scholarly journals Microwave assisted synthesis of some azo disperse dyes part 2: Eco-friendly dyeing of polyester fabrics by using microwave irradiation

2021 ◽  
Vol 12 (1) ◽  
pp. 64-68
Author(s):  
Mohamed Osman Saleh ◽  
Morsy Ahmed El-Apasery ◽  
Abdelhaleem Mostafa Hussein ◽  
Abu-Bakr Abdelhady El-Adasy ◽  
Magda Mohamed Kamel
Keyword(s):  
Microwave Irradiation ◽  
Disperse Dyes ◽  
Microwave Assisted Synthesis ◽  
Color Intensity ◽  
Light Fastness ◽  
Polyester Fabrics ◽  
Dye Absorption ◽  
Azo Disperse Dyes ◽  
Dyed Fabric ◽  
Green Technique

This study aimed to use microwave irradiation as a green technique, not only to enhance the dyeing efficiency of disperse-colored polyester fabrics, but also to conserve resources and minimize the environmental effects. Arylazopyrazolopyrimidinones dyes 1-9 were applied to polyester fabrics at 2% shade using conventional method and microwave at 100 °C. Both the color intensity expressed as dye absorption and the fastness characteristics of the dyed fabric were investigated. The K/S values are increased by increasing the time of irradiation from 10-60 minutes. The dyed substrate displayed good light fastness, and very good fastness levels to rubbing, perspiration washing, and sublimation, respectively.

Synthesis of 4-arylazo-2-(N-pyrazolylcarboxamido)thiophene disperse dyes for dyeing of polyester and their antibacterial evaluation

2020 ◽  
Vol 90 (23-24) ◽  
pp. 2795-2805
Author(s):  
Amal Al-Azmi ◽  
Elizabeth John
Keyword(s):  
Antibacterial Activities ◽  
Antimicrobial Activities ◽  
Disperse Dyes ◽  
Bacterial Strains ◽  
Light Fastness ◽  
Polyester Fabrics ◽  
Nuclear Magnetic Resonance Spectra ◽  
Current Article ◽  
Dyed Fabrics ◽  
Dyed Fabric

The current article aims to synthesize some new arylazo-thiophenes for dyeing polyester fabrics and screen their antimicrobial activities. The new 4-arylazo-2-( N-pyrazolylcarboxamido)-thiophene dyes 4a–e were prepared by the reaction of 2-acetyl-2-arylazo-thioacetanilide derivative 1 with 2-chloro- N-(3-methyl-1 H-pyrazol-5-yl)acetamide derivative 2. The structures of these prepared analogues were established via Fourier-transform infrared and 1H/13C nuclear magnetic resonance spectra. The synthesized dyestuffs were applied to polyester fabrics after establishing the optimal dyeing conditions at 130 ºC, high pressure, 3% shade, and liquor ratio 20:1 at pH 5. Furthermore, the dyed fabrics obtained under these optimal conditions resulted in proper colorfastness toward washing, rubbing, sublimation and perspiration, and were adequate for light fastness. They showed respectable antibacterial effectiveness against two bacterial strains, Staphylococcus aureus (Gram-positive) and Salmonella typhimurium (Gram-negative) bacteria. The dyed fabric with dye 4d displayed the best antibacterial activities with percentage reduction of 88% and 76% against S. aureus and S. typhimurium bacteria, respectively.

scholarly journals Synthesis and dyeing performance of some amphiphilic naphthalimide azo disperse dyes on polyester fabrics

2020 ◽  
Vol 85 (10) ◽  
pp. 1253-1264
Author(s):  
Umar Ameuru ◽  
Mohammed Yakubu ◽  
Kasali Bello ◽  
Peter Nkeonye ◽  
Azim Halimehjani
Keyword(s):  
Absorption Spectra ◽  
Electronic Absorption Spectra ◽  
Polyester Fabric ◽  
Disperse Dyes ◽  
Light Fastness ◽  
Visible Absorption ◽  
Polyester Fabrics ◽  
Dyeing Performance ◽  
Azo Disperse Dyes ◽  
Monoazo Disperse Dyes

A series of monoazo disperse dyes were synthesized by coupling diazotized 4-amino-N-dodecyl-1,8-naphthalimide with N,N-dialkyl anilines and naphthol derivatives. The synthesized intermediates and the dyes were characterized using FTIR, 1H-NMR, 13C-NMR, mass spectroscopy and elemental analysis (CHN). Visible absorption spectra of the dyes were examined in solvents of different polarities. The electronic absorption spectra cover a wavelength (?max) range of 515-535 nm in DMF at uniformly absorption intensity between 1.59-3.00?104 L mol-1 cm-1. The dyes gave deep and bright intense hues of light violet, maroon, pink and neon red on polyester fabrics. The dyes generally showed good washing and perspiration rating but poor to moderate light fastness properties on woven polyester fabric and could be recommended for commercial outlets.

scholarly journals Synthesis of some azo disperse dyes based on pyridone moiety and their application on polyester fabrics

2017 ◽  
Vol 60 (Conference Issue) ◽  
pp. 8-9 ◽  
Author(s):  
Morsy A. EL-Apasery ◽  
Salah Shakra ◽  
Dina Abbas ◽  
Hatem. E. Gaffer ◽  
Emad. A. Allam
Keyword(s):  
Disperse Dyes ◽  
Polyester Fabrics ◽  
Azo Disperse Dyes

scholarly journals Diphenyl (4′-(Aryldiazenyl)biphenyl-4-ylamino)(pyridin-3-yl)methylphosphonates as Azo Disperse Dyes for Dyeing Polyester Fabrics

2013 ◽  
Vol 2013 ◽  
pp. 1-5
Author(s):  
Mohamed F. Abdel-Megeed ◽  
Mohamed M. Azaam ◽  
Gamal A. El-Hiti
Keyword(s):  
Azo Dyes ◽  
Titanium Tetrachloride ◽  
Diazonium Salt ◽  
Disperse Dyes ◽  
Fastness Properties ◽  
Polyester Fabrics ◽  
Amino Compounds ◽  
Azo Disperse Dyes

Diphenyl (4′-aminobiphenyl-4-ylamino)(pyridin-3-yl)methylphosphonate(1)was synthesized in 88% yield from reaction of pyridine-3-carboxaldehyde with benzidine and triphenylphosphite in the presence of titanium tetrachloride as a catalyst. Diazotization of1gave the corresponding diazonium salt2which was coupled with several hydroxyl or amino compounds to give the corresponding azo dyes3–8in 82–88% yields after crystallization. The dyes produced were applied to polyesters as disperse dyes and their fastness properties were elevated.

Study of the Relationships between the Chemical Structures of Azo Disperse Dyes and their Dyeing Properties on Polyester

2010 ◽  
Vol 93-94 ◽  
pp. 332-335 ◽  
Author(s):  
T. Mungmeechai ◽  
Suesat Jantip ◽  
P. Suwanruji
Keyword(s):  
Bathochromic Shift ◽  
Spectroscopic Properties ◽  
Poly Lactic Acid ◽  
Disperse Dyes ◽  
Light Fastness ◽  
Dyeing Properties ◽  
Chemical Structures ◽  
Azo Disperse Dyes ◽  
Poly Ethylene ◽  
Dyed Fabrics

A series of azo disperse dyes was synthesized using 4-nitro aniline and 2-chloro-4-nitro aniline as diazo components. The coupling components were N,N-diethyl aniline, N,N-bis-β-hydroxyethyl aniline, N,N-bis-β-acetoxyethyl aniline, N,N-diethyl-m-toluidine, N,N-bis-β-hydroxyethyl-m-toluidine and N,N-bis-β-acetoxyethyl-m-toluidine. The structures of the synthesized dyes were confirmed by TLC, 1H NMR and elemental analysis. The spectroscopic properties of the dyes when dissolved in the organic solvents viz. ethyl acetate and methyl benzoate, were investigated. The absorption spectra of the dyes showed a bathochromic shift when the polarity of the solvents increased. In addition, the substituent groups on the dye structures influenced the spectroscopic properties of the dyes. The dyeing properties of the dyes on poly(ethylene terephthalate) and poly(lactic acid) fabrics were also studied. The dyes exhibited a slight difference in shade on the two polyester fabrics. Heat and light fastness properties of the dyed fabrics were also examined.

scholarly journals Microwave Assisted Synthesis of Some Azo Disperse Dyes part 3: Dye bath Reuse in Dyeing of Polyester

2021 ◽  
Vol 0 (0) ◽  
pp. 0-0
Author(s):  
Morsy Elapasery ◽  
Abdelhaleem Hussein ◽  
Mohamed Saleh ◽  
Abubaker Eladasy
Keyword(s):  
Disperse Dyes ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted ◽  
Azo Disperse Dyes
Sign in / Sign up

Export Citation Format

Share Document