Hot Pin Pull Method – New Test Procedure for the Adhesion Measurement for 3D-MID

2014 ◽  
Vol 1038 ◽  
pp. 115-120 ◽  
Author(s):  
Christian Goth ◽  
Thomas Kuhn ◽  
Gerald Gion ◽  
Jörg Franke
Keyword(s):  
Test Procedure ◽  
Test Methods ◽  
Test Method ◽  
Testing System ◽  
Adhesion Test ◽  
Metallic Structures ◽  
Adhesion Measurement ◽  
Molded Interconnect Devices ◽  
Unsolved Issue

The adhesion test of metallic structures on MID (Molded Interconnect Devices) parts is an unsolved issue. So far no method really works reliably. The test methods which are conventionally used are the pull-off test and the shear-test. Both show large standard deviation and the reproducibility is not assured. Nordson DAGE has introduced the new micro-material testing system 4000Plus. This device enables a new test method for the determination of the adhesion strength of MID structures using the hot pin pull (hot bump pull) method. Copper pins (tinned or untinned) are heated up with a user defined temperature profile, soldered to a metallized structure on the MID and then removed vertically upward, while the force is recorded. In this contribution investigations with this new test method are presented.

The modern methods of pin-type bearing test of metallic materials

2019 ◽  
Vol 85 (7) ◽  
pp. 41-49
Author(s):  
Yaroslava V. Sulimina ◽  
Nikolay O. Yakovlev ◽  
Vladimir S. Erasov ◽  
Aleksey Yu. Ampilogov ◽  
Andrey N. Polyakov ◽  
...  
Keyword(s):  
Elastic Modulus ◽  
Test Procedure ◽  
Test Methods ◽  
Test Method ◽  
Strength Characteristics ◽  
Metallic Materials ◽  
Bearing Strength ◽  
Bearing Stress ◽  
The Impact

The special features of various bearing deformation measurements for pin-type bearing tests of metallic materials are considered along with their impact on the magnitude of the «bearing elastic modulus» and bearing stress. These bearing test methods are present in ASTM and various institutional standards, though no state standard (GOST, GOST R) is currently available for bearing test method of metallic materials. Analysis of additional deformations which arise in determining the degree of hole bearing deformation is carried out. A set of sources of additional deformations is shown to be characteristic for each test procedure and is attributed to the design features of the device, the site and a way of mounting the extensometer. Additional deformations can be both tensile and compressive. It is shown that the impact of additional deformations on the «bearing elastic modulus» is limited to 14% for different procedures. No difference between the methods is revealed with regard to determination of the strength characteristics. At the same time the dispersion decreases with increase in plastic deformation and for bearing deformation about 4% the variation coefficient for all methods is no more than 1%. Advantages and shortcomings of the bearing test methods which affect the reproducibility of the results are considered. The effect of the specimen geometry on the bearing characteristics is considered. It is shown that increase both in the distance from the edge of the bearing specimen to the center of the hole for 1163T, VT6ch, 30KhGSA alloys and residual bearing deformation up to 6%, increase bearing strength characteristics.

scholarly journals Problems of the dynamic test method for individual protection equipment (shock absorbers)

2018 ◽  
Vol 193 ◽  
pp. 05034 ◽  
Author(s):  
Dmitry Korolchenko ◽  
Vasily Vasilenko ◽  
Georgy Lelikov
Keyword(s):  
Dynamic Performance ◽  
Dynamic Test ◽  
Test Methods ◽  
Test Method ◽  
Testing System ◽  
Protective Properties ◽  
Shock Absorbers ◽  
Individual Protection ◽  
European Standards ◽  
Protective Performance

This paper examines issues of safety of high-altitude works, using individual protection equipment to prevent falling from a height. In particular, the paper reviews personal protective equipment - shock absorber, its dynamic characteristics and related test methods to meet the requirements of Technical Regulations 019/2011 “Safety of Individual Protection Equipment”. The paper discusses the differences between the Russian and European standards for dynamic characteristic testing of shock absorbers, even as the former are harmonized texts of the latter, and the effect of such differences on protective performance of shock absorbers and ultimately on safety of works on heights. It have been shown that tests, conducted in accordance with the Russian regulative documents for dynamic performance of the shock absorbers, entail decreasing in safety usage of such type of IPE and increasing in injuries during falls from a height. It has been defined necessity to actualize the range of the testing system of shock absorbers, and to admit its larger value that will cause increase in protective properties of shock absorbers.

Use of Integrated Day-Long Stagnation Temperature for Measuring Changes in Solar Collector Materials Properties

1985 ◽  
Vol 107 (2) ◽  
pp. 170-175
Author(s):  
W. C. Thomas ◽  
A. G. Dawson ◽  
D. Waksman
Keyword(s):  
Analytical Model ◽  
Test Procedure ◽  
Daily Basis ◽  
Test Methods ◽  
Test Method ◽  
Solar Irradiation ◽  
Stagnation Temperature ◽  
Nonsteady State ◽  
Materials Used ◽  
Energy Absorbing

Measurements of the maximum temperatures reached by solar-energy-absorbing surfaces provide a useful method for detecting possible degradation in the optical and heat transfer properties of materials used in collectors. This investigation shows that a method based on integrating the absorber temperature rise over ambient and solar irradiation on a daily basis has advantages over alternative test methods based on steady-state measurements of either absorber stagnation temperature or collector thermal efficiency. A nonsteady-state analytical model is developed and used to evaluate the sensitivity of the proposed test method to material degradation and environmental effects. Outdoor data are presented to validate the analytical model and depict typical results that can be expected using the test procedure.

Study on the Bearing Capacity Test for the Saline Soil Soft Ground

2014 ◽  
Vol 587-589 ◽  
pp. 947-951
Author(s):  
Jun Yong Liu ◽  
Liu Jun Zhang
Keyword(s):  
Bearing Capacity ◽  
Saline Soil ◽  
Test Methods ◽  
Test Method ◽  
Soft Ground ◽  
Characteristic Value ◽  
Soft Foundation

The test methods provided by current related "specifications" do not apply to saline soil soft foundation bearing capacity test. Through discussing the limitations of the related specifications and based on the experience on saline soil soft ground capacity test, the paper made some improvements of test on such aspects: conditions of loading and stopping load, determination of the characteristic value of the ground bearing capacity and evaluation, the paper also put forward the saline soil soft ground capacity test method.

scholarly journals Analysis of Vitamin A in Multivitamin Products

2021 ◽  
Vol 11 (3) ◽  
pp. 174-184
Author(s):  
A. S. Alekseeva ◽  
T. B. Shemeryankina ◽  
M. N. Lyakina ◽  
M. S. Smirnova ◽  
E. P. Fedorova ◽  
...  
Keyword(s):  
Vitamin A ◽  
High Performance ◽  
Beta Carotene ◽  
Test Methods ◽  
Retinyl Palmitate ◽  
Test Method ◽  
Medicinal Products ◽  
Retinyl Acetate ◽  
Preliminary Purification

Vitamin A is present in multivitamin products mainly in the form of retinol esters: retinyl acetate, retinyl palmitate, and beta carotene—retinol precursor (dimer) found in plants, which is capable of converting into retinol in liver cells. Retinol is determined in medicinal products primarily by high performance liquid chromatography (HPLC), with preliminary purification and vitamin isolation by liquid-liquid extraction. However, scientific literature also describes other methods of sample preparation and analysis of such compounds. An important issue is differentiation of vitamin A from other fat-soluble vitamins often included as components in multivitamin products. The aim of the study was to analyse and summarise data on current methods used for determination of vitamin A and its derivatives in medicinal products. The authors analysed the range of vitamin A products authorised in the Russian Federation, and the test methods described in their product specification files. The study demonstrated that the test method most often used for determination of retinol esters was HPLC with isocratic elution mode using octadecylsilyl packing in the reverse-phase mode, and, less frequently, aminopropylsilyl packing in the normal phase mode. Determination of beta carotene in medicinal products is most often performed using spectrophotometry. 

scholarly journals What are the Alternatives of PG Plus Tests for Modified Asphalt Binders?

2019 ◽  
Vol 271 ◽  
pp. 03008
Author(s):  
MM Tariq Morshed ◽  
Mohammad Nazmul Hassan ◽  
Zahid Hossain
Keyword(s):  
Elastic Recovery ◽  
Test Procedure ◽  
Test Methods ◽  
Test Method ◽  
Asphalt Binders ◽  
Performance Grade ◽  
Empirical Performance ◽  
Alternative Test ◽  
Styrene Butadiene ◽  
Departments Of Transportation

For characterizing the polymer modified binders, different state Departments of Transportation (DOTs) use different time consuming and empirical Performance Grade (PG) Plus test methods. Furthermore, the PG Plus tests are silent when asphalt binders are modified with chemicals such as polyphosphoric acid (PPA). But, the effects of the polymer are not accurately identified through these conventional tests such as Elastic Recovery (ER) and tenacity. The main goal of this study is to recommend alternative test method(s), which can possibly be pursued by using, a Dynamic Shear Rheometer (DSR). Thus, Multiple Stress Creep and Recovery (MSCR), ER-DSR, Frequency Sweep, and Binder Yield Energy Test (BYET) are being explored to find their effectiveness. Three PG binders (PG 64-22, PG 70-22 and PG 76-22) have been selected for this investigation. These binders have been prepared with styrene-butadiene-styrene (SBS) polymer, PPA, or a combination of both. Further, chemical tests such as SARA (Saturate, Aromatic, Resin, and Asphaltene) analysis and FTIR (Fourier-transform Infrared spectroscopy) are also being explored to fulfill the objectives. Preliminary findings suggest that the PG Plus tests deem to be obsolete. Also, a single test procedure is not sufficient to identify the presence and effectiveness of modifiers in the PG binders.

Test Method for Determination of Virucidal Efficacy of Liquid Surface Disinfectants

1976 ◽  
Vol 59 (5) ◽  
pp. 1150-1155
Author(s):  
Charles R McDuff ◽  
John W Gaustad
Keyword(s):  
Collaborative Study ◽  
Test Procedure ◽  
Test Method ◽  
Virus Concentration ◽  
Ammonium Compound ◽  
Concentration Technique ◽  
Modified Method ◽  
Culture Cells

Abstract A test method was developed incorporating AOAC use-dilution stainless steel Penicylinders and H.Ep.-2 tissue culture cells for the evaluation of disinfectants as virucides. The subsequent collaborative study using Herpes simplex and poliovirus type 1 in evaluation against a quaternary ammonium compound, phenolic, and iodiphor disinfectants indicated that the basic test procedure is sound. However, an improved virus concentration technique and a modified method for drying virus-contaminated cylinders are recommended. In addition, other types of disinfectants and test viruses should be included in order to demonstrate that the procedure is versatile as well as reproducible.

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