Relationship between the Different Amount of LMZBS Glass and Dielectric Properties of Li2(Mg0.96Ni0.04)SiO4 Ceramics

2021 ◽  
Vol 1027 ◽  
pp. 10-14
Author(s):  
Rui Peng ◽  
Yuan Xun Li ◽  
Hua Su ◽  
Yong Cheng Lu ◽  
Xue Ying Wang ◽  
...  
Keyword(s):  
Dielectric Properties ◽  
Microwave Dielectric Properties ◽  
Composite Ceramic ◽  
Solid State Reaction Method ◽  
Sintering Behavior ◽  
Network Analyzer ◽  
Composite Ceramics ◽  
Dielectric Parameters ◽  
Densification Temperature ◽  
Microwave Dielectric

The effect of different amount of LMZBS glass on the sintering behavior, microstructure and microwave dielectric properties of the Li2(Mg0.96Ni0.04)SiO4 ceramics was investigated. The synthesis of materials was based on the solid-state reaction method. The micromorphology of the composite ceramics was confirmed using scanning electron microscopy. The microwave dielectric parameters were measured by the network analyzer. The mechanism of heat transfer coming from LMZBS glass lower the densification temperature of matrix ceramic from 1150°C down to 900°C. Excellent microwave dielectric properties were obtained with 1.2 wt% LMZBS glass sintered at 900°C for 4h (εr=5.77 and Q×f=29,558 GHz at 16 GHz, τf=-14.5 ppm/°C). There was a compatibility between the composite ceramic and Ag. Therefore, the aimed ceramic has great potential value of application in the field of low temperature co-fired ceramics of millimeter-wave devices.

scholarly journals SINTERING BEHAVIOR AND MICROWAVE DIELECTRIC PROPERTIES OF NOVEL LOW TEMPERATURE FIRING Bi3FeMo2O12 CERAMIC

2011 ◽  
Vol 01 (04) ◽  
pp. 379-382 ◽  
Author(s):  
DI ZHOU ◽  
LI-XIA PANG ◽  
JING GUO ◽  
YING WU ◽  
GAO-QUN ZHANG ◽  
...  
Keyword(s):  
Dielectric Properties ◽  
Low Temperature ◽  
Sintering Temperature ◽  
Microwave Dielectric Properties ◽  
Solid State Reaction Method ◽  
Sintering Behavior ◽  
Reaction Method ◽  
Temperature Firing ◽  
Microwave Dielectric ◽  
Dielectric Performance

In the present work, a novel low temperature firing Bi 3 FeMo 2 O 12 ceramic was synthesized via the solid-state reaction method. The monoclinic Bi 3 FeMo 2 O 12 phase can be formed at a low temperature 670°C. A relative density above 96% can be obtained when sintering temperature is above 800°C. The Bi 3 FeMo 2 O 12 ceramic sintered at 845°C for 2 h shows high microwave dielectric performance with a permittivity ~27.2, a Qf value of 14,500 GHz and a temperature coefficient of -80 ppm/°C. It might be a candidate for low temperature co-fired ceramics technology.

Effect of V2O5 and ZnO Additives on the Sintering Temperature and Microwave Dielectric Properties of Ca[(Li1/3Nb2/3) 0.8Ti 0.2]O3-δ Ceramics

2011 ◽  
Vol 239-242 ◽  
pp. 77-80 ◽  
Author(s):  
Ji Hong Liao ◽  
Ying Dai ◽  
Ren Zhou Yang ◽  
Wen Chen
Keyword(s):  
Dielectric Properties ◽  
Sintering Temperature ◽  
Microwave Dielectric Properties ◽  
Solid State Reaction Method ◽  
Sintering Behavior ◽  
Conventional Solid State Reaction ◽  
Microwave Dielectric ◽  
Diffraction Peaks ◽  
Dielectric Ceramics ◽  
The Relationship

Low-temperature sintered Ca[(Li1/3Nb2/3)0.8Ti0.2]O3-δ (CLNT) microwave dielectric ceramics with V2O5 and ZnO additives were prepared by the conventional solid state reaction method. The sintering behavior and microwave dielectric properties of CLNT ceramics were investigated. The main diffraction peaks of all the specimens sintered at the temperature under 1150◦C split due to the coexistence of the non-stoichiometric phase and stoichiometric phase, which all possess CaTiO3-type perovskite structures. ZnO and V2O5 combined additives lowered the sintering temperature of CLNT ceramics from 1150◦C to 1090◦C. and the Qf values were improved from 18,210 GHz to 20,740 GHz. The CLNT ceramics with 4 wt% ZnO addition sintered at 1090◦C showed good microwave dielectric properties with εr ~39.7, Qf ~20,740 GHz, τf ~8.6 ppm/◦C. The relationship between dielectric properties and the sintering behavior was also discussed.

scholarly journals Preparation and microwave dielectric properties of CaTiO3 added Mg0.95Ni0.05Ti0.98Zr0.02O3 composite ceramics for high frequency applications

2019 ◽  
Vol 37 (4) ◽  
pp. 639-644 ◽  
Author(s):  
Abdul Manan ◽  
Asif Nawaz ◽  
Arbab Safeer Ahmad ◽  
Atta Ullah ◽  
Arshad Hussain Wazir ◽  
...  
Keyword(s):  
Dielectric Properties ◽  
High Frequency ◽  
Microwave Dielectric Properties ◽  
Secondary Phase ◽  
Solid State Reaction Method ◽  
Composite Ceramics ◽  
Low Loss ◽  
Major Phase ◽  
Reaction Method ◽  
Microwave Dielectric

AbstractMg0.95Ni0.05Ti0.98Zr0.02O3 and CaTiO3 were prepared separately using solid state reaction method. The effect of CaTiO3 addition on the microwave dielectric properties of Mg0.95Ni0.05Ti0.98Zr0.02O3 was investigated to get low loss and temperature stable ceramics in (1 – x)Mg0.95Ni0.05Ti0.98Zr0.02O3-xCaTiO3 series. Mg0.95Ni0.05Ti0.98Zr0.02O3 formed as the major phase along with Mg0.95Ni0.05Ti2O5 phase that formed as minor secondary phase for the composition with x = 0. Microwave dielectric properties ∈r ~ 17.1, Qufo of 195,855 GHz and τf of –46.3 ppm/°C were obtained for the composition with x = 0. The positive τf value of CaTiO3, tuned the τf value of Mg0.95Ni0.05Ti0.98Zr0.02O3 through zero and ∈r ~ 28.4, Qufo ~ 108,775 GHz and τf ~ 3.1 ppm/°C were attained for x = 0.15 in this study. This composition is the best choice for high frequency applications.

Effects of zinc substitution on the dielectric properties of Ca5Nb4TiO17 microwave ceramics

2013 ◽  
Vol 03 (04) ◽  
pp. 1320003 ◽  
Author(s):  
Chunchun Li ◽  
Xiaoyong Wei ◽  
Haixue Yan ◽  
Michael J. Reece
Keyword(s):  
Dielectric Properties ◽  
Sintering Temperature ◽  
Microwave Dielectric Properties ◽  
Solid State Reaction Method ◽  
Sintering Behavior ◽  
Potential Candidate ◽  
Strongly Correlated ◽  
Microwave Ceramics ◽  
Microwave Dielectric ◽  
Method Effects

Ca 5-x Zn x Nb 4 TiO 17 ceramics with 0 ≤ x ≤ 0.4 were prepared through a solid-state reaction method. Effects of zinc substitution on sintering behavior and microwave dielectric properties of Ca 5 Nb 4 TiO 17 ceramics were investigated. The sintering temperature was significantly lowered from 1480°C for pure Ca 5 Nb 4 TiO 17 to 1260°C for x = 0.4. The microwave dielectric properties are strongly correlated with the composition. It is worth noting that the temperature coefficient of resonant frequency (τf) displays a tendency toward positive value, ranging from −126.4 ppm/°C to −8.6 ppm/°C. A temperature stable microwave ceramic with dielectric constant of 52 and Q × f value of 9937 GHz is achieved at x = 0.4 and is a potential candidate for application as cores in dielectrically loaded antennas.

Effect of CuO-Bi2O3 Co-Doping on Microwave Dielectric Properties of Ba4Sm9.33Ti18O54 Ceramics

2011 ◽  
Vol 197-198 ◽  
pp. 548-551
Author(s):  
Zhi Lan Tang ◽  
Chun Ying Shen ◽  
Zhao Xi Li ◽  
Jian Yang ◽  
Tai Qiu
Keyword(s):  
Dielectric Properties ◽  
Microwave Dielectric Properties ◽  
Solid State Reaction Method ◽  
Liquid Phase Sintering ◽  
Sintering Behavior ◽  
Conventional Solid State Reaction ◽  
Co Doping ◽  
Microwave Dielectric ◽  
Bst Ceramics ◽  
Quality Factor Q

Ba4Sm9.33Ti18O54(BST) ceramics were prepared by conventional solid-state reaction method. The effect of CuO-Bi2O3co-doping on the sintering behavior and microwave dielectric properties of BST ceramics has been investigated. The results indicated that when the total addition of CuO-Bi2O3doping agent was 1.0wt%, the sintering temperature of BST ceramics was reduced to 1240°C as a result of liquid-phase sintering effect derived from CuBi2O4. When the total addition of CuO-Bi2O3was fixed at 1.0wt%, the microwave dielelctric properties of BST were improved by adjusting the mass percentage of Bi2O3. With the increase of Bi2O3amount from 20wt% to 80wt%, the dielectric constant (εr) decreased, the quality factor (Q•f) increased and the temperature coefficient of resonant frequency (τf) shifted from negative value to positive value. The excellent microwave dielectric properties of εr=82.51, Q•f=7878GHz and τf=+6.02ppm/ were obtained for the sample with Bi2O3amount of 80wt% when sintered at 1240°C for 3h.

Effect of H3BO3 Coating on the Microwave Dielectric Properties of BZN Ceramics

2014 ◽  
Vol 906 ◽  
pp. 8-11
Author(s):  
Liu Shuan Yang ◽  
Biao Jin ◽  
Xiao Wang
Keyword(s):  
Dielectric Properties ◽  
Ceramic Composite ◽  
Microwave Dielectric Properties ◽  
Sintering Behavior ◽  
Network Analyzer ◽  
X Ray Diffraction ◽  
Ceramic Specimen ◽  
Coating Technology ◽  
X Ray ◽  
Microwave Dielectric

(Bi1.5Zn0.5)(Zn0.5Nb1.5)O7(BZN) ceramic samples were prepared by solid state reaction. B2O3 was introduced by liquid coating technology with H3BO3 solution in the BZN ceramic specimen to reduce its sintering temperature. The sintering behavior, phase composition and dielectric properties of ceramics were investigated by X-ray diffraction, scanning electron microscopy and vector network analyzer. The (Bi1.5Zn0.5)(Zn0.5Nb1.5)O7 ceramic composite could be sintered well at 900°C for 3h when 0.9M/l H3BO3 was added and showed good dielectric properties of εr=150,Q×f=228,τf=-362ppm/°C.

Effect of Li2CO3-V2O5 on the Sintering and Microwave Dielectric Properties of 0.6Mg4Nb2O9-0.4SrTiO3 Composite Ceramics

2010 ◽  
Vol 663-665 ◽  
pp. 608-611
Author(s):  
Cui Jin Pei ◽  
Guo Guang Yao ◽  
Xiu Lao Tian ◽  
Hong Ma
Keyword(s):  
Dielectric Properties ◽  
Sintering Temperature ◽  
Microwave Dielectric Properties ◽  
Solid State Reaction Method ◽  
Composite Ceramics ◽  
X Ray Diffraction ◽  
Reaction Method ◽  
X Ray ◽  
Microwave Dielectric ◽  
Co Doped

The effects of Li2CO3-V2O5 (LV) co-doped on the sinterability, phase compositions and microwave dielectric properties of 0.6Mg4Nb2O9-0.4SrTiO3 composite ceramics have been investigated. All specimens were prepared by solid-state reaction method and sintered at 1050-1200oC for 5h. With an amount LV addition, the densification sintering temperature is significantly lowed from 1300oC to 1175oC. The non-stoichiometric compounds Sr(NbTi)O3+δ and Mg4(Nb1-xTix)2O9-δ were confirmed by X-ray diffraction and energy dispersive X-ray analysis. For the specimen with 1.5 wt% LV addition sintered at 1175oC for 5 h exhibited dielectric properties: εr=20.1, Q•f=10 240 GHz, τf =0.15 ppm/oC.

Phase composition, crystal structure, infrared reflectivity and microwave dielectric properties of temperature stable composite ceramics (scheelite and zircon-type) in BiVO4–YVO4 system

2015 ◽  
Vol 3 (11) ◽  
pp. 2582-2588 ◽  
Author(s):  
Di Zhou ◽  
Wen-Bo Li ◽  
Hai-Hong Xi ◽  
Li-Xia Pang ◽  
Guang-Sheng Pang
Keyword(s):  
Crystal Structure ◽  
Phase Composition ◽  
Dielectric Properties ◽  
Microwave Dielectric Properties ◽  
Solid State Reaction Method ◽  
Composite Ceramics ◽  
Reaction Method ◽  
Microwave Dielectric ◽  
System P ◽  
Zircon Type

(1 − x)BiVO4–xYVO4 (x ≤ 0.65) ceramics were prepared using the solid state reaction method. Bi–O oscillations were proved to dominate the microwave dielectric polarizations.

scholarly journals Sintering Behavior and Microwave Dielectric Properties of MgO-2B 2 O 3 - Xwt %H 3 BO 3 - Ywt %BCB Ceramics

2021 ◽  
Author(s):  
Haiquan WANG ◽  
Shixuan LI ◽  
Kangguo WANG ◽  
Huanfu ZHOU ◽  
Xiuli Chen
Keyword(s):  
Dielectric Properties ◽  
Bulk Density ◽  
Single Phase ◽  
Sintering Temperature ◽  
Microstructural Analysis ◽  
Microwave Dielectric Properties ◽  
Solid State Reaction Method ◽  
Sintering Behavior ◽  
X Ray Diffraction ◽  
Microwave Dielectric

Abstract The bulk density, sintering behavior and microwave dielectric properties of MgO-2B2O3 series ceramics synthesized by solid-state reaction method were systematically studied in this paper. X-ray diffraction and microstructural analysis revealed that the as-prepared MgO-2B2O3 ceramics possessed a single-phase structure with rod-like morphology. Through the investigation of the effects of different dosages of H3BO3 and BCB on bulk density, sintering behavior and microwave dielectric properties of MgO-2B2O3 ceramics, the optimum sintering temperature was obtained at an addition of 30wt%H3BO3 and 8wt%BCB and the sintering temperature was reduced to 825 oC. The addition of 40wt %H3BO3 and 4 wt%BCB increased the quality factor Q×f, permittivity εr and temperature coefficient of resonance frequency τf of MgO-2B2O3 to 44,306 GHz, 5.1 and -32 ppm/oC, respectively, meeting the criteria of low-temperature co-fired ceramics.

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