Effect of Minor Silver Addition on Microstructure and Properties of Al-8Zn-1.Cu-1.3Mg-0.1Zr Alloys

2013 ◽  
Vol 834-836 ◽  
pp. 360-363
Author(s):  
X.Z. Wu ◽  
D.H. Xiao ◽  
Z.M. Zhu ◽  
X.X. Li ◽  
K.H. Chen

Effects of minor silver addition on microstructure, mechanical properties and corrosion resistances of Al-8Zn-1.Cu-1.3Mg-0.1Zr alloys were investigated using optical microscope (OM), scanning electron microscopy (SEM), mechanical properties and corrosion testing. The results show that minor silver addition decreases the recrystallization and corrosion resistance of the t77-tempered alloys.Tensile strength of the based alloy was increased by the 0.1 wt% silver addition.

2012 ◽  
Vol 562-564 ◽  
pp. 204-207
Author(s):  
Dong Wang ◽  
Hui Qin Li ◽  
Han Yu Zhao

In this study, 45 carbon steel was boronized and borosulphurized at 950°C for 2, 3, 4, 5, 6 and 8 h, respectively. The samples were characterized by scanning electron microscopy, optical microscope, microhardness tester and ring-on-block wear tester. It is found that the surface of borosulphurized samples was dense, compact and relatively smooth; Although the boride layers produced by boro- sulphurizing at 950°C showed a lower microhardness value compared with that produced by boronizing, the wear resistance of the borosulphurized carbon steel is higher than that of boronized sample due to formation of FeS phase in the boride layer.


2018 ◽  
Vol 202 ◽  
pp. 01001
Author(s):  
R. Ahmad ◽  
A.M.M. Elaswad ◽  
M. Z. Hamzah ◽  
N. R. Shahizan

The thermal parameters of Mg-2.8Nd-1.5Gd-0.5Zn-0.5Zr cast alloy with 0.25 wt.% of erbium (Er) were evaluated by the computer-aided cooling curve thermal analysis(CA CCTA), whereas the microstructure analysis was investigated by the optical microscope and scanning electron microscopy. Results from the cooling curve and microstructure analysis showed that Er altered the grain size of the alloys. In addition, the grain size was reduced by approximately 19.6% with the addition of Er. Scanning electron microscopy results showed that Er formed an Mg-Zn-Nd-Er phase which distributed along the grain boundaries. Furthermore, the mechanical properties were investigated by hardness and tensile tests with Er addition. The addition of 0.25 wt.% of Er significantly improved the ultimate tensile strength and yield strength. In addition, the hardness value of Mg-2.8Nd-1.5Gd-0.5Zn-0.5Zr increased by 13.9% with Er addition.


2009 ◽  
Vol 154 ◽  
pp. 107-112 ◽  
Author(s):  
Anna Boczkowska ◽  
Stefan F. Awietjan

In this paper studies on urethane magnetorheological elastomers (MREs) microstructure in respect to their magnetic and mechanical properties are reported. MREs were obtained from a mixture of polyurethane gel and carbonyl-iron particles cured in a magnetic field of 100 and 300 mT. The amount of particles was varied from 1.5 to 33 vol. %. Samples with different arrangements of particles were produced. Effect of the amount of ferromagnetic particles and their arrangement on microstructure and properties in relation to the external magnetic field was investigated. The microstructure was studied using scanning electron microscopy. Magnetic properties were measured using vibrating sample magnetometer. Rheological and mechanical properties under compression were also examined.


2014 ◽  
Vol 590 ◽  
pp. 181-186
Author(s):  
Xiao Song Li ◽  
An Hui Cai ◽  
Ji Jie Zeng

Using optical microscope, electronic tensile testing machine, scanning electron microscopy methods, such as detailed treatment of the B hypoeutectic Al-Si alloy microstructure, mechanical properties and fracture morphology were studied. The results showed that after treatment by the B refinement, α-Al dendrite phase was refined, resulting in mechanical properties of Al-Si alloy significantly improved. Which, B content 0.036wt.%, the alloy the best, the σb, δ, respectively, than the non-thinning increased 67.8% and 15.2%. From the fracture surface, the fracture morphology of the specimen showed a quasi-cleavage fracture. Which, B content 0.036wt.% at the time of fracture is more deep dimples, and a good plastic toughness.


2011 ◽  
Vol 217-218 ◽  
pp. 1454-1457
Author(s):  
Xiao Ming Chen ◽  
R.G. Song

The microstructure and properties of 7003 aluminum alloy with and without burning have been investigated by means of electronic tensile machine, optical microscope (OM) and scanning electron microscopy (SEM). The results showed that the burning level of 7003 alloy increases while the ultimate tensile strength (UTS) and yield strength (YS) for the alloy decrease with increasing the solution temperature. When the solution temperature is higher than 763 K, the UTS and YS for the alloy decline fast with wide-range. The remelting structure, namely burnt structure, appeared on the grain boundaries in 7003 aluminum alloy and then weaken grain boundary, hence resulting in the transition of fracture surfaces from transgranular fracture to intergranular fracture.


2011 ◽  
Vol 194-196 ◽  
pp. 1590-1593
Author(s):  
Jie Jin ◽  
Maolin Ni ◽  
Shen Hao Wang

In the article, porous silicon carbide composite is prepared based on stereo lithography apparatus (SLA). The microstructure of porous silicon carbide composite is characterized by mean of scanning electron microscopy (SEM). The properties of porous silicon carbide composite are studied, such as surface HV and corrosion resistance, and the influence of the pore agent content to mechanical properties.


Author(s):  
Li Li-Sheng ◽  
L.F. Allard ◽  
W.C. Bigelow

The aromatic polyamides form a class of fibers having mechanical properties which are much better than those of aliphatic polyamides. Currently, the accepted morphology of these fibers as proposed by M.G. Dobb, et al. is a radial arrangement of pleated sheets, with the plane of the pleats parallel to the axis of the fiber. We have recently obtained evidence which supports a different morphology of this type of fiber, using ultramicrotomy and ion-thinning techniques to prepare specimens for transmission and scanning electron microscopy.


Polymers ◽  
2021 ◽  
Vol 13 (13) ◽  
pp. 2174
Author(s):  
Diana Gregor-Svetec ◽  
Mirjam Leskovšek ◽  
Blaž Leskovar ◽  
Urška Stanković Elesini ◽  
Urška Vrabič-Brodnjak

Polylactic acid (PLA) is one of the most suitable materials for 3D printing. Blending with nanoparticles improves some of its properties, broadening its application possibilities. The article presents a study of composite PLA matrix filaments with added unmodified and lignin/polymerised lignin surface-modified nanofibrillated cellulose (NFC). The influence of untreated and surface-modified NFC on morphological, mechanical, technological, infrared spectroscopic, and dynamic mechanical properties was evaluated for different groups of samples. As determined by the stereo and scanning electron microscopy, the unmodified and surface-modified NFCs with lignin and polymerised lignin were present in the form of plate-shaped agglomerates. The addition of NFC slightly reduced the filaments’ tensile strength, stretchability, and ability to absorb energy, while in contrast, the initial modulus slightly improved. By adding NFC to the PLA matrix, the bending storage modulus (E’) decreased slightly at lower temperatures, especially in the PLA samples with 3 wt% and 5 wt% NFC. When NFC was modified with lignin and polymerised lignin, an increase in E’ was noticed, especially in the glassy state.


Coatings ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 652
Author(s):  
Divine Sebastian ◽  
Chun-Wei Yao ◽  
Lutfun Nipa ◽  
Ian Lian ◽  
Gary Twu

In this work, a mechanically durable anticorrosion superhydrophobic coating is developed using a nanocomposite coating solution composed of silica nanoparticles and epoxy resin. The nanocomposite coating developed was tested for its superhydrophobic behavior using goniometry; surface morphology using scanning electron microscopy and atomic force microscopy; elemental composition using energy dispersive X-ray spectroscopy; corrosion resistance using atomic force microscopy; and potentiodynamic polarization measurements. The nanocomposite coating possesses hierarchical micro/nanostructures, according to the scanning electron microscopy images, and the presence of such structures was further confirmed by the atomic force microscopy images. The developed nanocomposite coating was found to be highly superhydrophobic as well as corrosion resistant, according to the results from static contact angle measurement and potentiodynamic polarization measurement, respectively. The abrasion resistance and mechanical durability of the nanocomposite coating were studied by abrasion tests, and the mechanical properties such as reduced modulus and Berkovich hardness were evaluated with the aid of nanoindentation tests.


2019 ◽  
Vol 7 (1) ◽  
Author(s):  
Liu Liu ◽  
Decai Gong ◽  
Zhengquan Yao ◽  
Liangjie Xu ◽  
Zhanyun Zhu ◽  
...  

Abstract Historically, sutras played an important role in spreading Buddhist faith and doctrine, and today these remain important records of Buddhist thought and culture. A Mahamayuri Vidyarajni Sutra with polychrome paintings was found inside the cavity on top of the Nanmen Buddhist pagoda, built in the early Tang dynasty (618–627 CE) and located in Anhui Province, China. Textile was found on the preface which is strongly degraded and fragile. Unfortunately, the whole sutra is under severe degradation and is incomplete. Technical analysis based on scientific methods will benefits the conservation of the sutra. Optical microscopy (OM), micro-Raman spectroscopy combined with optical microscope (Raman), scanning electron microscopy in combination with energy dispersive X-ray analysis (SEM–EDS) and Fourier Transform Infrared Spectroscopy (FTIR) were used to characterize the pigment and gilded material, as well as the paper fiber and textile. Pigments such as cinnabar, minium, paratacamite, azurite, lead white were found. Gilded material was identified as gold. A five-heddle warp satin, made of silk, was found as the textile on the preface of the sutra. The sutra’s preface and inner pages were made of paper comprised of bamboo and bark. As a magnificent yet recondite treasure of Buddhism, the sutra was analyzed for a better understanding of the material. A conservation project of the sutra will be scheduled accordingly.


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