Determination of plutonium by isotopic dilution mass spectrometry following TTA-extraction

1969 ◽  
Vol 2 (3-4) ◽  
pp. 191-196 ◽  
Author(s):  
H. Bokelund
Keyword(s):  
Mass Spectrometry ◽  
Isotopic Dilution

Investigation of separation/purification methodologies for the determination of 232U and 236Pu in solution of spent nuclear fuels by α-spectrometry

2001 ◽  
Vol 89 (9) ◽  
Author(s):  
D. Solatie ◽  
P. Carbol ◽  
P. Peerani ◽  
M. Betti
Keyword(s):  
Mass Spectrometry ◽  
Anion Exchanger ◽  
Cooling Time ◽  
Isotopic Dilution ◽  
Nuclear Fuels

A methodology based on the use of several separation/purification steps exploiting TOPO, Dowex anion exchanger and UTEVA for attaining U and Pu fractions for α-spectrometry measurements is presented. The methodology is applied to the determination of the concentration ofAfter 2 years cooling time, the amount ofThe inventory of the major U and Pu are also determined by radiometric methods. The results are in agreement with those from isotopic dilution mass spectrometry.

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