Spectral X-ray tomography for 3D mineral analysis

Author(s):  
Jonathan Sittner ◽  
Jose R. A. Godinho ◽  
Axel D. Renno ◽  
Veerle Cnudde ◽  
Marijn Boone ◽  
...  

<p>Image based analytical tools in geoscience are indispensable for the characterization of minerals but most of them are 2D techniques, limited to the surface of a polished plane in a sample. X-ray micro computed tomography (micro-CT) is becoming a common analysis technique in geoscience and provides direct 3D information of the internal structure of a sample. A major drawback of micro-CT in the characterization of minerals, however, is the lack of chemical information. There have been different approaches to obtain chemical data using micro-CT but most of them are time consuming and difficult to adapt to regular use.</p><p>Therefore we introduce a potential new analytical tool: Laboratory-based Spectral X-ray Micro Computed Tomography (Sp-CT). Results from a spectral imaging detector prototype, installed inside a TESCAN CoreTOM micro-CT scanner, will be shown. This new analytical technique enables to obtain both high resolution structural and chemical information in 3D. With this information, the mineral distribution inside unbroken rocks and particles can be identified and quantified.</p><p>Based on the transmitted energy spectrum of a sample, main elements can be distinguished and minerals classified. It is also possible to quantify heavy elements within particles of complex composition and the measured sample volume is significantly larger compared to conventional analytical 2D techniques. Furthermore, Sp-CT is non-destructive and does not require sample preparation.</p><p>Sp-CT will open exciting new possibilities for mineral analysis. With this new technique, the 3D properties of the particles can now be measured and used for example in process mineralogy simulations. This is a major improvement to current simulations that predominantly use less representative 2D or bulk particle properties. Moreover, the Sp-CT could potentially be used as an alternative technique for regular characterization of ore deposits and processed ores since more representative volumes can be analyzed in a fast manner relative to existing techniques.</p><p>This research is part of the upscaling project “Resource Characterization: from 2D to 3D microscopy” and has received funding from European Institute of Innovation and Technology (EIT), a body of the European Union, under the Horizon 2020, the EU Framework Programme for Research and Innovation.</p>

Minerals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 178
Author(s):  
René Heyn ◽  
Abraham Rozendaal ◽  
Anton Du Plessis ◽  
Carene Mouton

The monetary value of gemstones is based on five variables: rarity, cut, weight, color and clarity. The latter refers to internal impurities and defects. Fashion may also dictate demand and price. To enhance some of these features and value, gemstones are treated. Disclosure or nondisclosure thereof has been controversial and affected consumer confidence. Most of these treatments are difficult to detect with the naked eye and accurately quantify with traditional optical and analytical methods. X-ray micro computed tomography (micro-CT or μCT) is proposed as a relatively low cost, physically non-destructive and complementary method to detect and quantify clarity enhancement and also to provide a unique 3D fingerprint of each gemstone. A collection of 14 cut colored gemstones was selected. Micro-CT scans allowed fracture detection, their distribution and calculation of filler volume as well as 3D mapping of inclusions, surface and internal imperfections and artificially induced modifications. As a result the method allows the construction of a digital twin. X-ray exposure could however induce unwanted color changes. This effect was minimized or eliminated by optimizing dosage and exposure time.


2020 ◽  
Vol 10 (1) ◽  
Author(s):  
Diana Ceballos-Francisco ◽  
Nuria García-Carrillo ◽  
Alberto Cuesta ◽  
María Ángeles Esteban

2020 ◽  
Author(s):  
Carlo Porfido ◽  
Roberto Rizzo ◽  
David Healy ◽  
Matteo Spagnuolo ◽  
Roberto Terzano ◽  
...  

<div><div><div><p>This work presents a study on the fracturing behaviour of a quartz tempered clay-based ceramic subjected to damage in freeze-thaw cycles. X-ray micro-computed tomography (micro-CT) provided high-resolution imaging of the ceramic before and during the freeze-thaw treatment, allowing to analyse a fully water-saturated sample using a special thermal stage designed to keep the sample frozen during analyses. Micro-CT 3D renderings showed the internal features of the specimen (i.e., quartz grain distribution), the increment of fracture count and size, and the detachment of ceramic and/or temper fragments from the edges of the sample over the cycles. Selected 2D micrographs, before and after freeze-thawing treatment, were analysed using the MATLAB toolbox FracPaQ. This software provided detailed data on fracture length, intensity, density, orientation and connectivity, and enabled to interpret the process of fracture initiation and propagation inside the material. These results showed that the temper plays a crucial role in ceramic fracturing behaviour under freeze- thawing conditions, as damage propagation is influenced by quartz grain distribution and orientation within the material. The study described in this work, not only offers new insights into the fracture dynamics of freeze-thawed clay-based ceramics, but also presents a new methodological approach to quantitatively measure fracture damage in porous materials.</p></div></div></div>


Materials ◽  
2020 ◽  
Vol 13 (16) ◽  
pp. 3606
Author(s):  
Armin Rashidi ◽  
Tina Olfatbakhsh ◽  
Bryn Crawford ◽  
Abbas S. Milani

X-ray computed tomography provides qualitative and quantitative structural and compositional information for a broad range of materials. Yet, its contribution to the field of advanced composites such as carbon fiber reinforced polymers is still limited by factors such as low imaging contrast, due to scarce X-ray attenuation features. This article, through a review of the state of the art, followed by an example case study on Micro-computed tomography (CT) analysis of low X-ray absorptive dry and prepreg carbon woven fabric composites, aims to highlight and address some challenges as well as best practices on performing scans that can capture key features of the material. In the case study, utilizing an Xradia Micro-CT-400, important aspects such as obtaining sufficient contrast, an examination of thin samples, sample size/resolution issues, and image-based modeling are discussed. The outcome of an optimized workflow in Micro-CT of composite fabrics can assist in further research efforts such as the generation of surface or volume meshes for the numerical modeling of underlying deformation mechanisms during their manufacturing processes.


2017 ◽  
Vol 35 (8) ◽  
pp. 933-938 ◽  
Author(s):  
Roberto Pisano ◽  
Antonello A. Barresi ◽  
Luigi C. Capozzi ◽  
Giorgia Novajra ◽  
Irene Oddone ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document