Phase Composition, Thermal Stability, Physical and Mechanical Properties of Superhard on Base Zr-Ti-Si-N Nanocomposite Coatings

Author(s):  
A.D. Pogrebnjak ◽  
O.V. Sobol ◽  
V.M. Beresnev ◽  
P.V. Turbin ◽  
G.V. Kirik ◽  
...  
Author(s):  
G.V. Shlyakhova ◽  
◽  
A.V. Bochkareva ◽  
M.V. Nadezhkin ◽  
◽  
...  

This study presents experimental results of structural analysis, such as phase composition, grains size assessment, strength and hardness of Ni-SPAN-C alloy 902 after various heat treatment modes (hardening and aging for stress relaxation). A thermal treatment mode has been selected to obtain higher physical and mechanical properties of the elinvar alloy. It is shown that the improvement of the alloy structure in thermal treatment occurs due to the thermic stresses, as well as the formation and dissolution of intermetallides.


Author(s):  
A. V. Hmelov

The effect of different с-BN and с-ZrO2 ratios on the phase composition, microstructure, relative density, open porosity, linear shrinkage, physicomechanical properties, and linear correlation of the elastic modulus and toughness of samples during plasma-spark sintering at pressing load 70 MPa in the range of 1200‒1600 °C is shown. The synthesized powders of TiC, c-BN and c-ZrO2, sintered at 1400 °C by the plasma-spark method, are characterized by intense crystallization of the phases. Sintered samples with different ratios of c-BN and c-ZrO2 show the intensive development of mullite and TiC. An increase in the c-BN / c-ZrO2 ratio promotes an active increase in c-BN and a less intensive increase in с-ZrO2 in the range of 1200‒1600 °C, and it causes the formation of a less uniform and densely sintered crystalline microstructure with a large number of pores at 1500 °C. This sample has lower values of physical and mechanical properties and a lower linear correlation of the modulus of elasticity and toughness in the range of 1200‒1600 °C and lower crack resistance at 1500 °C. Ill. 9. Ref. 13. Tab. 1.


2016 ◽  
Vol 29 (2) ◽  
pp. 197-204 ◽  
Author(s):  
Xiaodong Ji ◽  
Jingling Yan ◽  
Xiuju Liu ◽  
Zikun Wang ◽  
Zhen Wang

Several partially bio-based polyimides have been successfully synthesized by polycondensation between bis(4-aminophenyl)isohexides with various commercial dianhydrides. Flexible and free-standing films were readily obtained from their poly(amic acid) or polyimide solutions. A systematic investigation of the structure–property relationship of polyimides highlights the significant impact of the isohexides moieties on their physical and mechanical properties (glass transition temperature, inherent viscosity, thermal stability, solubility, and mechanical properties). The results revealed that these polyimides exhibited comparable thermal stability and mechanical properties to those of petrochemical-based ones.


2021 ◽  
Vol 410 ◽  
pp. 324-329
Author(s):  
Fedor V. Vodolazskiy ◽  
Anatoliy G. Illarionov ◽  
Natalya A. Shirinkina

Macro-, microstructural, fine structure, phase composition, texture and complex of physical and mechanical properties in titanium alloy VT23 (Ti-5.5Al-4.7V-2.5Mo-1.1Cr-0.7Fe, wt. %) tube were studded by the macroanalysis, optical and transmission microscopy, X-ray phase analysis, durometry and microindentation methods. A close relationship between the structural-textural-phase state formed during the extrusion and the obtained level of strength, plastic, durometric properties and the contact modulus of elasticity in a hot-extruded tube has been established.


2012 ◽  
Vol 585 ◽  
pp. 297-300 ◽  
Author(s):  
Prakriti Kumar Ghosh ◽  
Manjeet Singh Goyat ◽  
Deepak Mishra ◽  
Rishabh Nagori

The effect of type of nanoparticles on morphology, thermal and mechanical properties of epoxy-nanoparticulate composite adhesive produced via ultrasonic vibration process has been investigated. The morphology, thermal and mechanical properties of epoxy-nanoparticulate composite adhesive was measured with FESEM/AFM, DTA/TGA, and Hounsfield respectively. The FESEM/AFM images of the epoxy-nanoparticulate composite adhesive reveals significantly fine dispersion of nanoparticles. The incorporation TiO2 nanoparticles in epoxy adhesive results in improved glass transition temperature (Tg), thermal stability and tensile properties of the nanocomposite. But, the incorporation of comparatively finer size Al2O3 nanoparticles leads to decrease in the Tg, thermal stability and tensile properties of the nanocomposite.


2007 ◽  
Vol 534-536 ◽  
pp. 1093-1096
Author(s):  
Xi Yu Luo ◽  
Ming Qiang Tang ◽  
Xing Kuang ◽  
Man Huang ◽  
Hong Qiu Ma

In this paper, the fundamental attributes, phase composition of three pre-alloyed powders for diamond tools by water atomization were investigated. The density, hardness, bend strength and bending modulus of their sintered samples by hot pressing were examined under various temperatures. The results showed that the three pre-alloyed powders have excellent low temperature sintering characteristics. The physical and mechanical properties of the samples were found to be nearly the same as those of ultra-fine cobalt powders.


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