scholarly journals Laboratory Study of Color Stability of Different Types of Materials for Temporary Constructions

Folia Medica ◽  
2020 ◽  
Vol 62 (3) ◽  
pp. 553-562
Author(s):  
Atanas V. Doshev ◽  
Diyan Slavchev ◽  
Vasko Doshev

Introduction: A temporary construction serves as a preliminary representation of the type and appearance of a future permanent one that is tailored to the patient’s requirements. Like any prosthetic construction, it should meet the functional requirements, preserve or improve chewing and speech function. No matter how well maintained a prophylactic and functional prosthetic structure is, it will not be evaluated by the patient unless it retains and restores the existing shape, size and color of the natural teeth. Aim: To determine instrumentally to what extent different colorants change the color of temporary constructions. Materials and methods: Two materials for temporary restoration were tested – Protemp II and Protemp IV, of which a total of 100 test specimens, were fabricated. Under the equal storage conditions of room temperature and no direct access to sunlight, they were exposed to five 100-ml staining solutions: Coca-Cola, coffee (espresso), berry tea, orange juice and red wine in five separate containers. Measurements of color changes in the three areas of the tooth were performed using two spectrophotometric devices – Vita EasyShade and SpectroShade, at different time intervals – immediately before placement in the staining solution, at 1, 4, 7, and 14 days. Results: The results were analysed using the SPSS Statistical Processing Program (SPSS Inc., IBM SPSS Statistics) version 21.0. They were converted to a text file with the converter of the same program. In hypothesis testing, a standard value of p ≤ 0.05 was chosen for the level of significance that rejects the null hypothesis. Conclusion: Based on this study, the strong colouring effect of coffee and red wine on these restorations was demonstrated. We can conclude that Protemp IV material showed better color stability compared to Protemp II.

2015 ◽  
Vol 1088 ◽  
pp. 519-525
Author(s):  
Hua Li Huang ◽  
Dan Feng ◽  
Hai Huan Gong ◽  
Ai Yang Song ◽  
Song Zhu

Heat-cured denture base resin is an important component in removable partial dentures and complete dentures, and has been widely used in the clinic. However, during long-term use, its appearance may be affected by varying degrees of color change, affecting the appearance and longevity of the dentures. In this study we examined the color changes and water absorption and solubility of dental base resins to investigate the color stability of four types of resin materials: New Century, Heraeus, Nissin and BASIS-HI. They were soaked in artificial saliva (as control), red wine, cola, coffee and tea separately at 37°C for 1, 4 or 12 weeks. Results are presented on which the color changes of dental base resin materials were associated with different denture base resins, soak solutions and storage times. We found that most of the dental resins became darker at prolonged immersion time. Heraeus resins showed more significant changes after soaking in red wine for 12 weeks, and its water absorption and solubility values were also greater than those of the other three types of resins. The color changes of New Century, Nissin and BASIS-HI soaked in the four solutions were relatively stable. The information obtained here will help optimize maintenance of dentures and also inform choice of denture materials.


2019 ◽  
Vol 2019 ◽  
pp. 1-8 ◽  
Author(s):  
Luca Marigo ◽  
Giuseppina Nocca ◽  
Giulia Fiorenzano ◽  
Cinzia Callà ◽  
Raffaella Castagnola ◽  
...  

The aim of this study was to evaluate the effect of light-curing protocols on two modern resin composites using different air-inhibition coating strategies. This was accomplished by assessing the amount of monomer elution, surface microhardness, and composite discoloration in different storage conditions. A total of 120 specimens were prepared using Filtek Supreme XTE (3M ESPE, Seefeld, Germany) and CeramX Universal (Dentsply DeTrey, Konstanz, Germany). Specimens were light-cured in air as per manufacturer’s instructions or in the absence of oxygen. This latter condition was achieved using three different approaches: (i) transparent polyester strip; (ii) glycerin; (iii) argon gas. Specimens were assessed for release of monomers, Vickers hardness, and discoloration after storage in different solutions. The results were analyzed with ANOVA one-way test followed by Student-Newman-Keuls test. Moreover, multiple comparisons of means were performed using the Student t-test (p<0.05). The amount of monomers released from the tested specimens was very low in all conditions. The presence of oxygen induced some decrease in microhardness. The highest discoloration values, for both materials, were obtained after ageing in red wine. In case finish and polish procedures are awkward to achieve in posteriors composite restoration, light-curing in the absence of oxygen should be considered, especially when performing composite restoration in esthetic areas.


Medicina ◽  
2020 ◽  
Vol 56 (5) ◽  
pp. 234
Author(s):  
Mohammed M. Al Moaleem ◽  
Rashad AlSanosy ◽  
Nasser M. Al Ahmari ◽  
Mansoor Shariff ◽  
Abdulkhaliq A. Alshadidi ◽  
...  

Background and Objectives: Khat chewing is considered as a daily habit that is practiced by more than five million people globally. The effect of khat chewing on the surface roughness and the color stability of natural teeth and the material used in the fabrication of dental prosthesis remains unknown. This study was conducted to explore and compare the effect of khat homogenate (KH) on the surface roughness (Ra) and the average color changes (ΔE*) amongst natural teeth and selected shades from different porcelain types, namely, feldspathic metal ceramic (MC) VM13, computer-aided design/computer assisted manufacture (CAD/CAM) feldspathic (Vitablocs Mark II), and multilayer zirconia (Ceramill Zolid PS) porcelains. Materials and Methods: Seventy samples were prepared from natural teeth, feldspathic MC, CAD/CAM Vitablocs Mark II, and zirconia porcelain. The Ra values were measured using a profilometer and expressed in micrometers, whereas the ΔE* values were measured using VITA Easyshade® V spectrophotometer for all samples before and after frequent immersion and thermocycling in KH for 30 days. The surface topography was used to assess the materials surfaces (glazed or polished) after KH immersion by using a white light interferometry machine. Results: Results revealed that the Ra and the ΔE* values of the different types of tested porcelain were influenced by KH. The order of surface roughness values was glazed or polished MC > polished Zircon > polished Vitablocs Mark II > natural teeth. The lowest ΔE* values were recorded for glazed Vitablocs Mark II and MC, and the values could be arranged as polished zircon > natural teeth > glazed zircon > polished MC > polished Vitablocs Mark II. P values were significantly varied (<0.001) among all the tested groups, except the zircon group (>0.05) for both Ra and ΔE*. Conclusions: KH significantly affected both surface parameter and color of glazed or polished porcelain materials and natural teeth.


2014 ◽  
Vol 2014 ◽  
pp. 1-8 ◽  
Author(s):  
Mieszko Wieckiewicz ◽  
Volker Opitz ◽  
Gert Richter ◽  
Klaus W. Boening

Objectives.Polyamide-12 (PA) is a flexible material suited for denture bases and clasping. This study investigated its potential aging effects with a focus on surface roughness, color stability, and elasticity.Methods.PA specimens (Valplast) of40×10×2 mm and equally measuring PMMA specimens (Palapress) as control were fabricated. Color changes after storage in air, water, coffee, and red wine(n=10)were measured using the CIEL*a*b*color specification. Elasticity after thermocycling (1000, 3000, and 7000 cycles,  n=15) was measured by three-point bending testing. Mean surface roughness (Ra) was determined after storage in the liquids mentioned above and thermocycling(n=10).Results.Tukey’s HSD test(P<0.05)revealed statistically significant color changes of PA in red wine (ΔE=4.27after 12 days,ΔE=6.90after 12 days) and coffee (ΔE=3.93after 36 days) but no color changes in PMMA. Elastic modulus of PA was 845 MPa and not affected by thermocycling (Tukey's HSD test,  P>0.81). Dry specimens showed significantly decreased elasticity(P<0.001). Mean surface roughness (PA 0.20 μm, PMMA 0.28 μm) did not change significantly after thermocycling or storage (Mann-WhitneyU-test,  0.16<P<0.65).Significance. PA exhibited a higher susceptibility to discoloration than PMMA. Neither surface roughness nor elasticity of PA was altered by artificial aging.


Materials ◽  
2020 ◽  
Vol 13 (11) ◽  
pp. 2540
Author(s):  
Aikaterini Petropoulou ◽  
Maria Dimitriadi ◽  
Spiros Zinelis ◽  
Aspasia Sarafianou ◽  
George Eliades

The purpose of this study was to investigate the surface characteristics and color stability of gingiva-colored composite restorative materials (Anaxgum—ANG, Ceramage—CMG and Gradia Gum—GRG). The microstructure, composition, degree of conversion (DC %) and 3D roughness (Sa, Sz, Sdr, Sc) were examined by LV-SEM/EDS, ATR-FTIR and optical profilometry, respectively. For the color stability (CIE L*, a*, b* system) and hardness (HV), measurements were performed at baseline and after 30 days storage in distilled water, coffee and red wine. The ANG and GRG contain prepolymerized particles in aromatic and aliphatic resin matrices, respectively, whereas CMG contains inorganic zirconia silicate/silica particles, in an aromatic resin matrix, with a smaller particle size and a higher surface area fraction. Urethane monomers were mainly identified in CMG and GRG. The DC% showed statistically insignificant differences between the materials. The same applied for the roughness parameters, except for the greatest Sdr in CMG. ANG showed a color difference (ΔE) of > 3.3 after immersion in all media, CMG in coffee and wine and GRG only in coffee. Sc was the only roughness parameter demonstrating correlations with the ΔL*, Δb* and ΔE*. The HV values showed insignificant differences between the storage conditions per material. There are important differences in the color stability of the materials tested, which were mostly affected by the roughness parameters due to variations in their microstructure.


2018 ◽  
Vol 12 (01) ◽  
pp. 049-056 ◽  
Author(s):  
Riccardo Beltrami ◽  
Matteo Ceci ◽  
Gabriele De Pani ◽  
Lodovico Vialba ◽  
Ricaldone Federico ◽  
...  

ABSTRACT Objective: To evaluate the color stability of different esthetic restorative materials after surface finishing/polishing with different procedures. Materials and Methods: All materials were polymerized into silicone rubber rings to obtain specimens identical in size. Samples were randomly assigned into four groups (10 specimens of each composite for each group), and they were finished with different procedures: Control group (Group 1), three or two polishers interspersed with diamond grit (Groups 3 and 2, respectively), and one tungsten carbide bur + one polisher interspersed with diamond grit (Group 4). After staining process in coffee, a colorimetric evaluation according to the CIE L*a*b* system was performed by a blind trained operator at 7, 14, 21, and 28 days. Shapiro–Wilk test and Kruskal–Wallis analysis of variance were applied to assess significant differences among restorative materials. Means of the different polishing/finishing groups were compared with Scheffe’s multiple comparison test at the 0.05 level of significance. Results: In control group, significant lower discolorations were recorded for Essentia, Admira Fusion, and Estelite. After finishing, Filtek Supreme XTE and Ceram.X Universal showed a significantly lower degree of staining. The finishing technique used for Group 4 produced higher color changes. Conclusions: Tungsten carbide burs produced the higher color variations; after finishing, the nanofilled composites showed lower discoloration than nanohybrid ones, and the time of exposure to the staining agent and the polishing/finishing technique influenced the color change.


2014 ◽  
Vol 15 (5) ◽  
pp. 587-594 ◽  
Author(s):  
Rafat Ibrahim Farah ◽  
Hytham Elwi

ABSTRACT Spectrophotometric evaluation of color changes of Bleachshade resin-based composites after staining and bleaching. Aim The aim of this study was to evaluate the color stability of two commercially available bleach-shade resin composites (RC) after exposure to 3 storage solutions and the effect of 3 bleaching agents on the color stability and stain removal from stained RC. Materials and methods Two bleach-shade RC were evaluated in this study, including a nanofilled RC, FiltekTM Z350 XT (FZ), and a nanohybrid RC, Tetric® N-Ceram (TC), in the extra-white body (shade) (XWB) and L shades, respectively. Twenty-seven disk-shaped specimens, each measuring 12 mm in diameter and 2 mm in thickness, were prepared for each RC, with a total of 54 specimens. Specimens were randomly allocated into 3 groups of 9 specimens each and immersed in 3 storage solutions (distilled water, tea and coffee) for 7 days period. The 9 specimens in each staining group were further divided into 3 subgroups. Specimens in each subgroup (n = 3) were bleached using one of the bleaching agents (10 and 16% Zoom NiteWhite amorphous calcium phosphate (ACP), and Zoom 2 chairside with light activation) for 5 days period. The specimen colors were measured with spectrophotometer. The measurements were performed on each sample three times at baseline, after staining, and after bleaching. Color was expressed using the commission international de I'Eclairage (CIE) L*a*b* color space. The color differences (ÄE) between the three measurements were calculated and the results were statistically analyzed using Two-way and Three-way analysis of variance (ANOVA) and Tukey's posthoc tests. Level of significance was set at p < 0.05. Results Tetric® N-ceram materials demonstrated significantly less color change than the FZ and the color change, which was greater after storage in coffee compared to tea, was statistically significant. The bleaching agents significantly influence the color changes of composite specimens. All groups showed (ÄE) values below 3.3 after bleaching, except for ‘Zoom 2 chairside’ with light activation groups, which is shown clinically unacceptable lighter shade (ÄE >3.3). Conclusion Bleach-shade composites showed significant discoloration (ÄE > 3.3) after being immersed into coffee and tea solutions. Nanofilled composites discolored more than nanohybrid composites, and carbamide peroxide-based bleaching agents were effective in reducing the discoloration to a clinically acceptable value (ÄE > 3.3). How to cite this article Farah RI, Elwi H. Spectrophotometric Evaluation of Color Changes of Bleach-shade Resin-based Composites after Staining and Bleaching. J Contemp Dent Pract 2014;15(5):587-594.


2014 ◽  
Vol 19 (4) ◽  
pp. 114-121 ◽  
Author(s):  
Cibele Braga de Oliveira ◽  
Luiz Guilherme Martins Maia ◽  
Ary Santos-Pinto ◽  
Luiz Gonzaga Gandini Júnior

OBJECTIVE: The aim of this in vitro study was to analyze color stability of monocrystalline and polycrystalline ceramic brackets after immersion in dye solutions. METHODS: Seven ceramic brackets of four commercial brands were tested: Two monocrystalline and two polycrystalline. The brackets were immersed in four dye solutions (coffee, red wine, Coke and black tea) and in artificial saliva for the following times: 24 hours, 7, 14 and 21 days, respectively. Color changes were measured by a spectrophotometer. Data were assessed by Multivariate Profile Analysis, Analysis of Variance (ANOVA) and Multiple Comparison Tests of means. RESULTS: There was a perceptible change of color in all ceramic brackets immersed in coffee (ΔE* Allure = 7.61, Inspire Ice = 6.09, Radiance = 6.69, Transcend = 7.44), black tea (ΔE* Allure = 6.24, Inspire Ice = 5.21, Radiance = 6.51, Transcend = 6.14) and red wine (ΔE* Allure = 6.49, Inspire Ice = 4.76, Radiance = 5.19, Transcend = 5.64), but no change was noticed in Coke and artificial saliva (ΔE < 3.7). CONCLUSION: Ceramic brackets undergo color change when exposed to solutions of coffee, black tea and red wine. However, the same crystalline structure, either monocrystalline or polycrystalline, do not follow the same or a similar pattern in color change, varying according to the bracket fabrication, which shows a lack of standardization in the manufacturing process. Coffee dye produced the most marked color changes after 21 days of immersion for most ceramic brackets evaluated.


2015 ◽  
Vol 44 (5) ◽  
pp. 262-267 ◽  
Author(s):  
José Vitor Quinelli Mazaro ◽  
Luiz Miguel Minani ◽  
Adriana Cristina Zavanelli ◽  
Caroline Cantieri de Mello ◽  
Cleidiel Aparecido Araújo Lemos

AbstractIntroductionTemporary restorative materials are widely used, however, little is know about their color stability.Objectiveto evaluate the color stability of the following temporary restorative materials: acrylic and bis-acrylic resins after immersion in pigmenting solutions for different periods of storage.Material and methodFour materials were tested (Dêncor/Clássico, Protemp 4/3M ESPE; Structur 2 SC/Voco; Luxatemp AM Plus/DMG) and 30 test specimens (15 mm in diameter and 2 mm thick) per material were fabricated. They were divided according to the storage medium (artificial saliva, saliva + cola type soda, and saliva + coffee) and storage time intervals (2, 5, 7 and 15 days). Color measurements were made before and after immersions, with use of a spectrophotometer, by means of the CIE L*a*b* system. The data were analyzed by the analysis of variance and the Tukey Test, at a level of significance of 5%.ResultAcrylic resin presented greater color stability in comparison with bis-acrylic resins (p<0.001). When bis-acrylic resins were compared no significant difference was observed between the resins Structur and Luxatemp (p=0.767). As regards solutions tested, coffee showed the highest color change values (p<0.001), and the longer the storage time interval, the greater was the color change in all the temporary restorative materials analyzed (p<0.001).ConclusionAcrylic resin presented greater color stability in comparison with bis-acrylic resins (p<0.001). Coffee caused the greatest color change, and immersion time was determinant in color stability of the temporary materials analyzed.


2020 ◽  
Vol 14 (01) ◽  
pp. 085-091
Author(s):  
Sedighe Sadat Hashemikamangar ◽  
Farnoosh Hoseinpour ◽  
Nazanin Kiomarsi ◽  
Mehrzad Gholampour Dehaki ◽  
Mohammad Javad Kharazifard

Abstract Objectives This study aimed to assess the effect of an optical whitening toothpaste on color stability of microhybrid, nanofilled, and microfilled composite resins and resin-modified glass ionomer (RMGI) cement in comparison of two other toothpastes. Materials and Methods In this experimental study, disc-shaped composite samples were fabricated. The samples were then polished using silicon carbide papers. Twenty-seven samples of each material were fabricated and subjected to colorimetry using a spectrophotometer. Each group of material was then divided into three subgroups for the application of conventional whitening and whitening containing blue covarine toothpastes. One operator brushed the samples with an electric soft toothbrush with circular motion twice a day, each time for 30 seconds. Colorimetry was performed at 0, 1, 7, 30, and 90 days. Statistical Analysis Two-way analysis of variance (ANOVA), one-way ANOVA, and Tukey’s honestly significant difference (HSD) test were used for statistical analysis. Results The interaction effect of type of restorative material and time on ∆E was not significant at baseline or 1 day (p > 0.05). The effect of type of toothpaste on ∆E was not significant at baseline or 1 day (p = 0.78) but the effect of type of material was significant (p < 0.05). The toothpastes had significantly different effects on ∆E of Z250 at all time points (p < 0.05) except for ∆E0–30 (p = 0.106). The toothpastes had significantly different effects on ∆E of Z350 and Gradia at all time points (p < 0.05). The same was true for RMGI except for ∆E0–7 (p = 0.43) and ∆E0–90 (p = 0.52). The majority of color changes caused by toothpastes were not clinically perceivable (∆E < 3.3), except for ∆E0–90 by the whitening toothpaste (∆E = 9), ∆E0–90 by the conventional toothpaste for Z350 (∆E = 3.9), and ∆E0–1 by the whitening toothpaste for RMGI (∆E = 3.7). Conclusion The color change of all composite samples was not clinically perceivable (<3.3) at all time points, which shows that the tested toothpastes do not cause a significant change in color of composite materials.


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