The Role of Parent Phase Compliance on the Fatigue Lifetime of Ni–Ti

It has been previously suggested that the fatigue lifetime of superelastic Ni–Ti might be improved if the R-phase were the parent to martensite rather than austenite. This body of work tests that hypothesis in two separate side-by-side fatigue tests both carefully constructed to match the superelastic properties in the two study arms. Both experiments show the R-phase parent to be more durable than the more commonly considered austenitic parent phase. The first experiment considers straight wire specimens fabricated from standard purity material, in a tension–tension fatigue test to 107 cycles, at mean strain ranging of 0.5–5.8% and strain amplitudes of 0.15–0.45%. The second experiment considers formed wire specimens in bending fatigue, more representative of realistic medical components, with a maximum mean strain of 1.2%, and maximum strain amplitudes ranging from 0.72 to 1.64%. Compared with the austenitic parent material, the R-phase material tolerated 0.1–0.3% higher strain amplitudes.

Production of Single-Phase Hydroxyapatite Porous Bodies from Gypsum/Polystyrene

Porous bodies were produced using hydroxyapatite as a starting material, gypsum, high purity material, low cost and that can be molded into the desired shape. Also, beads of polystyrene polymer. The first step of this work was to produce porous gypsum blocks obtained by mixing gypsum, water and polystyrene. After drying, they were submerged in acetone solvent for solubilizing the polymer and pore formation. The porous hydroxyapatite was synthesized in a second stage, where the porous gypsum blocks were immersed in a solution of (NH4)2HPO4 0.5 mol L-1 to 100 ° C and pH 7.0-9.0 for 24 hours. From this method, it was possible to produce bodies single phase hydroxyapatite with a maximum porosity of 70 ± 3% and a compressive strength of 1.48 ± 0.17 MPa.

Microstructure and Texture Evolutions in AA1200 Aluminum Alloy Deformed by Accumulative Roll Bonding Method

The results of studies carried out on AA1200 aluminum alloy deformed by Accumulative Roll Bonding (ARB) are presented in this paper. The commercial purity material was deformed up to 10 cycles (equivalent plastic strain of 8) at room temperature. The deformed microstructures and the crystallographic textures were characterized by transmission (TEM) and scanning (SEM) electron microscopes and high resolution orientation mapping. It was found that increased deformation leads to a strong increase of quantity of high angle (>15°) grain boundaries and strong grain refinement (up to 200-300 nm). The microstructure observations and TEM and SEM local orientation measurements allowed identifying fine and strongly disoriented planar dislocation structure of nanolayers described by strong texture components close to two nearly complementary positions of {112} orientation.

The Effect of Purity of Zirconium Material on Mechanical Properties and Microstructure of Zr-Based Bulk Metallic Glass

Series of rod samples of Zr55Al10Ni5Cu30 alloy were prepared by magnetic suspend melting and copper mold suction casting method using 99.9wt% high purity zirconium and 99.4wt% low purity sponge zirconium respectively, the effect of purity of zirconium material on mechanical properties and microstructure of Zr-based bulk metallic glass were investigated. The result shows that high purity material alloy could enhance the thermal stability and glass forming ability of Zr-based bulk amorphous alloy, compression fracture surface analysis indicate that the vein patterns density increase with the material elements purity increase, the average compressive fracture strength is increased to 8.52% than that of low purity samples.

Effect of Strain Path on Microstructure and Texture Development in ECAP Processed AA3104 Alloy

The objective of the study was to determine the effect of strain path on texture, microstructure and mechanical properties development of severely deformed Al-Mn-Mg alloy. The commercial purity material (AA3104 alloy) was deformed via Equal Channel Angular Pressing (ECAP) up to 10 passes following routes A, B, and C. The deformed and partially recrystallized microstructures and the crystallographic textures were characterized by transmission (TEM) and scanning (SEM) electron microscopy including systematic local orientation measurements (TEM and SEM FEG orientation mapping). The crystallographic texture was determined using X-ray diffraction on a sample section perpendicular to the extension direction (ED). In order to estimate the homogeneity of strengthening the systematic measurements of Vickers micro hardness in the plane perpendicular to the ED was performed. It was found out that different routes led to strong differences in microstructure of billets. In the case of route A and B strong macro cracking appeared after 5 and 3 passes, respectively. A good quality billet after 10 passes was obtained only in the case of route C. Texture evolution turned out to follow nearly the same ‘course’ for different routes of ECAP. However, the intensity of particular texture components was different in each case. TEM observations and local orientation measurements allowed identifying fine and strongly disoriented planar dislocation structure of nanolayers in the case of route A and C. In the case of route B nearly equiaxed structure of fine grains was observed after 3 passes. Moreover, irrespective of the applied deformation routes large, not deformable second phase particles strongly influenced strengthening of the matrix and nucleation during the recrystallization.

Microcracking, Strain Rate and Large Strain Deformation Effects in Molybdenum Disilicide

High purity molybdenum disilicide was deformed in compression to strains ranging from 5 to >50%. The deformation was accomplished at temperatures in the range 1200°-1400°C and at strain rates from 10−3 to 10−5 sec−1. The strength of this high purity material was found to be at least twice that of MoSi2 produced by the hot pressing of commercial powder. Microstructural examination revealed that subgrain formation resulted from modest strains (≈10%) while dynamic recrystallization was observed following large strains. Transmission microscopy revealed a significant change in the dislocation substructure after straining as the temperature was increased from 1300°C to 1400°C.