scholarly journals A Low-Cost Assembly for Extraction of Hot Calcium Chloride Extractable Boron from Soil Samples

Agropedology ◽  
2019 ◽  
Vol 30 (2) ◽  
Author(s):  
P.C. Srivastava ◽  
◽  
S.P. Pachauri ◽  
Keyword(s):  
Low Cost ◽  
Calcareous Soils ◽  
Soil Samples ◽  
Water Soluble ◽  
Hot Water ◽  
Condenser Tube ◽  
Reflux Condenser ◽  
Hot Plate ◽  
Indian Agriculture ◽  
Different Soils

Among micronutrients, boron (B) occupies a prime place next to zinc (Zn) in Indian Agriculture. Acidic soils, coarse-textured soils subjected to leaching in high rainfall areas, and calcareous soils are likely to be deficient in B (Srivastava and Gupta 1996). According to an estimate based on soil testing of more than two lakh samples drawn from 508 districts of India indicated that 23.2 percent of soil samples are deficient in B (Shukla et al. 2019). Though there are several methods for the analysis of B in soils yet hot water-soluble B (Berger and Truog 1940; Gupta 1967) or dilute CaCl2 extractable B (Cartwright et al. 1983; Adams et al. 1991) are widely adopted for different soils all over the World (Diana 2008). The assembly adopted for the extraction of hot water soluble or dilute CaCl2 extractable B is costly as it requires the use of low B glass or quartz boiling flask equipped with a condenser tube for refluxing (Parker and Gardner 1981) which generally poses difficulty in handling and maintenance. Schuppli (1986) used a Teflon Erlenmeyer flask (125 ml) capacity attached to a Teflon reflux condenser to extract hot water-soluble B from soils, and an asbestos mat was placed between the hot plate and the flask to prevent damage to the Teflon flask. This publication proposes a low-cost assembly to extract hot water-soluble or hot CaCl2 extractable B in soils.

EXTRACTION OF BORON FROM CSSC REFERENCE SOILS BY HOT WATER, DILUTE CaCl2 AND MANNITOL-CaCl2 SOLUTIONS

1986 ◽  
Vol 66 (2) ◽  
pp. 377-381 ◽  
Author(s):  
P. A. SCHUPPLI
Keyword(s):  
Key Words ◽  
Soil Samples ◽  
Water Soluble ◽  
Hot Water ◽  
Distilled Water ◽  
Background Color ◽  
Color Development ◽  
Reference Soil ◽  
Highly Correlated

Soils were extracted by hot water, dilute CaCl2, and by mannitol-CaCl2 solutions and boron was determined by either azomethine-H or the curcumin method. Results were strongly method dependent; in particular results by the simplest method, mannitol-CaCl2, were generally lower and not highly correlated (r = 0.64) with those by the recommended procedure. This procedure involves extraction with hot distilled H2O (2:1 solution:soil), centrifugation, filtration, color development with azomethine-H and correction for background color. Extractable boron values by this procedure ranged from 0.1 to 1.4 mg kg−1. Background color can be further reduced by the substitution of 0.02 M CaCl2 for distilled water. Key words: CSSC reference soil samples, hot-water-soluble boron

scholarly journals Effect of Different Doses of Nutrients on Changes of Soil Organic Matter in Rendzic Leptosol

2012 ◽  
Vol 58 (4) ◽  
pp. 131-137
Author(s):  
Vladimír Šimanský ◽  
Erika Tobiašová
Keyword(s):  
Organic Matter ◽  
Soil Organic Matter ◽  
Soil Samples ◽  
Water Soluble ◽  
Hot Water ◽  
Fertilizer Treatment ◽  
Content Increase ◽  
Npk Fertilizer ◽  
Different Doses

Abstract The effect of different doses of NPK fertilizer on the changes in quantity and quality of soil organic matter (SOM) in Rendzic Leptosol was evaluated. Soil samples were taken from three treatments of different fertilization: (1) control - without fertilization, (2) NPK 1 - doses of NPK fertilizer in 1st degree intensity for vine, and (3) NPK 3 - doses of NPK fertilizer in 3rd degree intensity for vine in the vineyard. Soil samples were collected in years 2008-2011 during the spring. The higher dose of NPK fertilizer (3rd degree intensity of vineyards fertilization) was responsible for the higher content of labile carbon (by 21% in 0-0.3 m and by 11% as average of the two depths 0-0.3 m and 0.3-0.6 m). However, by application of a higher dose of NPK (1.39%) in comparison to no fertilizer treatment (1.35%) or NPK 1 (1.35%) the tendency of total organic carbon content increase and hot-water soluble carbon decrease were determined. Fertilization had a negative effect on SOM stability. Intensity of fertilization affected the changes in quantity and quality of SOM; therefore it is very important to pay attention to the quantity and quality of organic matter in productive vineyards.

scholarly journals Carbon fraction concentrations in a haplic Luvisol as affected by tillage

2014 ◽  
Vol 60 (No. 6) ◽  
pp. 262-266 ◽  
Author(s):  
J. Horáček ◽  
E. Strosser ◽  
V. Čechová
Keyword(s):  
Cultural Practices ◽  
Fulvic Acids ◽  
Soil Samples ◽  
Water Soluble ◽  
Hot Water ◽  
Protection Measures ◽  
Humus Substances ◽  
Conventional Ct ◽  
Soluble Carbon

Changes of soil organic matter (SOM) parameters were investigated in a haplic Luvisol with medium-heavy texture. Soil samples were taken from several layers at minimum (MT) and conventional (CT) tillage plots of a field experiment in Sitzenhof (Germany). All cultural practices except for tillage (crop rotation, fertilizing, protection measures, etc.) were identical over the whole time of the experiment. The concentrations of oxidizable carbon C<sub>ox</sub> and its constituents (humic acids (HA), fulvic acids (FA), and hot-water soluble carbon) are comparable in layers&nbsp;15&ndash;20 cm in both variants. In 0&ndash;15 cm and 30&ndash;55 cm layers, these concentrations were higher in the MT variant. A similar trend was observed in the colour quotient values of humic substances Q4/6, which indicates increasing condensation of humus substances (HS) at deeper layers in both variants, and it is also confirmed by a humic to fulvic acids ratio HA:FA. Concentrations of SOM fractions were higher (except 15&ndash;20 cm layers) in the MT than CT treatment throughout the profile, especially below the 30 cm depth. The SOM did not accumulate markedly in the surface layer of long-term MT treatment.

scholarly journals Status of Sulphur and Boron in Soils of North Gujarat Region of India

Agropedology ◽  
2019 ◽  
Vol 30 (2) ◽  
Author(s):  
V. P. Ramani ◽  
◽  
K.C. Patel ◽  
Dileep Kumar ◽  
K. P. Patel ◽  
...  
Keyword(s):  
Large Scale ◽  
Mean Value ◽  
Soil Samples ◽  
Water Soluble ◽  
Hot Water ◽  
Low Fertility ◽  
Fertility Level ◽  
S Deficiency ◽  
Nutrient Index ◽  
North Gujarat

The soils of North Gujarat region's were assessed for its Sulphur and Boron status due to its visible deficiency in plants. Study was conducted in three districts viz., Sabarkantha, Mehsana and Patan from which 60, 110 and 52 villages were selected and soils samples were collected with geo-tagging. A total of 1332 surface soil samples (Sabarkantha 360, Mehsana 660 and Patan 312) were collected from these respective districts. Analysis of these soil samples showed a wide variation in soil pH (6.04-9.72) from slightly acidic to alkaline. Organic carbon (OC) content ranged from 1.0 to 7.1 g kg-1, about 90, 65 and 74% of soil samples were found to be under the low OC in Mehsana, Sabarkantha and Patan districts, respectively. Available S content ranged from 1.7 to 68.5 mg kg-1 with a mean value of 15.6, 14.7 and 14.9 mg kg-1 in Mehsana, Sabarkantha and Patan districts, respectively. S deficiency in soils of all three districts was 18.1, 25.5 and 16.9 per cent, which appeared in medium-fertility class level as per Nutrient Index Value (NIV). The high magnitude of S deficiency was noticed in soils of Idar taluka (43.9 %) followed by Khedbrahma taluka (40.9%) of Sabarkantha district, showing medium-fertility class. Further, these samples were also found deficient in hot water-soluble boron (HWS-B) and it ranged from 0.06 to 3.12 mg kg-1 with a mean value of 0.44, 0.45 and 0.44 mg kg-1 in districts of Mehsana, Sabarkantha and Patan, respectively. The NIV indicated B fertility level of low to high. Per cent deficiency of B recorded about 29.4, 17.9 and 19.2 per cent in all three districts. A large scale of B deficiency was noticed in Satlasna taluka (52.4 %) of Mehsana district, which showed low fertility class.

Characterization of dissolved organic matter (DOM) extracted from soils by hot water percolation (HWP)

2010 ◽  
Vol 59 (1) ◽  
pp. 99-108 ◽  
Author(s):  
M. Takács ◽  
Gy. Füleky
Keyword(s):  
Organic Matter ◽  
Humic Acid ◽  
Natural Organic Matter ◽  
Extraction Methods ◽  
Soil Samples ◽  
Hot Water ◽  
Soil Extracts ◽  
Water Percolation ◽  
Soil Humic Acid

The Hot Water Percolation (HWP) technique for preparing soil extracts has several advantages: it is easily carried out, fast, and several parameters can be measured from the same solution. The object of this study was to examine the possible use of HWP extracts for the characterization of soil organic matter. The HPLC-SEC chromatograms, UV-VIS and fluorescence properties of the HWP extracts were studied and the results were compared with those of the International Humic Substances Society (IHSS) Soil Humic Acid (HA), IHSS Soil Fulvic Acid (FA) and IHSS Suwannee Natural Organic Matter (NOM) standards as well as their HA counterparts isolated by traditional extraction methods from the original soil samples. The DOM of the HWP solution is probably a mixture of organic materials, which have some characteristics similar to the Soil FA fractions and NOM. The HWP extracted organic material can be studied and characterized using simple techniques, like UV-VIS and fluorescence spectroscopy.

Water soluble nitrogen forms on two different soils as affected by biofertilization

2007 ◽  
Vol 35 (2) ◽  
pp. 597-600
Author(s):  
Ida Kincses ◽  
Tibor Filep ◽  
Péter Nagy ◽  
Andrea Kovács
Keyword(s):  
Water Soluble ◽  
Soluble Nitrogen ◽  
Nitrogen Forms ◽  
Different Soils

scholarly journals Effects of corn steep liquor on β-poly(l-malic acid) production in Aureobasidium melanogenum

AMB Express ◽  
2020 ◽  
Vol 10 (1) ◽  
Author(s):  
Genan Wang ◽  
Bingyi Shi ◽  
Pan Zhang ◽  
Tingbin Zhao ◽  
Haisong Yin ◽  
...  
Keyword(s):  
Malic Acid ◽  
Low Cost ◽  
Corn Steep Liquor ◽  
Enrichment Analysis ◽  
Tca Cycle ◽  
Water Soluble ◽  
Growth And Yield ◽  
The Tca Cycle ◽  
Steep Liquor ◽  
Aureobasidium Melanogenum

Abstractβ-poly(l-malic acid) (PMLA) is a water-soluble biopolymer used in medicine, food, and other industries. However, the low level of PMLA biosynthesis in microorganisms limits its further application in the biotechnological industry. In this study, corn steep liquor (CSL), which processes high nutritional value and low-cost characteristics, was selected as a growth factor to increase the PMLA production in strain, Aureobasidium melanogenum, and its metabolomics change under the CSL addition was investigated. The results indicated that, with 3 g/L CSL, PMLA production, cell growth, and yield (Yp/x) were increased by 32.76%, 41.82%, and 47.43%, respectively. The intracellular metabolites of A. melanogenum, such as amino acids, organic acids, and key intermediates in the TCA cycle, increased after the addition of CSL, and the enrichment analysis showed that tyrosine may play a major role in the PMLA biosynthesis. The results presented in this study demonstrated that the addition of CSL would be an efficient approach to improve PMLA production.

scholarly journals Soil fertility status of some of the intensive crop growing areas under major agroecological zones of Bangladesh

2016 ◽  
Vol 41 (4) ◽  
pp. 735-757 ◽  
Author(s):  
NC Shil ◽  
MA Saleque ◽  
MR Islam ◽  
M Jahiruddin
Keyword(s):  
Organic Matter ◽  
Soil Fertility ◽  
Calcareous Soils ◽  
Clay Content ◽  
Soil Samples ◽  
Exchangeable K ◽  
Low Level ◽  
Fertility Status ◽  
Agroecological Zones ◽  
High Level

Laboratory studies on soil fertility evaluation was carried out across major agroecological zones (AEZs) of Bangladesh to know the nutrient status of soils and to relate those with soil properties like pH, organic matter, CEC, and clay content. Thirty five composite soil samples were collected from intensive crop growing sites, which covered 17 AEZs of Bangladesh. After proper processing, the samples were analyzed for texture, pH, organic carbon, CEC, exchangeable cations (K, Ca, Mg and Na), total N, available P and S following standard methods. The textural class of the soils collected from AEZ 12 and 13 appeared to be mostly clay. Clay loam soil was found in AEZ 4, 8, 9, 11, 25 and 28. Loamy soil was seen in AEZ 1 while AEZ 22, 23 and 29 were mostly sandy textured. The results revealed that 65.7% of the tested soil was acidic while 25.7% was alkaline in nature. All the tested soils showed lower pHKCl compared to pHH2O thus possessed negative charge. About 68.6% of the collected soils contained low (1.10-1.70%) level of organic matter, 25.7% soils retained it at medium level (1.71-2.40) and 5.7% soils at very low level (<1.0%). All the tested soils appeared to be deficient (< 0.12%) in nitrogen content. 68.6% soil samples had the low level of available P while only 8.6% retained it an optimum amount. About 80% of the tested soils contained low level of available S (7.9- 14.7 mg kg -1) although coastal regions soils hold higher amount of available S. High CEC (20-38 cmol kg-1) was found in clay rich soils of AEZ 10, 11, 12, and 13. Study revealed that 40% of the collected soils were very low, 31.4% were low, 8.6% each of medium and optimum, and 11.4% contained high level of exchangeable K. The calcareous soils (AEZ 10, 11, 12 and 13) contained very high level of Ca. Non calcareous soils also showed fairly good level of Ca content except AEZ 1, 3, 23 and 29. Sandy textured soils of greater Dinajpur, Rangpur, Moulvibazar showed lower level of exchangeable Mg. About 86% of the tested soils had the lower (< 2%) potassium saturation percentage (KSP), which needs K application for sustainable crop production. Estimate showed that 44% variability for CEC may be attributed by clay content and the relationship was significant (p = 0.05). Again, 50.4 and 65.6% variability in exchangeable K and Mg, respectively may be governed by clay content of the soils, while such relationship for Ca was non-significant. CEC may contribute 62.2, 92.3 and 83.9% variability for exchangeable K, Ca and Mg content in soils, respectively. The fertility status of most of the studied soils (except AEZ 10, 12, 13 and to some extent 11) appeared to be low to very low, which demand judicious management in order to achieve food security and to conserve the soil fertility.Bangladesh J. Agril. Res. 41(4): 735-757, December 2016

Effect of previous cutting interval and of leaf area remaining after cutting on regrowth of Macroptilium atropurpureum cv. Siratro

1974 ◽  
Vol 14 (68) ◽  
pp. 343 ◽  
Author(s):  
RJ Jones
Keyword(s):  
Leaf Area ◽  
Practical Implication ◽  
Soluble Sugars ◽  
Ground Level ◽  
Fold Increase ◽  
Water Soluble ◽  
Hot Water ◽  
Lag Phase ◽  
Area Index ◽  
Plant Yield

Experiments with Siratro were conducted at Samford, south east Queensland to study the effects of previous cutting and defoliation treatments on regrowth. In the first experiment, swards of Siratro were cut at 7.5 cm above ground level every 4 weeks, every 8 weeks or cut once at 16 weeks during spring and summer. Regrowth of all treatments over ten weeks was measured after varying (by leaf removal) the stubble leaf area index (LAI) of the plots cut every four weeks. Pattern of regrowth yield was similar for all treatments with a pronounced lag phase after cutting. Regrowth yield after 10 weeks differed between treatments and was linearly related (P < 0.01 ) to residual LAI in the stubble at the start of regrowth. In the absence of stubble leaves, plots previously cut at 16 weeks or at 8 weeks yielded marginally more than those cut every 4 weeks. There were no marked treatment differences in gross root morphology other than a two fold increase in stolon rooting for the 16-week treatment. Nitrogen content of the roots (mean 1.38 per cent) was unaffected by treatment, but the per cent hot water soluble sugars were lower for the 16 week defoliation treatment than for the 8-week and the 4-week treatments. In the second experiment individual plants were cut to a uniform stubble every 4 weeks and either 0, 5, or 10 leaves were left. Dry weight of regrowth and stolon development were greatest when most leaves were left. Two thirds of the plants died after six cuttings with complete defoliation but none died when either 5 or 10 leaves were retained. Plant survival was not related to plant yield or degree of stoloniferous development. However, there was a strong correlation between stolon number and plant yield under this intensive cutting regime. The practical implication of the results in the management of Siratro is discussed.

scholarly journals Sorption of Clomazone in Brazilian Soils with Different Physical and Chemical Attributes1

2016 ◽  
Vol 34 (2) ◽  
pp. 357-364 ◽  
Author(s):  
G.A.M. PEREIRA ◽  
L.H. BARCELLOS JR. ◽  
V.A. GONÇALVES ◽  
D.V. SILVA ◽  
A.T. FARIA ◽  
...  
Keyword(s):  
Dry Matter ◽  
Organic Matter Content ◽  
Matter Content ◽  
Soil Samples ◽  
Chemical Characteristics ◽  
Abstract Knowledge ◽  
Analysis Of Similarity ◽  
Brazilian Soils ◽  
Physical And Chemical ◽  
Different Soils

ABSTRACT Knowledge of herbicides sorption by colloids predicts its movement in the soil profile and its effectiveness in controlling weeds and crops poisoning when directly applied to the soil. This knowledge becomes even more important for herbicides which have long persistence in the soil. In this research, clomazone sorption was estimated by the biological method in Brazilian soil samples with different physical and chemical characteristics, cultivated with sugarcane crops. As an indicator of the presence of clomazone in the soil, Sorghum bicolor was used. The data relating to assessments of poisoning and accumulation of dry matter of the plants were subjected to multivariate analysis of similarity among variables. After that, clomazone doses that caused 50% of intoxication in sorghum plants grown (C50) as well as sorption ratio (SR) of the herbicide in different soil types were estimated. There was similarity greater than 80% for data regarding the percentage of intoxication and accumulated dry matter, with the option to use only those related to the first variable. RS and C50 were higher in Organosol and lower in red-yellow Latosol with and without changing the pH. It was concluded that the clomazone dose to be recommended must be differentiated for different soils, since the value of clomazone sorption in the soil is dependent on its attributes, and the organic matter content is of the utmost importance.

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