Preparation and Characterization of Different Composition Mg-Cu Tapes

2010 ◽  
Vol 434-435 ◽  
pp. 518-521
Author(s):  
Jun Li ◽  
Guo Qiang Luo ◽  
Qiang Shen ◽  
Lian Meng Zhang

Tape casting was used for the preparation of Mg-Cu systems density graded materials. A series of tapes with uniform compositions ranging from 100wt% Cu to 100wt% Mg were fabricated with sufficient strength to be handled during the post-processing stage. The effect of the tape casting process parameters on the properties of the tape were studied, such as the composition of the Mg-Cu and the solid loading. The rheology of the slurry of different Mg-Cu composition for tape casting was characterized by viscosity. The tapes characterized by microstructure, thickness and bulk density were outlined. The results demonstrated that the different Mg-Cu composition slurry with well-dispersed, high stability, certain solid loading from 45 ~70 wt% were obtained. The viscosity of the slurry and the density of the green tapes were increased with the increasing of the content of Mg. The thickness of tapes of compositions ranging from 100wt% Cu to 100wt% Mg with certain strength could be achieved 68-110μm and the density of the tapes was 0.74-2.42g/cm3. For 100wt% Cu tapes, when the solid loading was 68wt%, the high density tape was produced. The tapes with different thickness, density and different Mg-Cu compositions were obtained.

2010 ◽  
Vol 434-435 ◽  
pp. 275-277
Author(s):  
Wei Liang Liu ◽  
Shuo Qi Liu ◽  
Du Song Mao

Sr0.7Ca0.3TiO3 (SCT) substrates were prepared through aqueous tape casting. Properties of SCT slurries with and without ammonium polyacrylate (NH4PAA) dispersant were characterized by zeta potential. The zeta potential measurement result shows that the isoelectric point (IEP) of the powder changed obviously with the addition of the dispersant. The optimum pH value of the slurry is in the range of 9-10. The rheological test result indicates that the proper content of the dispersant is between 0.6 and 0.8 wt%. The effect of different plasticizer/binder ratio (R) on the properties of the green tapes was investigated. For 56 wt% solid loading, the tensile strength of the green tape reached 2.02 MPa and the breaking elongation rate was about 8%. SEM micrographs show that the microstructure of the green tapes is homogeneous and the microstructure of the sintered tapes is dense.


Electronics ◽  
2021 ◽  
Vol 10 (2) ◽  
pp. 140
Author(s):  
Lichen Liu ◽  
Ziping Cao ◽  
Min Chen ◽  
Jun Jiang

This paper reports the fabrication and characterization of (Bi0.48Sb1.52)Te3 thick films using a tape casting process on glass substrates. A slurry of thermoelectric (Bi0.48Sb1.52)Te3 was developed and cured thick films were annealed in a vacuum chamber at 500–600 °C. The microstructure of these films was analyzed, and the Seebeck coefficient and electric conductivity were tested. It was found that the subsequent annealing process must be carefully designed to achieve good thermoelectric properties of these samples. Conductive films were obtained after annealing and led to acceptable thermoelectric performance. While the properties of these initial materials are not at the level of bulk materials, this work demonstrates that the low-cost tape casting technology is promising for fabricating thermoelectric modules for energy conversion.


2002 ◽  
Vol 28 (6) ◽  
pp. 675-683 ◽  
Author(s):  
Bernd Bitterlich ◽  
Christiane Lutz ◽  
Andreas Roosen

Author(s):  
Waqas Ahmed Sarwar ◽  
Jin-Ho Kang ◽  
Hyung-In Yoon

Additive manufacturing (AM) processes, including stereolithography (SL), can fabricate complex ceramic parts layer by layer using computer-aided design (CAD) models. A ceramic slurry with high solid loading is usually used in SL to fabricate the desired shape, which is further sintered to produce the final part. The traditional SL system utilizes a tank filled with printable material, known as a vat, which for ceramic slurry contributes several limitations and operational difficulties, and further renders it non-recyclable mainly due to its high viscosity and the fragility of the green state. In this study, we utilized a continuous film supply (CFS) printer integrated with a tape casting system using in-house-designed ceramic slurry to print standard prototype specimens. Various printing parameters, including viscosity, layer thickness control, and slurry recycling efficiency, were studied. In addition, post-processing optimizations of the prototype, characterizations, and the microhardness of sintered samples were studied to determine their properties and compare them with traditional methods. The effectiveness of slurry reusability was demonstrated by printing with original and recycled slurry to produce consistent densification of final parts. Post-processing was optimized to achieve a relative sinter density of 99.02% and microhardness of 12.59 GPa. This method provides new opportunities to realize dense complex ceramic features with final properties comparable to those produced by subtractive machining and traditional SL. Furthermore, slurry recycling helps to reduce the overall cost and material consumption.


2007 ◽  
Vol 280-283 ◽  
pp. 935-940 ◽  
Author(s):  
Yao Hui A. Lee ◽  
Wen Cheng J. Wei

Synthesis of La2O3-SiO2-B2O3 (LSB) based glass-ceramics using glass melting method has een investigated in this study. XRD result showed that some LSB glass systems in this study were ntirely amorphous phases. In addition, TMA results revealed that the LSB/mullite (LSBM) glassceramics ith a mass ratio of 60/40 could be densified at 850oC, which matches the requirements for theLTCC application. Moreover, dispersive behavior of the LSB glass powder with six kinds of commercial ispersants in MEK and toluene solvent had been studied. Furthermore, tape-casting process used for ow-temperature-cofired-ceramic (LTCC) chips was conducted in order to do crystal phase identification, microstructure analysis, and dielectric property measurement.


2018 ◽  
Vol 536 (1) ◽  
pp. 170-180
Author(s):  
Hui Wang ◽  
Zhongwei He ◽  
Xiao Wang ◽  
Biao He ◽  
Tao Ma ◽  
...  

2007 ◽  
Vol 280-283 ◽  
pp. 753-756
Author(s):  
Xue Min Cui ◽  
Yong Huang ◽  
Ji Zhou ◽  
Chang An Wang ◽  
Shi Xi Ouyang

As a good binder for aqueous Al2O3 suspensions tape-casting process, a commercial styrene-acrylic latex binder had been investigated. This paper studied on the rheological behaviors of the suspensions and drying process of aqueous slurries with latex binder system, and the research results indicated the rheological behaviors was affected by pH value, solid loading and dispersant (PAA-NH4) additives; and the drying speed of slurries was most decided by drying temperature and slurry coating thickness.


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