy based on a fixed-bed reactor configuration. In this study, we evaluated the effect of 10% propane in three different gas mixtures, namely, nitrogen (G1), argon (G2), and carbon dioxide (G3), as hydrate formers for the HyDesal process. The achieved water recovery was very low (~2%) in the presence of NaCl in the solution for gas mixtures G1 and G2. However, high water recovery and faster kinetics were achieved with the G3 mixture. To improve the water recovery and kinetics of hydrate formation for the G2 gas mixture, the effect of sodium dodecyl sulfate (SDS) was evaluated. The addition of SDS did improve the kinetics and water recovery significantly.


2020 ◽  
Vol 160 ◽  
pp. 107610
Author(s):  
Yapeng Zhang ◽  
Huan Liu ◽  
Xin Liu ◽  
Hongxia Zhu ◽  
Tianyi Fan ◽  
...  

1967 ◽  
Vol 50 (3) ◽  
pp. 423-425 ◽  
Author(s):  
E.M. Sparling ◽  
E.J. Baldi ◽  
R.O. Marshall ◽  
B. Heinemann ◽  
H.E. Walter ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document