Hysteretic Effect of Step by Step Heating on the Restriction of Gelatinization of Legume Starch

1987 ◽  
Vol 39 (7) ◽  
pp. 241-246 ◽  
Author(s):  
K. Minagawa ◽  
T. Ohkura ◽  
G. Goshima ◽  
Y. Miwa ◽  
H. Tsuge
Author(s):  
Lotte Melchior Larsen ◽  
David C. Rex ◽  
W. Stuart Watt ◽  
Philip G. Guise

NOTE: This article was published in a former series of GEUS Bulletin. Please use the original series name when citing this article, for example: Melchior Larsen, L., Rex, D. C., Watt, W. S., & Guise, P. G. (1999). 40Ar–39Ar dating of alkali basaltic dykes along the southwest coast of Greenland: Cretaceous and Tertiary igneous activity along the eastern margin of the Labrador Sea. Geology of Greenland Survey Bulletin, 184, 19-29. https://doi.org/10.34194/ggub.v184.5227 _______________ A 380 km long coast-parallel alkali basalt dyke swarm cutting the Precambrian basement in south-western Greenland has generally been regarded as one of the earliest manifestations of rifting during continental stretching prior to break-up in the Labrador Sea. Therefore, the age of this swarm has been used in models for the evolution of the Labrador Sea, although it has been uncertain due to earlier discrepant K–Ar dates. Two dykes from this swarm situated 200 km apart have now been dated by the 40Ar–39Ar step-heating method. Separated biotites yield plateau ages of 133.3 ± 0.7 Ma and 138.6 ± 0.7 Ma, respectively. One of the dykes has excess argon. Plagioclase separates confirm the biotite ages but yield less precise results. The age 133– 138 Ma is earliest Cretaceous, Berriasian to Valanginian, and the dyke swarm is near-coeval with the oldest igneous rocks (the Alexis Formation) on the Labrador shelf. A small swarm of alkali basalt dykes in the Sukkertoppen (Maniitsoq) region of southern West Greenland was also dated. Two separated kaersutites from one sample yield an average plateau age of 55.2 ± 1.2 Ma. This is the Paleocene–Eocene boundary. The swarm represents the only known rocks of that age within several hundred kilometres and may be related to changes in the stress regime during reorganisation of plate movements at 55 Ma when break-up between Greenland and Europe took place.


2021 ◽  
Vol 145 ◽  
pp. 106679
Author(s):  
Roberto Marani ◽  
Davide Palumbo ◽  
Umberto Galietti ◽  
Tiziana D'Orazio

1996 ◽  
Vol 62 (3) ◽  
pp. 446-452 ◽  
Author(s):  
Yoichi Abe ◽  
Kousaku Yasunaga ◽  
Seiichi Kitakami ◽  
Yuriko Murakami ◽  
Takao Ota ◽  
...  

2021 ◽  
Author(s):  
Zhenhua Xue ◽  
Wei Lin ◽  
et al.

Three figures (Figs. S1–S3) and two tables (Tables S1–S2). Figure S1: Images and related Energy Dispersive X-ray spectra to show that quartz melts infilled in feldspar crack; Figure S2: Features of samples selected for 40Ar-39Ar dating; Figure S3: Inverse isochron lines that yield false initial 40Ar/39Ar ratio; Table S1: Detailed SIMS U-Pb zircon results of sample CX48; Table S2: Detailed 40Ar/39Ar VG3600 Furnace Step-Heating Analytical Results.


Catalysts ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 1163
Author(s):  
Ning Cui ◽  
Kexiao Bi ◽  
Wei Sun ◽  
Qianqian Wu ◽  
Yinan Li ◽  
...  

MOF–derived porous carbon is a type of promising catalyst to replace expensive Pt–based catalysts for oxygen reduction reaction (ORR). The catalytic activity for ORR depends closely on pyrolysis conditions. In this work, a Co–doped ZIF–8 material was chosen as a research object. The effect of pyrolysis conditions (temperature, heating rate, two–step heating) on the ORR performance of ZIF–derived carbon catalysts was systematically studied. The Co–ZIF–8 catalyst carbonized at 900 °C exhibits better ORR catalytic activity than that carbonized at 800 °C and 1000 °C. Moreover, a low heating rate can enhance catalytic activity. Two–step pyrolysis is proven to be an effective way to improve the performance of catalysts. Reducing the heating rate in the low–temperature stage is more beneficial to the ORR performance, compared to the heating rate in the high–temperature stage. The results show that the Co–ZIF–8 catalyst exhibits the best performance when the precursor was heated to 350 °C at 2 °C/min, and then heated to 900 °C at 5 °C/min. The optimum Co–ZIF–8 catalyst shows a half–wave potential of 0.82 V and a current density of 5.2 mA·cm−2 in 0.1 M KOH solution. It also exhibits high content of defects and good graphitization. TEM mapping shows that Co and N atoms are highly dispersed in the polyhedral carbon skeleton. However, two–step pyrolysis has no significant effect on the stability of the catalyst.


Sign in / Sign up

Export Citation Format

Share Document