Parallel synthesis of 1,2,4-triazole derivatives using microwave and continuous-flow techniques

2012 ◽  
Vol 16 (1) ◽  
pp. 81-90 ◽  
Author(s):  
Tamás Szommer ◽  
András Lukács ◽  
József Kovács ◽  
Miklós J. Szabó ◽  
Michael G. Hoffmann ◽  
...  
Author(s):  
David C. Cowell

An automated method is described, using standard continuous flow techniques, for the determination of urine fluoride ion concentration using a fluoride ion selective electrode. It is shown that the kinetics of the electrode response to changes in fluoride ion can be used for the accurate measurement of fluoride ion concentration in urine, and that equilibration of the electrode response is not a prerequisite for the measurement of fluoride ion. Recovery experiments are in the range 83 to 90%; in-batch precision is between 0·9 and 1·6% and carryover 2·5% or less.


2021 ◽  
Vol 25 ◽  
Author(s):  
Alexander Leslie ◽  
Angel Maria Joseph ◽  
Marcus Baumann

: An overview of the current uptake of continuous flow techniques for various functional group interconversion reactions is presented. Besides highlighting a variety of prominent examples and their main features, this review provides insights into specific reaction classes, such as oxidations, reductions, rearrangements as well as different C-H functionalization processes. While this review can only include key examples from the last decade, the reader will find a solid foundation of important transformations along with further references to inform and appreciate the opportunities arising from modern synthesis technologies such as flow synthesis.


2003 ◽  
Vol 9 (23) ◽  
pp. 5708-5723 ◽  
Author(s):  
Gerhard Jas ◽  
Andreas Kirschning

RSC Advances ◽  
2019 ◽  
Vol 9 (4) ◽  
pp. 2199-2204 ◽  
Author(s):  
Chuan-Tao Zhang ◽  
Rui Zhu ◽  
Zheng Wang ◽  
Bing Ma ◽  
Adrian Zajac ◽  
...  

Continuous flow method for parallel synthesis of diaryl ketones using commercially available reagents.


2005 ◽  
Vol 38 (4) ◽  
pp. 541-564 ◽  
Author(s):  
A. Abad ◽  
S. C. Cardona ◽  
J. I. Torregrosa ◽  
F. López ◽  
J. Navarro-Laboulais

ChemInform ◽  
2004 ◽  
Vol 35 (12) ◽  
Author(s):  
Gerhard Jas ◽  
Andreas Kirschning

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