scholarly journals Komposisi kimia minyak atsiri daun cengkeh dari proses penyulingan uap

2018 ◽  
Vol 10 (1) ◽  
pp. 37 ◽  
Author(s):  
J Jayanudin
Keyword(s):  
Chemical Composition ◽  
Essential Oil ◽  
Food Industry ◽  
Steam Distillation ◽  
Composition Analysis ◽  
Distillation Process ◽  
Leaf Oil ◽  
Leaf Essential Oil ◽  
Anhydrous Na2so4 ◽  
Chemical Composition Analysis

The chemical composition of clove leaf essential oil obtained from steam distillation process Essential oils are needed in various industries such as industrial perfumes, cosmetics, pharmaceuticals, food industry, and beverages. This study aims to determine the chemical composition of clove leaf essential oil from steam distillation process using GCMS. Dry clove leaves weighing 1.5 kg are included in the kettle flute and sealed properly. Steam from the boiler flows into the kettle with the pressure of 0.5 barG, 1 barG and 1.5 barG for 5, 6 and 7 hours. Mixture oil and water out of the condenser are accommodated and let stand for 24 hours to separate water and oil. Clove leaf oil was purified with 10% bentonite by weight of oil at a temperature of 50oC with stirring for 1 hour. Clove leaf oil that has separated from bentonite added anhydrous Na2SO4 and let stand for 15 minutes and then separate the water and Na2SO4 in oil. Samples with % yield of the largest in its chemical composition analysis using GCMS. Based on the results obtained the largest yield is 1.84% with content of eugenol is 65.03% and 20.94% trans-caryophyllene. Keywords : Clove leaf, Eugenol, Essential Oil, Steam distillationAbstrakMinyak atsiri sangat dibutuhkan dalam berbagai industri seperti industri parfum, kosmetik, farmasi, industri makanan, dan minuman. Penelitian ini bertujuan untuk mengetahui komposisi kimia minyak atsiri daun cengkeh dari proses penyulingan uap menggunakan analisa GCMS. Daun cengkeh kering seberat 1,5 kg yang sudah bersih dari kotoran dimasukkan dalam ketel suling dan ditutup dengan rapat. Steam dari boiler dialirkan ke ketel suling dengan tekanan 0,5 barG, 1 barG dan 1,5 barG selama 5, 6 dan 7 jam. Campuran minyak dan air yang keluar dari kondenser ditampung dan diamkan selama 24 jam untuk memisahkan air dan minyak. Minyak daun cengkeh dimurnikan dengan bentonit 10% dari berat minyak pada suhu 50oC sambil diaduk selama 1 jam. Minyak daun cengkeh yang telah terpisah dari bentonit ditambahkan Na2SO4 anhidrat dan diamkan selama 15 menit kemudian pisahkan air dan Na2SO4 dalam minyak. Sampel dengan % rendemen terbesar di analisa komposisi kimianya menggunakan GCMS. Berdasarkan hasil penelitian didapat rendemen terbesar adalah 1,84% dengan kadar yaitu eugenol 65,03% dan trans-caryophyllene 20.94%.Kata kunci : Daun cengkeh, Eugenol, Minyak atsiri, Penyulingan uap

scholarly journals Bark and Leaf Essential Oil of Umbellularia californica, California Bay Laurel, from Oregon

2007 ◽  
Vol 2 (7) ◽  
pp. 1934578X0700200
Author(s):  
Rick G. Kelsey ◽  
Ovid McCuistion ◽  
Joe Karchesy
Keyword(s):  
Chemical Composition ◽  
Essential Oil ◽  
Steam Distillation ◽  
West Central ◽  
Umbellularia Californica ◽  
Leaf Oil ◽  
Leaf Essential Oil

The bark and leaf essential oil of Umbellularia californica (Hook. & Arn.) Nutt. from west central Oregon, USA, was isolated by steam distillation and the chemical composition analyzed by GC-FID and GC-MS. The three major components in bark oil were 1,8-cineole (36.0%), α-santalene (9.3), and α-terpineol (6.9%), while those in leaf oil were umbellulone (41.0%), 1,8-cineole (22.0%) and sabinene (10.2%).

scholarly journals Chemical composition analysis of the essential oil of Solanumn nigrum L. by HS/SPME method and calculation of the biochemical coefficients of the components

2017 ◽  
Vol 10 ◽  
pp. S2372-S2375 ◽  
Author(s):  
Avat (Arman) Taherpour ◽  
Mohammad Mehdi Khodaei ◽  
Baram Ahmed Hama Ameen ◽  
Majid Ghaitouli ◽  
Nosratollah Mahdizadeh ◽  
...  
Keyword(s):  
Chemical Composition ◽  
Essential Oil ◽  
Composition Analysis ◽  
Chemical Composition Analysis

scholarly journals Leaf Essential Oil of Manekia naranjoana (Piperaceae) from Costa Rica and its Cytotoxic Activity

2011 ◽  
Vol 6 (1) ◽  
pp. 1934578X1100600 ◽  
Author(s):  
Carlos Chaverri ◽  
Cecilia Díaz ◽  
José F. Cicció
Keyword(s):  
Costa Rica ◽  
Chemical Composition ◽  
Essential Oil ◽  
Tumor Cell ◽  
Cytotoxic Activity ◽  
Tumor Cell Lines ◽  
Capillary Gc ◽  
Leaf Oil ◽  
Leaf Essential Oil ◽  
Low Toxicity

The chemical composition of the leaf oil of Manekia naranjoana (C. DC.) Callejas (Piperaceae) from Costa Rica was analyzed by capillary GC/FID and GC/MS. Fifty-five compounds were identified. Major compounds from the leaf oil were β-pinene (30.6%), α-pinene (18.8%), limonene (13.7%), and β-caryophyllene (6.1%). The oil presented very low toxicity to tumor and non-tumor cell lines, even though it contains components, such as α- and β-pinene, limonene and others, which have been shown to be cytotoxic. This is the first report of the chemical composition of the essential oil obtained from this species.

scholarly journals Composition and in vitro Anticancer Activities of the Leaf Essential Oil of Neolitsea variabillima from Taiwan

2013 ◽  
Vol 8 (4) ◽  
pp. 1934578X1300800 ◽  
Author(s):  
Yu-Chang Su ◽  
Kuan-Ping Hsu ◽  
Eugene I-Chen Wang ◽  
Chen-Lung Ho
Keyword(s):  
Chemical Composition ◽  
Essential Oil ◽  
Cytotoxic Activity ◽  
Cancer Cells ◽  
Anticancer Activities ◽  
Leaf Oil ◽  
Leaf Essential Oil ◽  
Main Components ◽  
Type Apparatus

This study investigated the chemical composition and in vitro anticancer activities of the essential oil isolated from the leaf of Neolitsea variabillima. The essential oil was isolated using hydrodistillation in a Clevenger-type apparatus, and characterized by GC-FID and GC-MS. Sixty-seven compounds were identified, representing 100% of the oil. The main components identified were trans-β-ocimene (13.4%), α-cadinol (10.5%), terpinen-4-ol (9.3%), τ-cadinol (9.2%), β-caryophyllene (8.8%), and sabinene (6.7%). The anticancer activities of oil were evaluated. The results showed that the oil exhibited cytotoxic activity against human oral, liver, lung, colon, melanoma, and leukemic cancer cells. The presence of β-caryophyllene, τ-cadinol, and α-cadinol significantly contributed to the anticancer activities of N. variabillima leaf oil.

scholarly journals Characterization and Chemical Composition Analysis of Tea Tree (Meleuca alternifolia) Leaf Hydrosols Growing on Lombok Island

2022 ◽  
Vol 8 (1) ◽  
pp. 119-123
Author(s):  
Baiq Riyankati ◽  
Surya Hadi ◽  
Sri Seno Handayani
Keyword(s):  
Chemical Composition ◽  
Essential Oil ◽  
Essential Oils ◽  
Composition Analysis ◽  
Distilled Water ◽  
Tree Leaves ◽  
Tea Tree ◽  
Chemical Composition Analysis ◽  
By Products ◽  
Lombok Island

Tea tree is an essential oil-producing plant from Australia which is also found growing in several parts of Indonesia, including the island of Lombok. So far, tea tree essential oil producers on the island of Lombok do not utilize by-products in the form of hydrosol (distilled water) produced in the process of making essential oils. In this study, the characterization and analysis of the chemical composition of the hydrosol of tea tree leaves growing on the island of Lombok was carried out. The characteristic aroma of hydrosol is similar to that of tea tree essential oil. The results of the GC-MS analysis also showed that the hydrosol of tea tree leaves also had similarities with the essential oil, composed of major compounds in the form of trans-caryophyllene (28.58%), limonene (13.98%) and terpinen-4-ol (16.27%). Other compounds detected were -pinene (4.14%), -pinene (6.50%), -myrcene (8.09%), -terpineol (10.10%) and -terpinene (5.77%).

Sign in / Sign up

Export Citation Format

Share Document