dynamic mechanical spectroscopy
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2015 ◽  
Vol 293 (12) ◽  
pp. 3603-3610 ◽  
Author(s):  
Shiyuan Li ◽  
Xian Zhang ◽  
Zhen Gu ◽  
Hang Cao ◽  
Xin Ding ◽  
...  

2013 ◽  
Vol 48 ◽  
pp. 132-139 ◽  
Author(s):  
Xiaoan Wang ◽  
Kewei Xiang ◽  
Dian Zhang ◽  
Jinrong Wu ◽  
Guangsu Huang

2006 ◽  
Vol 115 ◽  
pp. 151-156 ◽  
Author(s):  
A. Gasmi ◽  
M. Gouasmia ◽  
S. Etienne

Dynamic mechanical spectroscopy and differential scanning calorimetry measurements carried out on PVDF films are reported. Several mechanical relaxations are observed around - 100° C, -40° C, and 17° C at 1 Hz, respectively. It is shown that thermomechanical treatments induce variation of material morphology as revealed by calorimetry and low-frequency mechanical spectroscopy. The effect of long-term ageing at room temperature is attributed to reversible melting and formation of small crystallites. The molecular rearrangements involved in ageing at room temperature are characterized by a slow dynamics.


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