Pure Nuclear Bragg Reflection due to Combined Magnetic and Quadrupole Interaction in Fe3O4

2021 ◽  
Vol 90 (10) ◽  
pp. 104713
Author(s):  
Shin Nakamura ◽  
Takaya Mitsui ◽  
Masayuki Kurokuzu ◽  
Susumu Shimomura
1979 ◽  
Vol 40 (C2) ◽  
pp. C2-350-C2-352 ◽  
Author(s):  
D. Chambaere ◽  
A. Govaert ◽  
E. de Grave ◽  
G. Harts ◽  
G. Robbrecht

2014 ◽  
Vol 134 (12) ◽  
pp. 1934-1935
Author(s):  
Tsunemasa Saiki ◽  
Yuya Matsui ◽  
Yasuto Arisue ◽  
Yuichi Utsumi ◽  
Akinobu Yamaguchi

Crystals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 312
Author(s):  
Florian Lauraux ◽  
Stéphane Labat ◽  
Sarah Yehya ◽  
Marie-Ingrid Richard ◽  
Steven J. Leake ◽  
...  

The simultaneous measurement of two Bragg reflections by Bragg coherent X-ray diffraction is demonstrated on a twinned Au crystal, which was prepared by the solid-state dewetting of a 30 nm thin gold film on a sapphire substrate. The crystal was oriented on a goniometer so that two lattice planes fulfill the Bragg condition at the same time. The Au 111 and Au 200 Bragg peaks were measured simultaneously by scanning the energy of the incident X-ray beam and recording the diffraction patterns with two two-dimensional detectors. While the former Bragg reflection is not sensitive to the twin boundary, which is oriented parallel to the crystal–substrate interface, the latter reflection is only sensitive to one part of the crystal. The volume ratio between the two parts of the twinned crystal is about 1:9, which is also confirmed by Laue microdiffraction of the same crystal. The parallel measurement of multiple Bragg reflections is essential for future in situ and operando studies, which are so far limited to either a single Bragg reflection or several in series, to facilitate the precise monitoring of both the strain field and defects during the application of external stimuli.


2013 ◽  
Vol 102 (1) ◽  
pp. 011113 ◽  
Author(s):  
Jin Yan ◽  
Zhenyue Luo ◽  
Shin-Tson Wu ◽  
Jyh-Wen Shiu ◽  
Yu-Cheng Lai ◽  
...  

1995 ◽  
Vol 39 ◽  
pp. 109-117
Author(s):  
Burkhard Beckhoff ◽  
Birgit Kanngießer

X-ray focusing based on Bragg reflection at curved crystals allows collection of a large solid angle of incident radiation, monochromatization of this radiation, and condensation of the beam reflected at the crystal into a small spatial cross-section in a pre-selected focal plane. Thus, for the Bragg reflected radiation, one can achieve higher intensities than for the radiation passing directly to the same small area in the focal plane. In that case one can profit considerably from X-ray focusing in an EDXRF arrangement. The 00 2 reflection at Highly Oriented Pyrolytic Graphite (HOPG) crystals offers a very high intensity of the Bragg reflected beam for a wide range of photon energies. Furthermore, curvature radii smaller than 10 mm can be achieved for HOPG crystals ensuring efficient X-ray focusing in EDXRF applications. For the trace analysis of very small amounts of specimen material deposited on small areas of thin-filter backings, HOPG based X-ray focusing may be used to achieve a very high intensity of monochromatic excitation radiation.


1991 ◽  
Vol 44 (13) ◽  
pp. 6728-6730 ◽  
Author(s):  
Dale W. Mitchell ◽  
S. B. Sulaiman ◽  
N. Sahoo ◽  
T. P. Das ◽  
W. Potzel ◽  
...  

1992 ◽  
Vol 47 (1-2) ◽  
pp. 353-360 ◽  
Author(s):  
W. S. Veeman

AbstractThe nutation frequency of a quadrupolar spin I depends on the quadrupole interaction. From nutation spectra, therefore, one obtains information about the direct surrounding of the atom. The theory of the straightforward and of more complicated nutation NMR experiments is outlined. Two applications of nutation NMR, to 23Na in zeolites and 27Al in alumina, are shown. In this way in CaO • 6 Al2O3 penta-coordinated aluminum has been detected


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