Superplastic Behavior of ATI 718Plus Superalloy

2016 ◽  
Vol 838-839 ◽  
pp. 557-562 ◽  
Author(s):  
Shamil Kh. Mukhtarov ◽  
Farid Z. Utyashev
Keyword(s):  
Strain Rate ◽  
Temperature Interval ◽  
Superplastic Forming ◽  
Low Flow ◽  
Superplastic Behavior ◽  
Fine Grained ◽  
Working Temperature ◽  
Ultrafine Grained ◽  
Thin Walled ◽  
Superplastic Properties

Complex shaped, ultra thin-walled parts can be manufactured using superplastic forming. Hot working temperature for the production of fine-grained billets (d=5-15 μm) out of ATI Allvac 718Plus® superalloy is in the range of 982-1038°C. An ultrafine-grained structure (d=0.3 μm) was produced by multi-axial forging with a gradual decrease of the forging temperature from 950 to 700°C. Superplastic properties of the alloy were carried out in the temperature interval of 700-950°C. It has been revealed that the fine-grained alloy provided superplastic elongations about 300% at 950°C and strain rate of 10-4 s-1. The highest elongation of ultrafine-grained alloy was about 1450% and very low flow stresses were reached at 900°C and strain rate of 3×10-4 s-1. The ultrafine-grained alloy showed superplastic properties also at 700°C (0.62Tm). The microstructure and superplastic properties of the alloys 718 and 718Plus are compared.

Effect of Rolling on Superplastic Behavior of an Al-Mg-Sc Alloy with Ultrafine-Grained Structure

2016 ◽  
Vol 838-839 ◽  
pp. 416-421 ◽  
Author(s):  
Andrii Dubyna ◽  
Sergey Malopheyev ◽  
Rustam Kaibyshev
Keyword(s):  
Cold Rolling ◽  
Strain Rate ◽  
Rolling Direction ◽  
Initial Strain Rate ◽  
Warm Rolling ◽  
Initial Strain ◽  
Superplastic Behavior ◽  
Ultrafine Grained ◽  
Elongation To Failure ◽  
Superplastic Properties

The superplastic behavior of a commercial aluminum alloy denoted as 1570 Al with a chemical composition of Al-6%Mg-0.5%Mn-0.2%Sc-0.07%Zr (in wt. %) and ultrafine-grained (UFG) structure produced by equal channel angular pressing at 300°C to a true strain ~12 was studied after final cold or warm rolling. The tensile specimens were machined along rolling direction and pulled up to failure in the temperature range of 250 to 500°C at strain rates ranging from 10-4 s-1 to 10-1 s-1. The specimens produced by warm or cold rolling exhibit different superplastic behavior. The material subjected to warm rolling exhibits excellent superplastic properties; the highest elongation-to-failure of ~1970% was recorded at a temperature of ~450°C and an initial strain rate of 1.4×10-1 s-1. On the other hand, the material subjected to cold rolling demonstrates moderate superplastic properties; the highest elongation-to-failure of ~755% appears at a temperature of ~300°C and an initial strain rate of 1.4×10-2 s-1.

Routes to Develop Fine-Grained Magnesium Alloys and Composites for High-Strain Rate Superplasticity

1999 ◽  
Vol 601 ◽  
Author(s):  
Toshiji Mukai ◽  
Hiroyuki Watanabe ◽  
T. G. Nieh ◽  
Kenji Higashi
Keyword(s):  
High Strain Rate ◽  
Strain Rate ◽  
Magnesium Alloys ◽  
High Strain ◽  
Thermomechanical Processing ◽  
Superplastic Forming ◽  
Fine Grained ◽  
Superplastic Properties ◽  
Rapidly Solidified

AbstractSuperplastic properties of magnesium alloys and their composites were reviewed with a special emphasis on the achievement of high strain rate superplastic forming. The role of grain size on superplastic deformation mechanisms was particularly addressed. Commercial Mg-Al-Zn alloys and a ZK60-based composite are used as model materials to illustrate the underlining principles leading to the observation of high strain rate superplasticity. In this paper, experimental results from several processing routes, including thermomechanical processing, severe plastic deformation, and extrusion of machined chips and rapidly solidified powders, are presented. High strain rate superplasticity (HSRS) is demonstrated in ZK60-based composites.

Superplastic Behavior of a Cu-Cr-Zr Alloy Subjected to ECAP

2016 ◽  
Vol 838-839 ◽  
pp. 404-409
Author(s):  
Roman Mishnev ◽  
Iaroslava Shakhova ◽  
Andrey Belyakov ◽  
Rustam Kaibyshev
Keyword(s):  
Grain Size ◽  
Dislocation Density ◽  
Strain Rate ◽  
Temperature Interval ◽  
Rate Sensitivity ◽  
Tensile Tests ◽  
Superplastic Behavior ◽  
Average Grain Size ◽  
Gauge Section ◽  
Zr Alloy

A Cu-0.87%Cr-0.06%Zr alloy was subjected to equal channel angular pressing (ECAP) at a temperature of 400 °C up to a total strain of ~ 12. This processing produced ultra-fine grained (UFG) structure with an average grain size of 0.6 μm and an average dislocation density of ~4×1014 m-2. Tensile tests were carried out in the temperature interval 450 – 650 °C at strain rates ranging from 2.8´10-4 to 0.55 s-1. The alloy exhibits superplastic behavior in the temperature interval 550 – 600 °C at strain rate over 5.5´10-3 s-1. The highest elongation-to-failure of ~300% was obtained at a temperature of 575 °C and a strain rate of 2.8´10-3 s-1 with the corresponding strain rate sensitivity of 0.32. It was shown the superplastic flow at the optimum conditions leads to limited grain growth in the gauge section. The grain size increases from 0.6 μm to 0.87 μm after testing, while dislocation density decreases insignificantly to ~1014 m-2.

scholarly journals SUPERPLASTIC DEFORMATION OF TWO PHASE MgLiAl ALLOYAFTER TCAP PRESSING.

2017 ◽  
Vol 23 (3) ◽  
pp. 215 ◽  
Author(s):  
Jan Marek Dutkiewicz ◽  
Stanislav Rusz ◽  
Dariusz Kuc ◽  
Ondrej Hilser ◽  
Paweł Pałka ◽  
...  
Keyword(s):  
Strain Rate ◽  
Rate Sensitivity ◽  
Superplastic Forming ◽  
Sensitivity Coefficient ◽  
Strain Rate Range ◽  
Two Phase ◽  
Angular Pressing ◽  
Slip Planes ◽  
Superplastic Properties ◽  
Grain Misorientation

<p>Magnesium based alloy containing 9 wt. % Li, 1,5 wt. % Al, composed of a + b (hcp + bcc) phases was cast under argon atmosphere and extruded at 350<sup>o</sup>C. Up to 3 passes of Twist Channel Angular Pressing TCAP deformation was applied at 160<sup>o</sup>C. TCAP tool consisted of helical part in horizontal area of the channel with angle of lead γ = 30° to simulate back pressure. The initial grain size of hexagonal a phase estimated at 30 mm decreased in following passes down to 6 mm and that of bcc b phase decreased after TCAP from initial 12 mm down to 5 mm. TEM studies after TCAP passes showed higher dislocation density in the b region than in the a phase. Crystallographic relationship (001) a || (110) b indicated parallel positioning of slip planes of both phases. Electron diffraction confirmed increase of grain misorientation with number of TCAP passes. Stress/strain curves measured at temperature 200<sup>o</sup>C showed superplastic forming after 1<sup>st</sup> and 3<sup>rd</sup> TCAP pass. Values of strain rate sensitivity coefficient <em>m</em> were calculated at 0.31 after 1 TCAP pass and increased after 3<sup>rd</sup> TCAP pass up to 0.47 for the strain rate range 10<sup>-5</sup> – 5 10<sup>-4</sup>. Increase of number of TCAP passes had positive effect on superplastic properties due to finer grains and increase of their misorientation;</p>

Superplastic Behavior and Microstructure of Titanium (Ti-6Al-4V) Friction Stir Welds Made under a Variety of Processing Conditions

2010 ◽  
Vol 433 ◽  
pp. 169-176 ◽  
Author(s):  
Paul Edwards ◽  
Mamidala Ramulu ◽  
Daniel G. Sanders
Keyword(s):  
Friction Stir Welding ◽  
Base Material ◽  
Superplastic Forming ◽  
Spindle Speed ◽  
Processing Conditions ◽  
Superplastic Behavior ◽  
Friction Stir ◽  
Fine Grained ◽  
Weld Parameters

Friction Stir Welding of Ti-6Al-4V was performed on 5 mm thickness plate in order to assess the affect of welding conditions on the resulting microstructure and superplastic forming behavior of the joints. A variety of welding conditions were tested and all welds were subsequently Superplastically formed. It was found that the weld parameters do influence the microstructure and degree of superplastic performance of the joints. Spindle speed was found to have the most dominant affect on the resulting microstructure and superplastic forming behavior. Low spindle speed welds lead to fine grained microstructures and highly superplastic welds, relative to the base material, while high spindle speed welds larger grained microstructures and less superplastic welds.

High-Temperature Deformation of Magnesium ElektronTM 43

2012 ◽  
Vol 735 ◽  
pp. 93-100
Author(s):  
Alexander J. Carpenter ◽  
Anthony J. Barnes ◽  
Eric M. Taleff
Keyword(s):  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
Rate Sensitivity ◽  
Superplastic Forming ◽  
Solute Drag ◽  
Grain Boundary Sliding ◽  
High Temperature Deformation ◽  
Temperature Deformation ◽  
Fine Grained ◽  
Boundary Sliding

Complex sheet metal components can be formed from lightweight aluminum and magnesium sheet alloys using superplastic forming technologies. Superplastic forming typically takes advantage of the high strain-rate sensitivity characteristic of grain-boundary-sliding (GBS) creep to obtain significant ductility at high temperatures. However, GBS creep requires fine-grained materials, which can be expensive and difficult to manufacture. An alternative is provided by materials that exhibit solute-drag (SD) creep, a mechanism that also produces elevated values of strain-rate sensitivity. SD creep typically operates at lower temperatures and faster strain rates than does GBS creep. Unlike GBS creep, solute-drag creep does not require a fine, stable grain size. Previous work by Boissière et al. suggested that the Mg-Y-Nd alloy, essentially WE43, deforms by SD creep at temperatures near 400°C. The present investigation examines both tensile and biaxial deformation behavior of ElektronTM 43 sheet, which has a composition similar to WE43, at temperatures ranging from 400 to 500°C. Data are presented that provide additional evidence for SD creep in Elektron 43 and demonstrate the remarkable degree of biaxial strain possible under this regime (>1000%). These results indicate an excellent potential for producing complex 3-D parts, via superplastic forming, using this particular heat-treatable Mg alloy.

Superplastic Behavior of Friction-Stir Welded Joints of an Al-Mg-Sc Alloy with Ultrafine-Grained Microstructure

2016 ◽  
Vol 838-839 ◽  
pp. 338-343 ◽  
Author(s):  
Sergey Malopheyev ◽  
Sergey Mironov ◽  
Igor Vysotskiy ◽  
Rustam Kaibyshev
Keyword(s):  
Strain Rate ◽  
True Strain ◽  
Rate Sensitivity ◽  
Initial Strain Rate ◽  
Sensitivity Coefficient ◽  
Friction Stir ◽  
Angular Pressing ◽  
Ultrafine Grained ◽  
Elongation To Failure ◽  
Superplastic Properties

The commercial Al-5.4Mg-0.2Sc-0.1Zr alloy was subjected to equal-channel angular pressing at 300°C to a true strain ~12 followed by cold rolling to a total thickness reduction of 80%. The ultrafine-grained sheets were joined by friction stir welding (FSW). To evaluate superplastic properties of the weldments, the tensile samples including all of the characteristic FSW microstructural zones were machined perpendicular to the welding direction and pulled up to failure in the temperature range of 400 to 500°C and at strain rates of 2.8×10-4 s-1 to 5.6×10-1 s-1. The friction-stir welded material exhibited excellent superplastic properties. The highest elongation-to-failure of ~1370% was recorded at a temperature of ~450°C and an initial strain rate of 5.6×10-2 s-1, where the strain rate sensitivity coefficient was about 0.64. The relationship between superplastic ductility and microstructure is discussed.

Effects of Temperature, Strain Rate and Grain Size on Superplastic Behavior of Magnesium

2012 ◽  
Vol 488-489 ◽  
pp. 27-34 ◽  
Author(s):  
Muhammad Waseem Soomro ◽  
Thomas Rainer Neitzert
Keyword(s):  
Grain Size ◽  
Strain Rate ◽  
Magnesium Alloys ◽  
Room Temperature ◽  
Superplastic Forming ◽  
Experimental Results ◽  
Superplastic Behavior ◽  
Influence Of Temperature ◽  
Effects Of Temperature ◽  
Temperature Strain

The influence of temperature, grain size and strain rate on superplasticity of magnesium is investigated. Different approaches are compared along with their experimental results to show the variation in the amount of superplasticity by varying above mentioned parameters. At room temperature magnesium alloys usually have poor formability but recent studies of some alloys such as ZE10, AZ31, AZ61 AZ60, AZ80 and AZ91 are pointing that by varying the temperature along with grain size and strain rate improved formability is possible or even superplastic forming of these alloys can be achieved to meet the demands of automotive, aircraft and other weight conscious industries.

Superplastic Forming of Combustion Chamber

2011 ◽  
Vol 87 ◽  
pp. 132-135 ◽  
Author(s):  
Ho Sung Lee ◽  
Jong Hoon Yoon ◽  
Joon Tae Yoo ◽  
Yeng Moo Yi
Keyword(s):  
Stainless Steel ◽  
Combustion Chamber ◽  
Duplex Stainless Steel ◽  
Superplastic Forming ◽  
Liquid Propellant ◽  
Superplastic Behavior ◽  
Fine Grained ◽  
Forming Technology ◽  
Duplex Steel ◽  
Two Phases

The major advantage of superplastic forming (SPF) technology is that it can form integral and complex components in simple operation, since it is possible to form one or more sheets of superplastic grade metal into single surface tools by relatively low gas pressure. Duplex steel contains two phases in nearly equal proportions which can suppress grain growth at a high temperature, like superplastic Ti-6Al-4V, and many duplex stainless steels with fine grained microstructures show superplastic behavior. In this study, superplastic forming technology was developed to fabricate a duplex stainless steel sheet for the outer surface of liquid propellant combustion chamber. Superplasticity of this alloy was investigated and forming methodology was analyzed and developed. The experimental results show a complex configuration of aerospace component was successfully fabricated by superpalstic forming of a sheet of duplex stainless steel.

Mechanism of Low-Temperature Superplastic Deformation in Aluminum Alloys Containing a Dispersion of Nanoscale Al3(Sc,Zr) Particles

2016 ◽  
Vol 838-839 ◽  
pp. 150-156
Author(s):  
Rustam Kaibyshev
Keyword(s):  
Low Temperature ◽  
Strain Rate ◽  
Equal Channel Angular Extrusion ◽  
Rate Sensitivity ◽  
Sensitivity Coefficient ◽  
Superplastic Behavior ◽  
Ultrafine Grained ◽  
Elongation To Failure ◽  
The Difference ◽  
Average Size

The ultrafine grained (UFG) structure with an average size of ∼0.8 μm was produced in an Al-Li-Mg-Sc alloy by equal-channel angular extrusion (ECAE) at 325oC with a total strain of ~16. Superplastic behavior was examined in the temperature range 150-250oC at strain rates ranging from 10-5 to 10-2 s-1. A maximum elongation-to-failure of 440% was recorded at 175oC (~0.5 Tm, where Tm is the melting point) and a strain rate of 2.8×10-5 s-1 with the corresponded strain rate sensitivity coefficient of 0.32. Mechanisms of low-temperature superplasticity (LTSP) and high-strain-rate superplasticity (HTSP) are essentially the same. The difference between superplastic behaviors at low and high temperatures is attributed to applied stress.

Sign in / Sign up

Export Citation Format

Share Document