Analysis of brittle layer forming mechanism in Ti6Al4V sloping structures by SLM technology

2018 ◽  
Vol 98 (5-8) ◽  
pp. 1783-1789 ◽  
Author(s):  
Zhiling Xiao ◽  
Yuhui Chen ◽  
Anthimos Georgiadis ◽  
Jianxiu Liu ◽  
Xiangkui Zhou ◽  
...  
Author(s):  
Uwe Lücken ◽  
Michael Felsmann ◽  
Wim M. Busing ◽  
Frank de Jong

A new microscope for the study of life science specimen has been developed. Special attention has been given to the problems of unstained samples, cryo-specimens and x-ray analysis at low concentrations.A new objective lens with a Cs of 6.2 mm and a focal length of 5.9 mm for high-contrast imaging has been developed. The contrast of a TWIN lens (f = 2.8 mm, Cs = 2 mm) and the BioTWTN are compared at the level of mean and SD of slow scan CCD images. Figure 1a shows 500 +/- 150 and Fig. 1b only 500 +/- 40 counts/pixel. The contrast-forming mechanism for amplitude contrast is dependent on the wavelength, the objective aperture and the focal length. For similar image conditions (same voltage, same objective aperture) the BioTWIN shows more than double the contrast of the TWIN lens. For phasecontrast specimens (like thin frozen-hydrated films) the contrast at Scherzer focus is approximately proportional to the √ Cs.


2011 ◽  
Vol 31 (5) ◽  
pp. 73-78
Author(s):  
Huijun LI ◽  
Xunhua ZHANG ◽  
Shuyin NIU ◽  
Kaining YU ◽  
Aiqun SUN ◽  
...  

2021 ◽  
Vol 10 (1) ◽  
Author(s):  
Ming-Xiang Mei ◽  
Muhammad Riaz ◽  
Zhen-Wu Zhang ◽  
Qing-Fen Meng ◽  
Yuan Hu

AbstractAs a type of non-laminated microbial carbonates, dendrolites are dominated by isolated dendritic clusters of calcimicrobes and are distinct from stromatolites and thrombolites. The dendrolites in the upper part of the Miaolingian Zhangxia Formation at Anjiazhuang section in Feicheng city of Shandong Province, China, provide an excellent example for further understanding of both growth pattern and forming mechanism of dendrolites. These dendrolites are featured by sedimentary fabrics and composition of calcified microbes as follows. (1) The strata of massive limestones, composed of dendrolites with thickness of more than one hundred meters, intergrade with thick-bedded to massive leiolites, formimg the upper part of a third-order depositional sequence that constitutes a forced regressive systems tract. (2) A centimeter-sized bush-like fabric (shrub) typically produced by calcified microbes is similar to the mesoclot in thrombolites but distinctive from clotted fabrics of thrombolites. This bush-like fabric is actually constituted by diversified calcified microbes like the modern shrub as a result of gliding mobility of filamentous cyanobacteria. Such forms traditionally include: the Epiphyton group (which actually has uncertain biological affinity), the Hedstroemia group which closely resembles modern rivulariacean cyanobacteria, and the possible calcified cyanobacteria of the Lithocodium–Bacinella group. (3) Significantly, dense micrite of leiolite is associated with sponge fossils and burrows, and is covered by microstromatolite. The Lithocodium–Bacinella group is a controversial group of interpreted calcified cyanobacteria in the Cambrian that has also been widely observed and described in the Mesozoic. Therefore, dendrolites with symbiosis of leiolites in the studied section provide an extraordinary example for further understanding of growing style of bush-like fabrics (shrubs) of the dendrolites dominated by cyanobacterial mats. Furthermore, the present research provides some useful thinking approaches for better understanding of the history of the Early Paleozoic skeletal reefs and the microbe–metazoan transitions of the Cambrian.


2019 ◽  
Vol 488 (1) ◽  
pp. 495-511
Author(s):  
Yuefang Wu ◽  
Xunchuan Liu ◽  
Xi Chen ◽  
Lianghao Lin ◽  
Jinghua Yuan ◽  
...  

Abstract Using the new equipment of the Shanghai Tian Ma Radio Telescope, we have searched for carbon-chain molecules (CCMs) towards five outflow sources and six Lupus I starless dust cores, including one region known to be characterized by warm carbon-chain chemistry (WCCC), Lupus I-1 (IRAS 15398-3359), and one TMC-1 like cloud, Lupus I-6 (Lupus-1A). Lines of HC3N J = 2 − 1, HC5N J = 6 − 5, HC7N J = 14 − 13, 15 − 14, 16 − 15, and C3S J = 3 − 2 were detected in all the targets except in the outflow source L1660 and the starless dust core Lupus I-3/4. The column densities of nitrogen-bearing species range from 1012 to 1014 cm−2 and those of C3S are about 1012 cm−2. Two outflow sources, I20582+7724 and L1221, could be identified as new carbon-chain-producing regions. Four of the Lupus I dust cores are newly identified as early quiescent and dark carbon-chain-producing regions similar to Lup I-6, which together with the WCCC source, Lup I-1, indicate that carbon-chain-producing regions are popular in Lupus I which can be regard as a Taurus-like molecular cloud complex in our Galaxy. The column densities of C3S are larger than those of HC7N in the three outflow sources I20582, L1221, and L1251A. Shocked carbon-chain chemistry is proposed to explain the abnormal high abundances of C3S compared with those of nitrogen-bearing CCMs. Gas-grain chemical models support the idea that shocks can fuel the environment of those sources with enough S+ thus driving the generation of S-bearing CCMs.


2021 ◽  
Vol 12 (1) ◽  
Author(s):  
Chen Peng ◽  
Gan Luo ◽  
Junbo Zhang ◽  
Menghuan Chen ◽  
Zhiqiang Wang ◽  
...  

AbstractElectrochemical CO2 reduction can produce valuable products with high energy densities but the process is plagued by poor selectivities and low yields. Propanol represents a challenging product to obtain due to the complicated C3 forming mechanism that requires both stabilization of *C2 intermediates and subsequent C1–C2 coupling. Herein, density function theory calculations revealed that double sulfur vacancies formed on hexagonal copper sulfide can feature as efficient electrocatalytic centers for stabilizing both CO* and OCCO* dimer, and further CO–OCCO coupling to form C3 species, which cannot be realized on CuS with single or no sulfur vacancies. The double sulfur vacancies were then experimentally synthesized by an electrochemical lithium tuning strategy, during which the density of sulfur vacancies was well-tuned by the charge/discharge cycle number. The double sulfur vacancy-rich CuS catalyst exhibited a Faradaic efficiency toward n-propanol of 15.4 ± 1% at −1.05 V versus reversible hydrogen electrode in H-cells, and a high partial current density of 9.9 mA cm−2 at −0.85 V in flow-cells, comparable to the best reported electrochemical CO2 reduction toward n-propanol. Our work suggests an attractive approach to create anion vacancy pairs as catalytic centers for multi-carbon-products.


Author(s):  
Mateus Dobecki ◽  
Alexander Poeche ◽  
Walter Reimers

AbstractDespite the ongoing success of understanding the deformation states in sheets manufactured by single-point incremental forming (SPIF), the unawareness of the spatially resolved influence of the forming mechanisms on the residual stress states of incrementally formed sheet metal parts impedes their application-optimized use. In this study, a well-founded experimental proof of the occurring forming mechanisms shear, bending and stretching is presented using spatially resolved, high-energy synchrotron x-ray diffraction-based texture analysis in transmission mode. The measuring method allows even near-surface areas to be examined without any impairment of microstructural influences due to tribological reactions. The depth-resolved texture evolution for different sets of forming parameters offers insights into the forming mechanisms acting in SPIF. Therefore, the forming mechanisms are triggered explicitly by adjusting the vertical step-down increment Δz for groove, plate and truncated cone geometries. The texture analysis reveals that the process parameters and the specimen geometries used lead to characteristic changes in the crystallites’ orientation distribution in the formed parts due to plastic deformation. These forming-induced reorientations of the crystallites could be assigned to the forming mechanisms by means of defined reference states. It was found that for groove, plate and truncated cone geometries, a decreasing magnitude of step-down increments leads to a more pronounced shear deformation, which causes an increasing work hardening especially at the tool contact area of the formed parts. Larger step-down increments, on the other hand, induce a greater bending deformation. The plastic deformation by bending leads to a complex stress field that involves alternating residual tensile stresses on the tool and residual compressive stresses on the tool-averted side incrementally formed sheets. The present study demonstrates the potential of high-energy synchrotron x-ray diffraction for the spatially resolved forming mechanism research in SPIF. Controlling the residual stress states by optimizing the process parameters necessitates knowledge of the fundamental forming mechanism action.


2003 ◽  
Vol 10 (3) ◽  
pp. 216-221 ◽  
Author(s):  
Yong-jun Shao ◽  
Sheng-lin Peng ◽  
Gan-guo Wu ◽  
Liang-ming Liu ◽  
Jian-qing Lai ◽  
...  
Keyword(s):  

2013 ◽  
Vol 781-784 ◽  
pp. 2490-2493
Author(s):  
Shuang Hong Liu ◽  
Kun Wang ◽  
Bing Feng

On the base of analysis about the capabilities of appropriative fuel, forming mechanism of accumulated ash in private engine firebox and causation that hardly blown away. Result show that the forming of accumulated ash is caused by sublimation of alumina and silicon oxide because blaze center is too close to the insulation apron. Excessive transgression of alumina and aggradation is the causation that accumulated ash was hardly blown away.


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