Optimization of Extracting Condition of Active Components in Perilla by Ultrasonic

2014 ◽  
Vol 1033-1034 ◽  
pp. 713-716
Author(s):  
Dan Huang ◽  
You Qing Liu ◽  
Yuan Liang ◽  
Xiang Mao

Using ultrasonic-extraction technology, the condition of extracting the active compounds-flavonoids and rosmarinic acid ofPerillawas studied. The effects of four main factors include ultrasonic power, temperature, time and solid-liquid ratio on the extraction-rate of the flavonoids and the rosmarinic acid ofPerillawere reviewed by single factor experiments,and the flavonoids and the rosmarinic acid was determined by NaNO2-Al (NO3)3-NaOH method and FeSO4method. On the base of single factor experiments, the extraction technique was optimized in the orthogonal test. The result showed that temperature was the most important factor in the influencing factors on the extraction-rate. The subsequence of importance was temperature > time > solid-liquid ratio > ultrasonic. The optimal extraction conditions were: extraction solvent 3%borax, solid-liquid ratio 1:50(w/v), ultrasonic power 300W, time 90min , temperature 75°C. Under the optimum technological conditions, 34.64mg/g of flavonoids and rosmarinic acid fromPerillacould be obtained.

2012 ◽  
Vol 550-553 ◽  
pp. 1071-1075
Author(s):  
Yong Guang Bi ◽  
Chun Chun Liu

In order to study the the Chuanxiong polysaccharide ultrasonic extraction process, examine the ultrasonic time, ultrasonic power, solid-liquid ratio and extraction temperature on the Chuanxiong polysaccharide extract rate. The results show that the role of time at 30min Polysaccharide better, the extraction rate is 26.63%. when the ultrasonic power is 320W, Polysaccharide extraction rate is 26.15%.When the solid-liquid ratio is 1:20, polysaccharide extraction rate is 27.73%. When the extraction temperature is 60°C, the polysaccharide extraction rate is 27.73%.


2012 ◽  
Vol 550-553 ◽  
pp. 1629-1632 ◽  
Author(s):  
Yu Hong Zou ◽  
Qiu Xia Han ◽  
Lin Guo

To optimize the extraction process of total flavonoids from RADIX RHIZOMA GLYCYRRHIZAE and Study on the Antioxidant Activity. Total flavonoids were extracted from RADIX RHIZOMA GLYCYRRHIZAE with ethanol by ultrasonic-assisted method, whose extraction process was optimized by orthogonal test design.The scavenging effect of pumpkin polysaccharide on OH and O2-were studied by salicylic acid and pyrogallic acid method. The optimum extraction process was as follows: ethanol concentration of 75%, solid-liquid ratio of 1:25,ultrasonic power of 350 W and ultrasonic duration of 25 min.Under the above conditions, the extraction rate of total flavonoids reached as high as 1.943%. The influencing order of each factor on extraction rate of polysaccharides was determined to be: ethanol concentration>solid-liquid ratio>ultrasonic power>ultrasonic duration. When the solution concentration is 1.1296mg/ml, the scavenging rate of crude flavonoids on superoxide radical is 50%.Suggesting that it would be an effctive natural free radical scavenger. The study could provide a scientific basis for the further exploitation and utilization of RADIX RHIZOMA GLYCYRRHIZAE


2021 ◽  
Vol 251 ◽  
pp. 02052
Author(s):  
Feng Xuehua ◽  
Song Zurong ◽  
Tao Ali ◽  
Gong Panpan

Using pitaya as raw material, this paper used ethanol subsiding method to study the extraction technology of pitaya polysaccharide by single factor test and orthogonal test. Through orthogonal test, we have found the optimum extraction conditions of pitaya polysaccharide as follows: extraction temperature 60℃, solid-liquid ratio 1:30, extraction time 3h. Under the optimal extraction conditions, the yield of pitaya polysaccharide was 1.13%.


2013 ◽  
Vol 781-784 ◽  
pp. 606-609
Author(s):  
Chen Guang Jiang ◽  
Qing Jie Tang

Balsam pear was used as the research object in experiment, the technological parameters were studied such as the way of crushing, leaching agent type and its concentration, solid-liquid ratio, ultrasonic extraction temperature, time, power's influence on the extraction yield of Vc, and the ultrasonic extraction time, temperature, ultrasonic power on the L9 (34) orthogonal test analysis. Results showed that bitter melon slices, and solid-liquid ratio is 1:7, citric acid as leaching agent and the concentration of 1%, ultrasonic power is 80 w, leaching temperature 30 °C, 40 min leaching time, leaching of balsam pear Vc the highest rate.


2013 ◽  
Vol 781-784 ◽  
pp. 1194-1198
Author(s):  
Yan Ge ◽  
Rong Kai Ma ◽  
Li Sheng Wang ◽  
Xuan Hai Li ◽  
Xuan Luo

Single factor experiments and orthogonal experiments were successively carried out to optimize the water extraction technology of flavonoids in Thlaspi arvense Linn. Results showed that the influential order of factors was extraction times >solid-liquid ratio >extraction time. The optimum conditions were adding 16 times amount of water, extracting 3 times and every time with 4 hours. Under these conditions, the yield of flavonoids from Thlaspi arvense Linn was 1.17%.


2013 ◽  
Vol 634-638 ◽  
pp. 1016-1021
Author(s):  
Li Sheng Wang ◽  
Wei Wang ◽  
Yan Ge ◽  
Jiangtao Tang

Single factor experiments and orthogonal experiments were successively carried out to optimize the water extraction technology of flavonoids in Emilia sonchifolia (Linn.) DC. The results showed that the influential order of factors was extraction times >solid-liquid ratio >extraction time. The optimum conditions were 15:1 of solid-liquid ratio, 2h of the extraction time and 3 of the extraction times. Under these conditions, the extraction yield of flavonoids from Emilia sonchifolia (Linn.) DC was 3.35%.


2013 ◽  
Vol 690-693 ◽  
pp. 1400-1403
Author(s):  
Hong Li Zhou ◽  
Li Cheng ◽  
Shi Lin

To study the extraction technology of polysaccharide from Pleurotus ostreatus. In order to explore the influence of temperature, time, and solid-liquid ratio on polysaccharide yield, single factor test had been done. The optimum extraction conditions was obtained though orthogonal test and interactive analysis: extraction temperature 50°C, extraction time 2h, and solid-liquid ratio 1:30. Under those conditions, the extraction rate of Pleurotus ostreatus polysaccharides was 28.79%.


2014 ◽  
Vol 1082 ◽  
pp. 106-111
Author(s):  
Yu Hong Yang ◽  
Zong Li Kang ◽  
Rui Xin Guo ◽  
Hong Ling Wang ◽  
Zhuo Wang ◽  
...  

We had studied using single factor and orthogonal experimental design method for extracted from actinidia arguta of wild fructification polyphenols conditions optimization, as actinidia arguta of wild raw material. The results showed that: extracted from actinidia arguta of wild fructification polyphenols optimization the best conditions is acetone solution of 30 percent, according to the solid-liquid ratio of 1:9, at 35°C, the extraction 30 min best, the amount of polyphenols extracted 763.8 mg / L.


2014 ◽  
Vol 955-959 ◽  
pp. 1466-1470 ◽  
Author(s):  
Dan Liu ◽  
Fang Yu ◽  
Wei Tan ◽  
Gui Zhen Li ◽  
Min Yang ◽  
...  

Response surface methodology based on single factors was used to optimize the process condition for extraction of nitrite nitrogen in sediment . The results indicated that the extraction amount of nitrite nitrogen was 9.5μg /g under the optimum condition of extraction time of 44min, ultrasonic power of 280W, solid-liquid ratio of 1:19,which was closed to the predicated yield of 9.3μg/g. The process can be used for the extraction of nitrite nitrogen in sediments.


2011 ◽  
Vol 201-203 ◽  
pp. 2935-2938
Author(s):  
Guo En Yang ◽  
Gui Wu Wang ◽  
Zhi Ping Wu ◽  
Xiang Zhou Li

Evaluated with the yield of anise star oil, steam extraction method assisted by microwave is studied for the extraction of anise star oil from Illicium verum Hook. f. in contrast with the traditional steam distillation (SD) method in this paper. The new optimal steam extraction technology assisted by microwave of anise star oil is obtained as: extracting time 80 minutes, solid-liquid ratio(g/mL) 1:7, size of material 80~100 mesh and extracting temperature 80°C. Average yield of anise star oil is up to 11.6% (g/g) under the above technology. Size of material is the most important influencing factor in the extraction process. The optimal traditional steam distillation technology is: extracting time 120 minutes, solid-liquid ratio(g/mL) 1:6, size of material 80~100 mesh and extracting temperature 100°C , the average yield of anise star oil is only 9.81% (g/g). The steam extraction technology assisted by microwave has advantages in both the technological conditions and the yield of anise star oil than the traditional steam distillation technology.


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