scholarly journals The effect of cavity disinfectants on the micro-shear bond strength of dentin adhesives

2014 ◽  
Vol 08 (02) ◽  
pp. 184-190 ◽  
Author(s):  
Dina Wafik Elkassas ◽  
Elham Mostafa Fawzi ◽  
Ahmed El Zohairy

ABSTRACT Objectives: This study was carried out to examine the effect of application of four different disinfecting agents on the micro-shear bond strength (μ-SBS) of an etch-and-rinse and self-etch adhesive systems. Materials and Methods: One hundred flat dentin surfaces of human molars were produced by wet grinding the buccal surfaces. Specimens were randomly assigned to five groups according to the disinfectant used: Group I: Control (no disinfectant); Group II: 5.25% sodium hypochlorite based; Group III: 2% chlorhexidine based (Consepsis), Group IV: 0.1% benzalkoniumchloride based (Tubulicid red) and Group V: 3% doxycycline based (Biopure, MTAD). Specimens were bonded using either Adper Single Bond 2 or Clearfil S3 Bond, which were employed according to the manufacturer's instructions. Resin composite microcylinders were bonded using Tygon® tubes for μ-SBS testing. The modes of failure were noted after visual examination using a binocular stereomicroscope at ×25 magnification. Failures were classified as adhesive, or mixed. μ-SBS results were analyzed using two-way ANOVA followed by Tukey's post-hoc test. Results: Dentin disinfectants tested significantly negated the bonding of Adper Single bond 2 and the groups were ranked; Group I > Group V = Group IV > Group II = Group III, meanwhile they enhanced significantly the μ-SBS values upon using Clearfil S3 Bond and were ranked; Group II > Group III = Group IV = Group V > Group I. Most failures were adhesive with the Adper single bond adhesive system. Mixed modes of failure were evident with Clearfil S3 bond. Conclusions: The disinfectants tested should not be used with Adper Single Bond 2 when applied before the etching step, However they could be used safely prior to bonding with Clearfil S3 Bond.

2015 ◽  
Vol 09 (02) ◽  
pp. 224-227 ◽  
Author(s):  
Shenbagakuttalam Anand ◽  
Ambrose Vedamanickam Rajesh Ebenezar ◽  
Nirupa Anand ◽  
Kothandaraman Rajkumar ◽  
Sekar Mahalaxmi ◽  
...  

ABSTRACT Objectives: To comparatively assess the micro shear bond strength (MSBS) of dentin bonded surface pre-treated zirconia ceramics. Materials and Methods: Zirconia blocks were sectioned into 50 cubical blocks. The blocks were further categorized into five groups (n = 10 each). Group I: No treatment was performed on zirconia samples; Group II: The zirconia samples were sand-blasted; Group III: Group II + etched with 9.8% of hydrofluoric (HF) acid for 60 s; Group IV: The sandblasted zirconia samples were selectively infiltrated with low fusing porcelain; and Group V: Group IV + etched using 9.8% HF acid gel. The zirconia specimens were then bonded to dentin samples, and the samples were tested for MSBS evaluation using universal testing machine. Results: The MSBS of all the four experimental groups shows greater value than group I. Among the experimental groups, group V and group IV do not show any statistical significant difference, whereas the mean MSBS of groups IV and V were statistically greater than group III and group II. However, groups I, II, and III do not show any statistical significant difference in mean MSBS values between them. Conclusion: Selective infiltration etching of zirconia ceramics provides the highest bond strength with resin cement.


2021 ◽  
Vol 48 (4) ◽  
pp. 397-404
Author(s):  
Seung-Hee Woo ◽  
Jisun Shin ◽  
Joonhaeng Lee ◽  
Miran Han ◽  
Jong Soo Kim

The purpose of this study was to evaluate the effect of a hemostatic agent containing aluminum chloride on the shear bond strength of resin-modified glass ionomer cement (RMGIC) to the dentin of primary teeth. Thirty-six extracted non-carious human primary teeth were collected in this study. Dentin surfaces were cut and polished. The specimens were randomly divided into 4 groups; group I: RMGIC without conditioning; group II: polyacrylic acid (PAA), RMGIC; group III: aluminum chloride, RMGIC; group IV: aluminum chloride, PAA, RMGIC. All teeth were thermocycled between 5.0℃ and 55.0℃ for 5000 cycles. Fifteen specimens from each group were subjected to shear bond strength test and 3 specimens from each group were inspected using scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy. The mean shear bond strength of each group was as follows: 4.04 ± 0.88 MPa in group I, 8.29 ± 1.40 MPa in group II, 1.39 ± 0.47 MPa in group III, 6.24 ± 2.76 MPa in group IV. There were significant differences among all groups (p < 0.001). SEM image of the dentinal tubules were partially exposed in group III and group IV. Fully exposed dentinal tubules were found in group II. In conclusion, aluminum chloride decreased the shear bond strength of RMGIC to dentin, regardless of PAA conditioning.


2010 ◽  
Vol 04 (03) ◽  
pp. 257-262 ◽  
Author(s):  
Oral Sokucu ◽  
Seyda Herguner Siso ◽  
Firat Ozturk ◽  
Ruhi Nalcaci

Objectives: The aim of this study was to compare the shear bond strength (SBS) of two different light sources under different thermal cycle frequencies.Methods: Ninety human premolar teeth were divided into six groups, in which three groups consisted of halogen groups – Group I was cured with halogen without thermocycle, Group II cured with halogen with 500 thermocycles, and Group III cured with halogen with 10,000 thermocycles. The other three groups consisted of Plasma arc (PAC) group – Group IV was cured with PAC without thermocycle, Group V cured with PAC thermocycled 500 cycles, and Group VI cured with PAC thermocycled 10,000 cycles. Two way ANOVA was used to compare the SBS between the groups, and chi squaretest was used to compare the bond failure of ARI scores among the groups.Results: A significant difference was found for curing lights (P<.001) and thermocycling (P<.01). However, there was no interaction between light curing and thermocycling (P=.177). The halogen groups demonstrated higher mean SBS than the PAC groups. Both groups showed a significant reduction between no cycles and 10,000 cycles (P<.05).Conclusions: Both light sources showed favorable SBS performance without the thermocycle procedure. Thermocycling significantly decreased the SBS values of both groups. (Eur J Dent 2010;4:257- 262)


2020 ◽  
Author(s):  
Purna Prasad Khanal ◽  
Basanta Kumar Shrestha ◽  
Rajiv Yadav ◽  
Sanjay Prasad Gupta

Abstract Background: Recycling the old or debonded bracket is one possible alternative to the replacement with new bracket. The aim of this study was to evaluate and compare the effect of different methods of recycling stainless steel orthodontic brackets on shear bond strength.Methods: One hundred twenty human premolars extracted for orthodontic purpose were randomly divided into four groups. Standard MBT (0.022”) brackets, (Leone co., Sesto, Florentine, Florence, Italy) were bonded on buccal surface of all samples with light cured adhesive primer Orthosol (Enlight, Ormco corp., USA) using LED curing unit for 10 seconds. Group I was assigned as control and the brackets of Group II, Group III and Group IV were subjected to recycling by flaming (Gas microtorch: RS Pro, Nozzle, MT 790) ,flaming with sandblasting (Bio-Art sandblaster; Rua Teotônio Vilela, Brazil) and flaming with ultrasonic cleaning (Ultrasonic cleaning unit ,Confident dental equipments Ltd, India) respectively. The recycled brackets were rebonded and final debonding of all brackets was done with universal testing machine (AG-IC/100 KN, Shimadzu, Japan) at a crosshead speed of 0.5mm/min and shear bond strength (MPa) was determined. The adhesive remnant index was evaluated by stereomicroscope at 10X magnification (Olympus corp., Japan). Results: The highest shear bond strength was obtained with Group I (10.35 ± 0.46 MPa), followed by Group III (9.36 ± 0.55 MPa), Group IV (5.97 ± 0.66 MPa) and the least value was obtained with Group II (4.30 ± 0.55 Mpa). Significant differences among the groups were detected by analysis of variance. Tukey post hoc multiple comparison test showed that the shear bond strength of each group was significantly different from one another (p < 0.001). The Chi-square showed statistically significant differences in the adhesive remnant index of the 4 groups (p < 0.001). Conclusions: Shear bond strength of new brackets was significantly higher than that of the recycled brackets. Among recycled brackets, flaming with sandblasting provided adequate shear bond strength, flaming with ultrasonic cleaning provided borderline value for clinical use while flaming alone led to significantly lower value.


2021 ◽  
Vol 2021 ◽  
pp. 1-7
Author(s):  
Purna Prasad Khanal ◽  
Basanta Kumar Shrestha ◽  
Rajiv Yadav ◽  
Dr. Sanjay Prasad Gupta

Aim. The aim of this study was to evaluate and compare the effect of different methods of recycling stainless steel orthodontic brackets on shear bond strength. Methods. One hundred twenty human premolars extracted for orthodontic purpose were randomly divided into four groups. Standard MBT (0.022″) brackets were bonded on the buccal surface of all samples with light cured adhesive primers using an LED curing unit for 10 seconds. Group I was assigned as control, and the brackets of Group II, Group III, and Group IV were subjected to recycling by flaming, flaming with sandblasting, and flaming with ultrasonic cleaning, respectively. The recycled brackets were rebonded, and final debonding of all brackets was performed using a universal testing machine at a crosshead speed of 0.5 mm/min and shear bond strength was determined. Data were analyzed with descriptive statistics, ANOVA, and post hoc tests. The adhesive remnant index was evaluated using a stereomicroscope at 10X magnification. Results. The highest shear bond strength was obtained with Group I (10.35 ± 0.46 MPa), followed by Group III (9.36 ± 0.55 MPa) and Group IV (5.97 ± 0.66 MPa), and the least value was obtained with Group II (4.30 ± 0.55 Mpa). Significant differences among the groups were detected by analysis of variance. Tukey’s post hoc multiple comparison test showed that the shear bond strength of each group was significantly different from one another ( p < 0.001 ). Conclusions. Shear bond strength of new brackets was significantly higher than that of the recycled brackets. Among recycled brackets, flaming with sandblasting provided adequate shear bond strength, flaming with ultrasonic cleaning provided a borderline value for clinical use, and flaming alone led to a significantly lower value.


2021 ◽  
Author(s):  
Purna Prasad Khanal ◽  
Basanta Kumar Shrestha ◽  
Rajiv Yadav ◽  
Sanjay Prasad Gupta

Abstract Aim: The aim of this study was to evaluate and compare the effect of different methods of recycling stainless steel orthodontic brackets on shear bond strength.Methods: One hundred twenty human premolars extracted for orthodontic purpose were randomly divided into four groups. Standard MBT (0.022”) brackets were bonded on buccal surface of all samples with light cured adhesive primer using LED curing unit for 10 seconds. Group-I was assigned as control and the brackets of Group-II, Group-III and Group-IV were subjected to recycling by flaming, flaming with sandblasting and flaming with ultrasonic cleaning respectively. The recycled brackets were rebonded and final debonding of all brackets was done with universal testing machine at a crosshead speed of 0.5mm/min and shear bond strength was determined. Data were analyzed with descriptive statistics, ANOVA and post hoc test. The adhesive remnant index was evaluated by stereomicroscope at 10X magnification.Results: The highest shear bond strength was obtained with Group I (10.35 ± 0.46 MPa), followed by Group III (9.36 ± 0.55 MPa), Group IV (5.97 ± 0.66 MPa) and the least value was obtained with Group II (4.30 ± 0.55 Mpa). Significant differences among the groups were detected by analysis of variance. Tukey post hoc multiple comparison test showed that the shear bond strength of each group was significantly different from one another (p < 0.001). Conclusions: Shear bond strength of new brackets was significantly higher than that of the recycled brackets. Among recycled brackets, flaming with sandblasting provided adequate shear bond strength, flaming with ultrasonic cleaning provided borderline value for clinical use while flaming alone led to significantly lower value.


2017 ◽  
Vol 18 (10) ◽  
pp. 947-958 ◽  
Author(s):  
Joao Cardoso Ferreira ◽  
Patrícia T Pires ◽  
Álvaro F de Azevedo ◽  
Sofia Arantes-Oliveira ◽  
Mário J Silva ◽  
...  

ABSTRACT Aim The study aimed to analyze the morphology of the dentin–resin interface yielded by two-step etch-and-rinse adhesive systems with different solvents and compositions. Materials and methods A total of 32 dentine disks were prepared and randomly assigned to four groups of one-bottle etchand-rinse adhesive systems containing different solvents: group I, Adper Scotchbond-1XT™ (ethanol/water); group II, XP-Bond™ (tertiary butanol); group III, Prime and Bond NT® (acetone); and group IV, One Coat bond® (5% water). Adhesive systems were applied onto dentin disks, which were then thermal cycled, divided into two hemi-disks (n = 16), and prepared for field-emission scanning electron microscopy to examine the dentin–resin interdiffusion zone. Microphotographs were scanned and data were processed. Data were compared with analysis of variance multivariant test after Kolmogorov–Smirnov and Shapiro–Wilk tests using Statistic Package for the Social Sciences. Results The adhesive layer thickness average found was group I: 45.9 ± 13.41 μm, group II: 20.6 ± 16.32 μm, group III: 17.7 ± 11.75 μm, and group IV: 50.7 ± 27.81 μm. Significant differences were found between groups I and IV and groups II and III (p<0.000). Groups I (3.23 ± 0.53 μm) and II (3.13 ± 0.73 μm) yielded significantly thicker hybrid layers than groups III (2.53 ± 0.50 μm) and IV (1.84 ± 0.27 μm) (p<0.003). Group III presented a less homogeneous hybrid layer, with some gaps. Tag length average was greater in groups II (111.0 ± 36.92 μm) and IV (128.9 ± 78.38 μm) than in groups I (61.5 ± 18.10 μm) and III (68.6 ± 15.84 μm) (p<0.008). Conclusion Adhesives systems with different solvents led to significant differences in the dentin–resin interface morphology. Solvents role in adhesives bond strength should be considered together with the other adhesive system components. Clinical significance The adhesive containing tertiary butanol, in addition, seems to originate a good-quality hybrid layer and long, entangled tags and also appears to have greater ability to originate microtags, which may indicate higher bond strength. How to cite this article Ferreira JC, Pires PT, de Azevedo ÁF, Arantes-Oliveira S, Silva MJ, de Melo PR. Morphology of the Dentin–resin Interface yielded by Two-step Etch-and-rinse Adhesives with Different Solvents. J Contemp Dent Pract 2017;18(10):947-958.


Coatings ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 273
Author(s):  
Abdulmajeed Ali Asiri ◽  
Rawaiz Khan ◽  
Sultan Saeed Alzahrani ◽  
Sajjad Haider ◽  
Salah Ud-Din Khan ◽  
...  

This study aimed to measure and compare the shear bond strength (SBS) of a self-adhering flowable resin composite to dentin with a conventional flowable composite, and evaluate the various modes of failure. Thirty human premolar teeth (n = 30) were randomly allocated to two groups (Group I: Vertise™ Flow; Group II: Filtek Ultimate + Single Bond Universal) of 15 specimens each, and SBS was measured for specimens from each group by applying a shear load using a universal testing machine (UTM). Modes of failure were observed with an optical microscope. An independent-samples T-test was performed to test Levene’s assumption of homogeneity of variance across both groups, with the critical value set at 0.05. The results revealed, that the self-adhering flowable composite (Group I: Vertise™ Flow) resulted in a lower shear bond strength compared with the conventional adhesive system composite (Group II: Filtek Ultimate + Single Bond Universal). Moreover, group I predominantly exhibited non-cohesive failure, which reflects poor bonding to dentin. On the other hand, Group II showed mixed failure for most of the samples, which demonstrated strong adhesive bonding. Therefore, it could be concluded that the self-adhering flowable resin composite (Group I) results in lower SBS to dentin compared with a conventional adhesive system.


2020 ◽  
pp. 1-11
Author(s):  
Anip K. Roy ◽  
Govind N. Prasad ◽  
Tushar V. Bhagat ◽  
Saurabh Chaturvedi ◽  
Vishwanath Gurumurthy ◽  
...  

BACKGROUND: The increased strength of zirconia has resulted in its widespread application in clinical dentistry. Nevertheless, the fracture of veneering porcelains remains one of the key reasons of failure. OBJECTIVE: The objective of this study was to compare and analyze the influence of surface conditioning methods on the core-veneer bond strength of zirconia restorations. METHODS: Thirty specimens of zirconia core with sizes 10 × 5 × 5 mm were layered with porcelain of sizes 5 × 3 × 3 mm. On the basis of different surface conditioning methods, four groups were made: Group I: abrasion with airborne alumina particles of 110 μm size, Group II: sandblasting with silica coated alumina particles of 50 μm in size, Group III (modified group): alteration with a coating of zirconia powder prior to sintering, and Group IV (control group): metal core specimens. The shear force of all specimens was tested using a universal testing machine with a 0.5 mm/min crosshead speed. One-way analysis of variance (ANOVA) and Tukey’s post hoc pair wise comparison (p= 0.05) were performed to analyze the shear bond strength. A scanning electron microscope was used to assess the fractured specimens. RESULTS: A statistically significant difference was noted between the groups. The mean value of shear bond strength was 40.25 MPa for Group I, 41.93 MPa for Group II, 48.08 MPa for Group III and 47.01 MPa for Group IV. CONCLUSIONS: The modified zirconia group and control group demonstrated a significantly higher mean bond strength than that of Group I, where airborne particle abrasion was used. The scanning electron microscope showed that cohesive fracture in the porcelain veneers was the main problem of failure in altered zirconia. The modified zirconia specimens in Group III demonstrated significantly improved values of shear bond strength.


2012 ◽  
Vol 17 (4) ◽  
pp. 1-7 ◽  
Author(s):  
Roberto Hideo Shimizu ◽  
Karlos Giovani Grando ◽  
Isabela Almeida Shimizu ◽  
Augusto Ricardo Andriguetto ◽  
Ana Cláudia Moreira Melo ◽  
...  

OBJECTIVE: This in vitro study was designed to evaluate the shear bond strength (SBS) of orthodontic metal brackets bonded by direct and indirect techniques. METHODS: Thirty healthy human maxillary premolar teeth were used. The teeth were divided into three groups of 10 teeth each: Group I - indirect bonding with SondhiTM Rapid-Set system (3M/Unitek), Group II - indirect bonding with TransbondTM XT adhesive system (3M/Unitek) and Group III - direct bonding with TransbondTM XT adhesive system (3M/Unitek). After bonding and obtaining the specimens for the study, the specimens were subjected to SBS testing in a universal testing machine (Emic, model DL-500). The Kolmogorov-Smirnov test was applied to ascertain that the data had a normal distribution and the Bartlett test to check whether there was homogeneity of variance. One-factor analysis of variance was performed and, subsequently, Tukey's test for paired means. A 5% significance level was adopted. RESULTS: The results of Group I were 67.6 (N) and 5.9 (MPa); Group II, 68.9 (N) and 6.1 (MPa) and Group III (control), 92.5 (N) and 8.1 (MPa). CONCLUSION: It can therefore be concluded that the means for Group III were significantly higher compared with Groups I and II in both Newton (N) and Megapascal (MPa) values. The means attained by the indirect bonding technique used in Groups I and II, however, exhibited no statistically significant differences.


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