Grain Growth Kinetics of (NdPr)2Fe14B Magnets

2014 ◽  
Vol 802 ◽  
pp. 540-545 ◽  
Author(s):  
Kaio Sérgio Torres de Souza ◽  
Célio de Jesus Marcelo ◽  
Daniel Rodrigues ◽  
José Adilson de Castro ◽  
Marcos Flavio de Campos

Two different effects need to be considered in the sintering: (i) The densification should be maximum, to optimize the energy product BHmax and the remanence, however, (ii) the .grain size should be small, in order to maximize the coercivity. Grain growth takes place during the sintering step of the magnets, usually performed at the range 1000-1100°C. In this study, the grain growth kinetics is investigated. Samples of NdPrFeB magnets (proportion 3 Nd : 1 Pr) were heat treated at the temperature of 1050 °C, for times between 1 to 12 hours. The knowledge of the grain growth and coarsening kinetics allows extrapolation to other temperatures, and this information is helpful to maximize coercivity and remanence at the same time.

2006 ◽  
Vol 20 (25n27) ◽  
pp. 3830-3835 ◽  
Author(s):  
PENG CAO ◽  
DELIANG ZHANG

The grain growth kinetics of nanocrystalline copper thin film samples was investigated. The grain size of nanocrystalline copper samples was determined from the broadening of X-ray spectra. It was found that the grain size increased linearly with isothermal annealing time within the first 10 minutes, beyond which power-law growth kinetics is applied. The activation energy for grain growth was determined by constructing an Arrhenius plot, which shows an activation energy of about 21 – 30 kJ/mol. The low activation energy is attributed to the second phase particle drag and the porosity drag, which act as the pinning force for grain growth in nanocrystalline copper.


2015 ◽  
Vol 17 (11) ◽  
pp. 1598-1607 ◽  
Author(s):  
Leyla Hashemi-Sadraei ◽  
S. Ebrahim Mousavi ◽  
Enrique J. Lavernia ◽  
Julie M. Schoenung

2006 ◽  
Vol 515 (1) ◽  
pp. 353-356 ◽  
Author(s):  
O. Yevtushenko ◽  
H. Natter ◽  
R. Hempelmann

2007 ◽  
Vol 550 ◽  
pp. 339-344 ◽  
Author(s):  
Shigeo Saimoto ◽  
Hai Ou Jin

A nominally pure Al slab was thermo-mechanically treated to result in a near random texture of 90 m grain size. Subsequent cold rolling with intermediate anneals at 230, 275, and 300°C reduced the Fe solute to near equilibrium compositions below 0.5 ppm atomic. The final cold rolled sheet continuously recrystallized; grain growth of this structure is reported. A grain-growth kinetics mapping was generated, correlating the parameters of Fe-in-Al solubility limit, Fe diffusivities in the grain boundaries and the Al lattice and the activation energies for migration rates.


2000 ◽  
Vol 104 (11) ◽  
pp. 2467-2476 ◽  
Author(s):  
H. Natter ◽  
M. Schmelzer ◽  
M.-S Löffler ◽  
C. E. Krill ◽  
A. Fitch ◽  
...  

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