Plane-wave X-ray images of dislocations parallel to the diffraction vector

1984 ◽  
Vol 83 (1) ◽  
pp. 195-205 ◽  
Author(s):  
V. L. Indenbom ◽  
V. M. Kaganer ◽  
W. Möhling ◽  
E. V. Suvorov
Keyword(s):  
2014 ◽  
Vol 70 (a1) ◽  
pp. C1137-C1137
Author(s):  
Vahan Kocharyan ◽  
Sargis Khlopuzyan ◽  
Poghos Grigoryan ◽  
Edik Baghdasaryan ◽  
Ruben Amiraghyan

The research of the focusing and defocusing of the diffracted X-rays with different wave fronts in crystals under the influences of the temperature gradient and the ultrasonic vibrations is given in the works [1,2]. This work is dedicated experimentally investigation of Laue diffraction of the hard X-rays in quartz single crystals under the influence of the temperature gradient. It is shown that the reflected beams under the influence of the temperature gradient are focused. When the vector of the temperature gradient is anti parallel to the diffraction vector, in accordance to the increasing value of the temperature gradient the focus point continuously approaches the crystal. When the vector of the temperature gradient is parallel to the diffraction vector, in accordance with the increasing value of the temperature gradient the focus point continuously distances itself from the crystal, and at a certain value of the temperature gradient it becomes a plane wave. Parallel to the further increasing of the temperature gradient we see an imaginary focus, which continuously approaches the entry surface of the crystal. It is shown that by using a thicker single crystal it is possible to focus and pump a larger angular and spectral width of X-rays in the direction of diffraction.


1984 ◽  
Vol 49 (1) ◽  
pp. L1-L4
Author(s):  
Kohtaro Ishida ◽  
Yoshinori Kobayashi ◽  
Hiroyuki Katoh
Keyword(s):  

2018 ◽  
Vol 74 (6) ◽  
pp. 673-680 ◽  
Author(s):  
V. G. Kohn

The article reports an accurate theory of X-ray coplanar multiple diffraction for an experimental setup that consists of a generic synchrotron radiation (SR) source, double-crystal monochromator (M) and slit (S). It is called for brevity the theory of X-ray coplanar multiple SRMS diffractometry. The theory takes into account the properties of synchrotron radiation as well as the features of diffraction of radiation in the monochromator crystals and the slit. It is shown that the angular and energy dependence (AED) of the sample reflectivity registered by a detector has the form of a convolution of the AED in the case of the monochromatic plane wave with the instrumental function which describes the angular and energy spectrum of radiation incident on the sample crystal. It is shown that such a scheme allows one to measure the rocking curves close to the case of the monochromatic incident plane wave, but only using the high-order reflections by monochromator crystals. The case of four-beam (220)(331)({\overline {11}}1) diffraction in Si is considered in detail.


1966 ◽  
Vol 10 ◽  
pp. 67-79
Author(s):  
P. Penning

AbstractComplete dynamical solutions for three coupled plane-wave components in crystal structures with inversion symmetry have been found. After reviewing briefly the dynamical solutions for wave fields with two coupled plane-wave components, the results for the three-beam case are discussed in qualitative terms. Attention is paid to singular points and lines on the ω-surface, and to the attenuation of the mode-intensity because of absorption. The most surprising result is that in the case one of the reflections is forbidden (Umweganregung) the absorption is reduced in comparison with the adjoining two-beam cases. Experimental data are in reasonable agreement with the theory. Quantitative data are presented for a few three-beam cases of simultaneous diffraction of Cu Kα. radiation in germanium.


1999 ◽  
Vol 32 (2) ◽  
pp. 345-350 ◽  
Author(s):  
Hugo Mändar ◽  
Jürgen Felsche ◽  
Valdek Mikli ◽  
Toivo Vajakas

Dialogues for the estimation of crystallite size, shape and lattice strain are designed and included in an X-ray powder diffraction (XRPD) program, namedAXES. They implement peak fitting and Voigt analysis followed by a Williamson–Hall plot (WHP). Eight different peak-shape functions can be used for individual peak fitting. Volume-weighted crystallite size and effective lattice deformation are calculated from linear interpolation of the WHP. Actual dimensions (diameters of spheres, diameters and heights of cylinders) are calculated, assuming spherical or cylindrical shapes of the crystallites. Results of size–shape analyses can be visualized in the form of a WHP and as an arrow diagram (HPGL format), which shows distribution of observed apparent and true sizes of crystallites with a diffraction vector. The program has been written in Borland Pascal 7.0 for MS-DOS. The executable code is availableviathe World Wide Web.


1983 ◽  
Vol 22 (Part 2, No. 3) ◽  
pp. L151-L153
Author(s):  
Kohtaro Ishida ◽  
Yoshinori Kobayashi ◽  
Hiroyuki Katoh ◽  
Satio Takagi
Keyword(s):  

1982 ◽  
Vol 26 ◽  
pp. 275-282 ◽  
Author(s):  
C.N.J. Wagner ◽  
M.S. Boldrick ◽  
V. Perez-Mendez

AbstractA ϕ-ψ diffractometer has been designed and constructed to evaluate residual stresses in polycrystalline samples by x-ray diffraction. It permits rotations of the x-ray diffraction apparatus, consisting of an x-ray tube and a position-sensitive proportional counter, about two axes ϕ and ψ. The ϕ-rotation from 0° to 360° is carried out about the normal to the surface of the stationary sample, whereas the ψ-motion consists of a rotation from -45° to +45° about an axis lying in the sample surface and the diffraction plane, but perpendicular to the diffraction vector. This ϕ-ψ diffractometer permits the application of the ϕ- and ψ-differential and integral methods for the evaluation of the strain tensor and its gradient averaged over the depth of x-ray penetration into the sample. Assuming that isotropic elasticity theory is applicable, the stress tensor can then be evaluated from the measured strain tensor.


1984 ◽  
Vol 40 (a1) ◽  
pp. C324-C324
Author(s):  
K. Ishida ◽  
K. Umezawa ◽  
M. Kawata ◽  
T. Ogawa ◽  
S. Takagi

1992 ◽  
Vol 247 ◽  
Author(s):  
Yoshio Nogami ◽  
Kazuyoshi Ogasawara ◽  
Shigeki Takeuchi ◽  
Takehiko Ishiguro ◽  
Kazumasa Ohsumi ◽  
...  

ABSTRACTStacking of heterogeneous Langmuir-Blodgett films was studied by high resolution X-ray diffraction method using synchrotron radiation (SR) source. The diffraction patterns of the heterogeneous films formed with alternately deposited Cd salts of fatty acids with different length of alkyl chains exhibit anomalous oscillatory structure in diffraction vector.


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