Simultaneous determination of p-hydroxyacetophenone, chlorogenic acid, and caffeic acid in Herba Artemisiae Scopariae by capillary electrophoresis with electrochemical detection

2007 ◽  
Vol 388 (2) ◽  
pp. 475-481 ◽  
Author(s):  
Xiao Yao ◽  
Gang Chen
2013 ◽  
Vol 750-752 ◽  
pp. 1613-1616
Author(s):  
You Yuan Peng

A method based on capillary electrophoresis with electrochemical detection was developed for the determination of polyphenols inLycopus LucidusTurcz. Operated in a wall-jet configuration, a 300 μm diameter carbon-disk electrode was used as the working electrode. Under the optimum conditions, the targeted analytes, i.e. rutin, chlorogenic acid, apigenin, luteolin and quercetin were baseline separated within 25 min in a 60mmol/L borate buffer (pH 9.0). Notably, excellent linearity was obtained over three orders of magnitude with detection limits (S/N=3) ranging from 1×10-7g/mL to 1×10-6g/mL for all analytes.


2012 ◽  
Vol 12 (6) ◽  
pp. 427-430
Author(s):  
FangJian CHEN ◽  
HongJie SONG ◽  
HongBn GAO ◽  
ZhiJun WANG ◽  
Peng FU ◽  
...  

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