scholarly journals Monitoring the phase evolution in LiCoO 2 electrodes during battery cycles using in‐situ neutron diffraction technique

2019 ◽  
Vol 67 (3) ◽  
pp. 344-352 ◽  
Author(s):  
Anirudha Jena ◽  
Po‐Han Lee ◽  
Wei Kong Pang ◽  
Kuang‐Che Hsiao ◽  
Vanessa K. Peterson ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Phase Evolution ◽  
In Situ Neutron Diffraction ◽  
Neutron Diffraction Technique

In Situ Neutron Diffraction Measurement during Bainite Transformation and Accompanying Carbon Enrichment in Austenite at iMATERIA, J-PARC MLF

2021 ◽  
Vol 1016 ◽  
pp. 1079-1084
Author(s):  
Yusuke Onuki ◽  
Takashi Hirano ◽  
Kazuki Umemura ◽  
Shigeo Sato ◽  
Toshiro Tomida
Keyword(s):  
High Temperature ◽  
Neutron Diffraction ◽  
Analytical Approach ◽  
Diffraction Measurement ◽  
Experimental Equipment ◽  
Bainite Transformation ◽  
Neutron Diffraction Measurement ◽  
In Situ Neutron Diffraction ◽  
Neutron Diffraction Technique

The authors have developed the in situ neutron diffraction technique focusing on bainite transformation during austempering. Thanks to the features of time-of-flight type neutron diffraction, textures, phase fractions and lattice parameters can be simultaneously measured at high temperature. In this paper, the design of experimental equipment and analytical approach are mainly described.

Optimising Sintering in Metal Injection Moulding Using In Situ Neutron Diffraction

2012 ◽  
Vol 706-709 ◽  
pp. 1737-1742 ◽  
Author(s):  
D.J. Goossens ◽  
R.E. Whitfield ◽  
A.J. Studer
Keyword(s):  
Stainless Steel ◽  
High Temperature ◽  
Neutron Diffraction ◽  
Injection Moulding ◽  
Phase Evolution ◽  
Rietveld Analysis ◽  
Formation Temperature ◽  
Lower Temperature ◽  
In Situ Neutron Diffraction

The phase evolution during the sintering of metal injection moulded stainless steel, 316Land 17-4PH, has been observed using in situ neutron diffraction and Rietveld analysis. The formationof the ferrite phase in the final product is associated with the production of -ferrite at high temperatures.Coexistence of phases at high temperature is thought to allow the segregation of alloyingelements, stabilising the ferrite to lower temperature. To prevent ferrite in the final products the sinteringmust occur at a lower temperature than that at which -ferrite is formed. An alternative regimeis proposed in which the temperature would be cycled around the formation temperature of -ferrite.

scholarly journals Coexistence of Two Cubic-Lattice Co Matrices at High Temperatures in Co-Re-Cr-Ni Alloy Studied by Neutron Diffraction

2018 ◽  
Vol 2018 ◽  
pp. 1-6 ◽  
Author(s):  
Přemysl Beran ◽  
Debashis Mukherji ◽  
Pavel Strunz ◽  
Ralph Gilles ◽  
Markus Hölzel ◽  
...  
Keyword(s):  
High Temperature ◽  
Neutron Diffraction ◽  
Diffusion Processes ◽  
Phase Evolution ◽  
Ni Alloy ◽  
The Matrix ◽  
The Face ◽  
Fcc Phase ◽  
In Situ Neutron Diffraction

In situ neutron diffraction measurements were performed during heating to high temperature and cooling for a Co-17Re-23Cr-25Ni alloy. The allotropic transformation of the Co matrix and the evolution of the low-temperature hexagonal and high-temperature cubic Co phases were studied. A surprising observation was the splitting of the face-centred cubic (fcc) Co phase peaks at high temperature during heating as well as cooling. The phase evolution was monitored, and an appearance of the secondary fcc phase could be linked to the formation of σ phase (Cr2Re3 type) associated with a compositional change in the matrix due to diffusion processes at high temperature.

Deformation Behaviour of TRIP Steel Monitoring by in-Situ Neutron Diffraction

2011 ◽  
Vol 465 ◽  
pp. 390-394 ◽  
Author(s):  
Jozef Zrník ◽  
Ondrej Muránsky ◽  
Petr Šittner ◽  
E.C. Oliver
Keyword(s):  
Neutron Diffraction ◽  
Trip Steel ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Tensile Deformation ◽  
Deformation Behaviour ◽  
Tensile Load ◽  
Phase Evolution ◽  
In Situ Neutron Diffraction

The paper presents results of in-situ neutron diffraction experiments aimed on monitoring the phase evolution and load distribution in TRIP steel when subjected to tensile loading. Tensile deformation behaviour of TRIP steel with different initial microstructures showed that the applied tensile load is redistributed at the yield point and the harder retained austenite (Feγ) bears larger load then ferrite (Feα) matrix. After load partioning is finished, macroscopic yielding comes through simultaneous activity of the martensite transformation (in the austenite) and plastic deformation process in ferrite. The steel with higher volume fraction of retained austenite and less stronger ferrite appears to be a better TRIP steel having efficient structure for better plasticity purpose.

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