scholarly journals Solutions for thermally mismatched brazing operations for ceramic tokamak magnetic sensor

2016 ◽  
Vol 2016 (CICMT) ◽  
pp. 000058-000063 ◽  
Author(s):  
Caroline Jacq ◽  
Thomas Maeder ◽  
Benoit R. Ellenrieder ◽  
Philipp Windischhofer ◽  
Xinyue Jiang ◽  
...  

Abstract To monitor high-frequency fluctuations of the equilibrium magnetic field in tokamaks, a 3D magnetic sensor has been developed. The sensor, which is positioned inside the vacuum vessel behind the protective tiles of the tokamak and is exposed to potential temperatures up to 400°C, is based on thick-film and LTCC (low-temperature co-fired ceramic) technology. To connect the sensor to the cabling that runs inside the vacuum vessel, mineral-insulated cables have to be brazed to the sensor to ensure electrical connection together with mechanical robustness and sufficient thermal stability. As the brazing temperature is about 600°C, direct brazing to the alumina sensor substrate can cause failure by cracking induced by thermal stresses. It arises both by temperature gradients stemming from the localised heating and by the high thermal mismatch of alumina with the braze and wire materials. In previous work, high stresses from temperature gradients were efficiently decoupled by brazing indirectly to alumina beams attached to the main substrate, and local thermal stresses between alumina and braze/wire by using a porous metallisation. However, as the slender alumina beams protruding out of the substrate are somewhat cumbersome and fragile, three alternatives were studied in the present work: 1) testing shorter and more robust beams, 2) replacing the alumina beam by a silver wire, and 3) depositing a porous temperature- and stress-decoupling dielectric to enable direct brazing on the main alumina substrate. These solutions are characterised with respect to their mechanical robustness and of the degree of thermal decoupling with the substrate they provide.

2011 ◽  
Vol 59 (2) ◽  
pp. 376-396 ◽  
Author(s):  
D. Testa ◽  
Y. Fournier ◽  
T. Maeder ◽  
M. Toussaint ◽  
R. Chavan ◽  
...  

Author(s):  
Naoto Kasahara ◽  
Nobuyuki Kimura ◽  
Hideki Kamide

Fluid temperature fluctuates at an incomplete mixing area of high and low temperature fluids in nuclear components. It induces random variations of local temperature gradients in structural walls, which lead to cyclic thermal stresses. When thermal stresses and cycle numbers are large, there are possibilities of fatigue crack initiations and propagations. It is recognized that there are attenuation factors depending on fluctuation frequency in the transfer process from fluid temperature to thermal stresses. If a frequency of fluctuation is very low, whole temperature of the wall can respond to fluid temperature, because thermal diffusivity homogenizes structural temperature. Therefore, low frequency fluctuations do not induce large thermal stress due to temperature gradients in structures. On the other hand, a wall surface cannot respond to very high frequency fluctuation, since a structure has a time constant of thermal response. High frequency fluctuations do not lead to large thermal stress. Paying attention to its attenuation mechanism, Japan Nuclear Cycle Development Institute (JNC) has proposed a fatigue evaluation method related to frequencies. The first step of this method is an evaluation of Power Spectrum Density (PSD) on fluid, from design specifications such as flow rates, diameters of pipes and materials. In the next step, the PSD of fluid is converted to PSD of thermal stress by the frequency transfer function. Finally, the PSD of thermal stress is transformed to time history of stress under an assumption of random phase. Fatigue damage factors can be evaluated from stress ranges and cycles obtained by the rain flow wave count method. Proposed method was applied to evaluate fatigue damage of piping junction model tests conducted at Oarai Engineering Center. Through comparison with direct evaluation from measurements and predictions by conventional methods, the accuracy of the proposed method was validated.


2015 ◽  
Vol 2015 (CICMT) ◽  
pp. 000234-000238 ◽  
Author(s):  
Caroline Jacq ◽  
Thomas Maeder ◽  
Lucas Güniat ◽  
Adrien Corne ◽  
Duccio Testa ◽  
...  

A novel sensor based on thick-film + LTCC (low-temperature cofired ceramic) technology has been recently developed for sensing high-frequency 3D magnetic fields in tokamak fusion devices. For integration within the walls of the tokamak, the sensor has to be connected to the mineral-insulated cabling, which is carried out by brazing to ensure sufficient thermal stability. However, thermal mismatch stresses between the braze and the cable vs. the alumina substrate may cause local cracking of the latter during cooling, as the basic dense silver metallisation of the alumina does not provide a sufficient degree of stress decoupling. To address this issue, a series of porous metallisations have been formulated by incorporation of a mix of silver and fugitive graphite powder into a thick-film paste. To allow co-firing of thick, multi-layered prints. Such porous metallisations have allowed successful brazing operations, without cracking of the alumina substrate. Metallisations were assessed by measuring their electrical resistivity and shear stress have been realised as preliminary results to measure the influence of the porosity on the maximal stress before cracking.


2019 ◽  
Vol 23 (3) ◽  
pp. 746-754
Author(s):  
Dinar Dilshatovich Fazullin ◽  
Gennady Vitalievich Mavrin ◽  
Vladislav Olegovich Dryakhlov ◽  
Ildar Gilmanovich Shaikhiev ◽  
Irek Rashatovich Nizameyev

1998 ◽  
Vol 5 (3) ◽  
pp. 937-939 ◽  
Author(s):  
Nobuhiko Sakai ◽  
Hiroshi Ohkubo ◽  
Yasushi Nakamura

A 3 T superconducting magnet has been designed and constructed for magnetic Compton-profile (MCP) measurements with the new capabilities that the magnetic field direction can be altered quickly (within 5 s) and liquid-He refill is not required for more than one week. For the latter capability, two refrigerators have been directly attached to the cryostat to maintain the low temperature of the radiation shields and for the recondensation of liquid He. The system has been satisfactorily operated for over one week.


2020 ◽  
Vol 0 (0) ◽  
Author(s):  
Robert Müller ◽  
Janna Kuchinka ◽  
Thomas Heinze

Abstract Magnetic nanocomposites are a class of smart materials that have attracted recent interest as drug delivery systems or as medical implants. A new approach toward the biocompatible nanocomposites suitable for remote melting is presented. It is shown that magnetite nanoparticles (MNPs) can be embedded into a matrix of biocompatible thermoplastic dextran esters. For that purpose, fatty acid esters of dextran with adjustable melting points in the range of 30–140 °C were synthesized. Esterification of the polysaccharide by activation of the acid as iminium chlorides guaranteed mild reaction conditions leading to high-quality products as confirmed by Fourier-transform infrared (FTIR) and nuclear magnetic resonance (NMR) spectroscopy as well as by gel permeation chromatography (GPC). A method for the preparation of magnetically responsive bionanocomposites (BNCs) was developed consisting of combined dissolution/suspension of the dextran ester and hydrophobized MNPs in an organic solvent followed by homogenization with ultrasonication, casting of the solution, drying and melting of the composite for a defined shaping. This process leads to a uniform distribution of MNPs in BNC as revealed by scanning electron microscope (SEM). Samples of different geometries were exposed to high-frequency alternating magnetic field (AMF). It could be shown that defined remote melting of such biocompatible nanocomposites is possible for the first time. This may lead to a new class of magnetic remote-control systems, which are suitable for controlled release applications or self-healing materials. BNCs containing biocompatible dextran fatty acid ester melting close to human body temperature were prepared and loaded with Rhodamine B (RhB) or green fluorescent protein (GFP) as model drugs to evaluate their potential use as drug delivery system. The release of the model drugs from the magnetic BNC investigated under the influence of a high-frequency AMF (20 kA/m at 400 kHz) showed that on-demand release is realized by applying the external AMF. The BNC possessed a long-term stability (28 d) of the incorporated iron oxide particles after incubation in artificial body fluids. Temperature-dependent mobility investigations of MNP in the molten BNC were carried out by optical microscopy, magnetometry, alternating current (AC) susceptibility, and Mössbauer spectroscopy measurements. Optical microscopy shows a movement of agglomerates and texturing in the micrometer scale, whereas AC susceptometry and Mössbauer spectroscopy investigations reveal that the particles perform diffusive Brownian motion in the liquid polymer melt as separated particles rather than as large agglomerates. Furthermore, a texturing of MNP in the polymer matrix by a static magnetic field gradient was investigated. First results on the preparation of cross-linkable dextran esters are shown. Cross-linking after irradiation of the BNC prevents melting that can be used to influence texturing procedures.


Sign in / Sign up

Export Citation Format

Share Document