Application of Calcium Carbonate in Resin Transfer Molding Process

2014 ◽  
Vol 353 ◽  
pp. 39-43 ◽  
Author(s):  
Iran Rodrigues de Oliveira ◽  
Sandro Campos Amico ◽  
R. Barcella ◽  
Antônio Gilson Barbosa de Lima

Resin Transfer Molding (RTM) is one of the most widely known composite manufacturing techniques of the liquid molding family, being extensively studied and used to obtain advanced composite materials comprised of fibers embedded in a thermoset polymer matrix. Nowadays, RTM is used by many industrial sectors such as automotive, aerospace, civil and sporting equipment. Therefore, the objective of this study is to verify the effect of calcium carbonate mixed in resin in the RTM process. Several rectilinear infiltration experiments were conducted using glass fiber mat molded in a RTM system with cavity dimensions of 320 x 150 x 3.6 mm, room temperature, maximum injection pressure 0.202 bar and different content of CaCO3 (10 and 40%) with particle size of 75μm. The results show that the use of filled resin with CaCO3 influences the preform impregnation during the RTM molding, changing the filling time and flow from position, however it is possible to make the composite with a good quality and low cost.

2013 ◽  
Vol 334-335 ◽  
pp. 188-192 ◽  
Author(s):  
Iran Rodrigues de Oliveira ◽  
Sandro Campos Amico ◽  
F. Ferreira Luz ◽  
R. Barcella ◽  
V.M. França Bezerra ◽  
...  

Composite material can be defined as a combination of two or more materials on a macroscale to form a useful material, often showing properties that none of the individual independent components shows. Resin Transfer Molding (RTM) is one of the most widely known composite manufacturing technique of the liquid molding family, being extensively studied and used to obtain advanced composite materials comprised of fibers embedded in a thermoset polymer matrix. This technique consists in injecting a resin pre-catalysed thermosetting in a closed mold containing a dry fiber preform, where the resin is impregnated. The aim of this study is to investigate the effect caused by the use of CaCO3filled resin on the characteristics of the RTM process. Several experiments were conducted using glass fiber mat and polyester resin molded in a RTM system with cavity dimensions of 320 x 150 x 3.6 mm, at room temperature, and different CaCO3content (0, 10, 20, 30 and 40% in weight). The results show that the use of filled resin with CaCO3influences the resin viscosity and the porous media permeability, making it difficult to fill the porous media during the molding process, however it is possible to make composite with a good quality and low cost.


Polymers ◽  
2018 ◽  
Vol 11 (1) ◽  
pp. 20 ◽  
Author(s):  
Felice Rubino ◽  
Pierpaolo Carlone

In liquid composite molding processes, such as resin transfer molding (RTM) and vacuum assisted resin transfer molding (VARTM), the resin is drawn through fiber preforms in a closed mold by an induced pressure gradient. Unlike the RTM, where a rigid mold is employed, in VARTM, a flexible bag is commonly used as the upper-half mold. In this case, fabric deformation can take place during the impregnation process as the resin pressure inside the preform changes, resulting in continuous variations of reinforcement thickness, porosity, and permeability. The proper approach to simulate the resin flow, therefore, requires coupling deformation and pressure field making the process modeling more complex and computationally demanding. The present work proposes an efficient methodology to add the effects of the preform compaction on the resin flow when a deformable porous media is considered. The developed methodology was also applied in the case of Seeman’s Composite Resin Infusion Molding Process (SCRIMP). Numerical outcomes highlighted that preform compaction significantly affects the resin flow and the filling time. In particular, the more compliant the preform, the more time is required to complete the impregnation. On the other hand, in the case of SCRIMP, the results pointed out that the resin flow is mainly ruled by the high permeability network.


Author(s):  
Kiran M. D’Silva ◽  
Su-Seng Pang ◽  
Kurt C. Schulz

Abstract Low mold filling time and improper fiber wetting are the main problems faced by the manufacturers applying the Resin Transfer Molding (RTM) process. The objective of this work was to minimize these problems and to study the effect of weirs on the RTM process. A mold was designed such that the lower mold plate contains two weirs, one at the resin inlet port and the other at the outlet port. The purpose of adding the weirs is to provide a continuous inlet stream near the resin inlet port and to cause backpressure near the outlet port to induce complete mold filling. Laminated plates were prepared using glass fibers and epoxy resin (combination of EPON resin-862 and curing agent W). The test parameters investigated, such as void contents, dry spots and mold filling time, were compared with those of samples that were prepared without the use of weirs. It was found that the presence of weirs resulted in significant elimination of dry spots, minimization of void contents and a reduction in mold filling time. As a result, the cost required to manufacture composite parts can be reduced by the use of weirs. In addition to the experimental investigation, a computer simulation (using LCMFLOT software) of resin flow inside the mold cavity was conducted. Many simulations were run in order to optimize the height and shape of the weir. Rectangular weirs of height 2.54 mm showed minimum mold fill time. It was found that the results obtained from the experimental work and flow simulations are in good agreement. Based on this work, it is evident that complex parts can be produced in less cycle time if weirs are positioned at appropriate locations.


1995 ◽  
Vol 29 (16) ◽  
pp. 2180-2191 ◽  
Author(s):  
Wen-Bin Young ◽  
Cheng-Wey Chiu

Resin transfer molding (RTM) finishes the resin impregnation and composite fabrication at the same time. It simplifies the process for composites fabrication and has the advantages of automation, low cost, and versatile design of fiber reinforcement. Therefore, the RTM process is widely used in the architecture, automotive, and aerospace industries. However, in the RTM process, resin must flow through the fiber reinforcement in the planar direction, which, in some cases such as fabrications of large panels, may need a long time for the mold filling. If the part dimension is too large or the fiber permeability is too low, the mold filling process may not be able to complete before the resin gels. Therefore, some modification for the RTM process is necessary in order to reduce the mold filling time. In the compression transfer molding, the mold opens a small gap for the resin to fill in between fiber mats and the mold, and then compresses the fiber reinforcement to be impregnated by the resin in the thickness direction. In this way, since resin is forced into the fiber reinforcements in the thickness direction, the damage of the fibers will be minimized. In addition, the mold filling time will be reduced due to the different flow path of the resin inside the mold. This study explored the possibility of using the compression transfer molding process and also identified the key parameters regarding the process.


2015 ◽  
Vol 365 ◽  
pp. 88-93 ◽  
Author(s):  
I.R. Oliveira ◽  
Sandro Campos Amico ◽  
J.A. Souza ◽  
Antônio Gilson Barbosa de Lima

This work aims to investigate the infiltration of a CaCO3filled resin in fibrous porous media (resin transfer molding process) using the PAM-RTM software. A preform of glass fiber mat (fraction 30%), with dimensions 320 x 150 x 3.6 mm, has been used in rectilinear injection experiments conducted at room temperature and injection pressure 0.25, 0.50 and 0.75 bar. The polyester resin contain 0% and 40% CaCO3. The numerical results were evaluated by direct comparison with experimental data. The flat flow-front profile of the rectilinear flow was reached approximately half length of the mold. It was observed, that the both velocity infiltration and permeability have decreased with increasing the CaCO3content, thus, increasing the time to processing of the composite material.


2011 ◽  
Vol 686 ◽  
pp. 468-473
Author(s):  
Yan Liang Li ◽  
Xiao Su Yi ◽  
Bang Ming Tang

The objective of this paper was focused on predicting the thickness and the interior quality of carbon fiber composite panel during the vacuum assisted resin transfer molding (VARTM) process. The character of the VARTM process determined that it was low cost. A panel made of Epoxy resin, and carbon fibers, was used as the simplest article to experiment and except routine items, the thickness and the interior quality was focused. In the process, the flow front of the resin was record using a digital camera. Darcy’s law was the model of resin flow. The results showed that the flow front history would reach unanimous, thickness near the edges was difficult to control, and most of the porosity came from the injection line where more resin cumulated.


2013 ◽  
Vol 33 (3) ◽  
pp. 211-219 ◽  
Author(s):  
Chih-Yuan Chang

Abstract In the present study, a modified vacuum-assisted compression resin transfer molding (VACRTM) process has been developed to reduce the cycling period. The process uses an elastic bag placed between the upper mold and the preform to replace the mobile rigid mold in compression resin transfer molding. During resin injection, the bag is pulled upward by the vacuum applied in between the upper mold and the bag, and a loose fiber stack is then present. Resin is easily injected into the mold. Once enough volume of resin is injected, the compression pressure is applied on the bag, which compacts the preform and drives the resin through the remaining dry preform. Numerical results show that the bag compression phase is much longer than the resin injection one. A multistage compression strategy can be used to control the compression time. Due to inherent process defects, a higher volume of the injected liquid is essential and thus leads to a longer injection and compression phase in order to inject and squeeze the excess resin. The late compression is very slow in draining the residual resin. As compared with resin transfer molding, VACRTM can reduce the mold-filling time/injection pressure.


2013 ◽  
Vol 762 ◽  
pp. 612-620 ◽  
Author(s):  
Yun Hae Kim ◽  
Jin Woo Lee ◽  
Jun Mu Park

Reducing the cost of composite material production is significant for expanding its usage and application in many ways, such as in the fields of aerospace, aviation, ocean industry and so on. To do this, It is important to minimize the production process of the material and to decrease the amount of scraps or any unnecessary particles. The Vacuum Assisted Resin Transfer Molding (VARTM) process, which is known for having many advantages, has become recognized as one of the most low-cost manufacturing model. VARTM process can be divided into three main steps: performing, resin filling and hardening steps. The most important step among all these three steps is the Resin Filling stage, a process when resin is impregnated into the mat. Mostly, Resin Filling stage is greatly affected by the level of permeability, a characteristic of stiffener due to pneumatic resistant nature in the process. Other factors such as viscosity, technological vacuuming, or even stiffening process itself could also influence the production as well. During Resin Filling stage, Resin tends to spread out in the center first because of capillary phenomenon. In this research, the researchers examined the mechanical property and the pneumatic nature of Resin by dividing the pneumatic movement of the Resin into sections. Based on this result, the researchers found the correlations between the capillary phenomenon and Resin impregnation, and analyzed the movement mechanism in Resin filling stage.


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