Effect of Water on the Mechanical Response of Monocrystalline Silicon to Repeated Micro-Indentation

2003 ◽  
Vol 233-236 ◽  
pp. 609-614 ◽  
Author(s):  
Irena Zarudi ◽  
Liang Chi Zhang ◽  
Michael V. Swain
2004 ◽  
Vol 844 ◽  
Author(s):  
Douglas E. Burkes ◽  
Guglielmo Gottoli ◽  
John J. Moore ◽  
Reed A. Ayers

ABSTRACTThe Center for Commercial Applications of Combustion in Space (CCACS) at the Colorado School of Mines is currently using combustion synthesis to produce several advanced materials. These materials include ceramic, intermetallic, and metal-matrix composites in both porous and dense form. Currently, NiTi – TiC intermetallic ceramic composites are under investigation for use as a bone replacement material. The NiTi intermetallic has the potential to provide a surface that is capable of readily producing an oxide layer for corrosion resistance. The TiC ceramic has the potential to increase the hardness and wear resistance of the bulk material that can improve the performance lifetime of the implant. Processing parameters are critical to the production of the NiTi – TiC composite and will be discussed. These parameters can lead to the formation of substoichiometric TiC and nickel rich NiTi that changes the overall mechanical and material properties. In addition, the size of the TiC particles present within the bulk product varies with porosity. Both porous and dense samples have been mechanically analyzed employing micro-indentation techniques as well as compression tests in an attempt to characterize the mechanical response of these composites. The effects of the TiC particles, the formation of Ni3Ti intermetallic and the effects of porosity on the overall mechanical and material properties will be discussed.


2015 ◽  
Vol 52 (5) ◽  
pp. 587-598 ◽  
Author(s):  
Carlos Ovalle ◽  
Christophe Dano ◽  
Pierre-Yves Hicher ◽  
Mónica Cisternas

It has been widely shown that particle crushing increases the compressibility of granular materials. For a particular crushable material and given test conditions, an empirical relation can be established between the breakage ratio and the plastic work. Along these lines, constitutive models have been developed based on the effect of grading evolution during crushing. In parallel, due to corrosive attacks of the humid environment at the tip of microcracks within solid grains, the mechanical behavior of crushable granular materials depends also on the water content: the higher the material humidity, the higher the particle crushing. However, the experimental data on the relation between loading–wetting conditions and the breakage ratio are still quite scarce. In this paper, we present experimental results on crushable sand to study the effect of flooding under isotropic, oedometric, and triaxial stress paths. The main objective of this study is to obtain a consistent framework for the effect of water based on the breakage ratio. Our results have shown that, for a given initial density and stress path, the dry material after flooding reaches the equivalent behavior of the initially wetted material in terms of compression curve, particle crushing, and creep compressibility index, regardless of the point of flooding. Moreover, the relation between the breakage ratio and the final void ratio is unique and depends neither on the stress path, the water content, the point of flooding, nor the loading condition (time of creep or relaxation), but exclusively on the initial density and on intrinsic parameters. These findings could improve the prediction of the effect of water and time on the mechanical response of crushable granular materials through constitutive models based on grading evolution.


Author(s):  
I Zarudi ◽  
L C Zhang ◽  
M V Swain

This paper studies the difference in the mechanical response of monocrystalline silicon to cyclic microindentations in air and in water. It shows that in air the indentations with a spherical indenter generated consequent phase transformations. In the first indentation cycle, the decomposition featured amorphous phase at low maximum indentation load, Pmax, that was converged to a crystalline compound in repeated indentations. A high Pmax generated crystalline R8/BC8 phases only. After a few cycles, the transformed material behaved linearly elastically, and its properties became stable. However, when the same indentations were conducted in water, the property stabilization process of the transformed material was significantly slowed down, featuring non-linear elasticity. It seemed that at a high Pmax a chemical effect took place in the central part of the transformation zone.


Nanomaterials ◽  
2020 ◽  
Vol 10 (5) ◽  
pp. 959 ◽  
Author(s):  
Emre Topal ◽  
Harishankaran Rajendran ◽  
Izabela Zgłobicka ◽  
Jürgen Gluch ◽  
Zhongquan Liao ◽  
...  

Diatom frustules, with their hierarchical three-dimensional patterned silica structures at nano to micrometer dimensions, can be a paragon for the design of lightweight structural materials. However, the mechanical properties of frustules, especially the species with pennate symmetry, have not been studied systematically. A novel approach combining in situ micro-indentation and high-resolution X-ray computed tomography (XCT)-based finite element analysis (FEA) at the identical sample is developed and applied to Didymosphenia geminata frustule. Furthermore, scanning electron microscopy and transmission electron microscopy investigations are conducted to obtain detailed information regarding the resolvable structures and the composition. During the in situ micro-indentation studies of Didymosphenia geminata frustule, a mainly elastic deformation behavior with displacement discontinuities/non-linearities is observed. To extract material properties from obtained load-displacement curves in the elastic region, elastic finite element method (FEM) simulations are conducted. Young’s modulus is determined as 31.8 GPa. The method described in this paper allows understanding of the mechanical behavior of very complex structures.


Author(s):  
D. L. Rohr ◽  
S. S. Hecker

As part of a comprehensive study of microstructural and mechanical response of metals to uniaxial and biaxial deformations, the development of substructure in 1100 A1 has been studied over a range of plastic strain for two stress states.Specimens of 1100 aluminum annealed at 350 C were tested in uniaxial (UT) and balanced biaxial tension (BBT) at room temperature to different strain levels. The biaxial specimens were produced by the in-plane punch stretching technique. Areas of known strain levels were prepared for TEM by lapping followed by jet electropolishing. All specimens were examined in a JEOL 200B run at 150 and 200 kV within 24 to 36 hours after testing.The development of the substructure with deformation is shown in Fig. 1 for both stress states. Initial deformation produces dislocation tangles, which form cell walls by 10% uniaxial deformation, and start to recover to form subgrains by 25%. The results of several hundred measurements of cell/subgrain sizes by a linear intercept technique are presented in Table I.


Author(s):  
D. L. Callahan

Modern polishing, precision machining and microindentation techniques allow the processing and mechanical characterization of ceramics at nanometric scales and within entirely plastic deformation regimes. The mechanical response of most ceramics to such highly constrained contact is not predictable from macroscopic properties and the microstructural deformation patterns have proven difficult to characterize by the application of any individual technique. In this study, TEM techniques of contrast analysis and CBED are combined with stereographic analysis to construct a three-dimensional microstructure deformation map of the surface of a perfectly plastic microindentation on macroscopically brittle aluminum nitride.The bright field image in Figure 1 shows a lg Vickers microindentation contained within a single AlN grain far from any boundaries. High densities of dislocations are evident, particularly near facet edges but are not individually resolvable. The prominent bend contours also indicate the severity of plastic deformation. Figure 2 is a selected area diffraction pattern covering the entire indentation area.


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