scholarly journals Evolution of Microstructure and Internal Stresses in Multi-Phase Oxide Scales Grown on (110) Surfaces of Iron Single Crystals at 650 °C

2009 ◽  
Vol 73 (1-2) ◽  
pp. 115-138 ◽  
Author(s):  
C. Juricic ◽  
H. Pinto ◽  
D. Cardinali ◽  
M. Klaus ◽  
Ch. Genzel ◽  
...  
2018 ◽  
Vol 275 ◽  
pp. 81-88
Author(s):  
Monika Karoń ◽  
Marcin Adamiak

The purpose of this paper is to present the microstructure and mechanical behavior of 6060 aluminum alloy after intense plastic deformation. Equal Channel Angular Pressing (ECAP) was used as a method of severe plastic deformation. Before ECAP part of the samples were heat treated to remove internal stresses in the commercially available aluminium alloy. The evolution of microstructure and tensile strength were tested after 1, 3, 6 and 9 ECAP passes in annealed and non annealed states. It was found that intensely plastically deformed refined grains were present in the tested samples and exhibited increased mechanical properties. Differences were noted between samples without and after heat treatment


1994 ◽  
Vol 356 ◽  
Author(s):  
Laurence Gea ◽  
Jean-Luc Loubet ◽  
Roger Brenier ◽  
Paul Thevenard

Abstract(001) MgO single crystals were implanted with 150 keV krypton ions (Kr+) at a fluence of 5.1016 ions.cm-2 . The implanted surface, observed with an Atomic Force Microscope (AFM) exhibits striking features that can be described as undulations with a wavelength of 0.5 [μm. We correlate these features to the decrease in density and the stresses induced by the implantation damage. As a matter of fact, a model of surface instabilities provides a relationship between the wavelength of the ondulations and internal stresses. Using this model, implantation stresses are calculated to 2.2 GPa. This is in good agreement with the value of 2 GPa obtained with the help of the microindentation technique and the literature data. Some effects of an ionizing post-irradiation on stress and surface roughness are described.


1995 ◽  
Vol 78 (1) ◽  
pp. 41-48 ◽  
Author(s):  
Shiro Shimada ◽  
Masaru Nishisako ◽  
Michio Inagaki ◽  
Kazuhide Yamamoto

2003 ◽  
Vol 788 ◽  
Author(s):  
Long Li ◽  
Judith C. Yang

ABSTRACTSilver single crystals (Ag(100), Ag(111)) were exposed to 5eV hyperthermal atomic oxygen, created by a laser detonation of molecular oxygen at a substrate temperature of 220°C for 7 hours. Oxide scales of more than ten microns formed on both Ag (100) and Ag (111) substrates. The microstructural investigation of the oxide layers by high resolution transmission electron microscopy (HRTEM) revealed that the “oxide” scales are predominately composed of nanosized polycrystalline silver grains (5–100nm) as well as a small amount of nanosized silver oxides. The results were remarkably different than the O2 oxidation. The HRTEM investigation suggested that the grains of polycrystalline silver were first carved off from the substrate into “oxide” scale by lattice expansion and decohesion, which are driven by atomic oxygen diffusion in Ag lattice, occupation of oxygen atoms at the interstitial sites of Ag lattice, and partially internal oxidation. The grains in the scale were also subject to continuing oxidations with the atomic oxygen--secondary poly-crystallization, and changed to smaller grains. The preferred oxidation fronts in silver lattice is along the {111} planes.


1994 ◽  
Vol 364 ◽  
Author(s):  
S. Shrivastava ◽  
F. Ebrahimi

AbstractIn the present study, single-edge notched bend specimens of NiAl single crystals were tested in {100}<010>, {101}<101=, and {101}<010} orientations before and after heat-treating the notched specimens at 1000°C for one hour. The fracture toughness data for the non heat-treated specimens were found to be consistent with the previous results. An increase in the fracture toughness of NiAl was observed in all orientations studied upon heat-treating the notched specimens. The toughness ratio for the two orientations obtained from the heat-treated notched specimens was found to be 1.2. This ratio is in agreement with the reported stress analysis considering the crack kinking in {100} oriented specimens. A detailed SEM analysis revealed that the electric discharge machine (EDM) cutting of the notch caused the formation of sharp microcracks at the notch front and also created internal stresses in the vicinity of the notch. The increase in toughness upon heat treatment is attributed to the modification of EDM damage.


The experiments of Obreimow & Schubnikoff (1927) on the birefringence produced by the plastic deformation of single crystals of rock salt have been extended to a polycrystallirie material. Rolled sheets of silver chloride have been recrystallized and then deformed plastically in various ways—by simple extension and by bending, for example. The sheets are transparent and very ductile and, since silver chloride is cubic in structure, the birefringence patterns observed under the microscope provide a picture of the distribution of the internal stresses uncomplicated by natural double refractions. It is suggested that results obtained with this optical method are applicable to metals. Silver chloride appears to deform by glide, and when the glide packets are observed on edge the glide plane and glide direction to the crystal structure has been studied by making observations upon these bands and upon the glide lines formed on the surfaces of bars of square cross-section consisting effectively of chains of single crystals. The orientations of the fifteen sets of glide bands examined in this way were all consistent with glide movements in a <110> direction; the glide plane, however, was not always a crystallographic plane of low indices. In the six cases in which the measurement was possible, it lay within 9° of the plane in the.<110> zone on which the maximum shear stress, resolved in the <110> direction, acted. It is concluded that silver chloride deforms by ‘pencil glide’, the mechanism postulated by Taylor & Elam in 1926 to explain the plastic behaviour of a-iron. The transmission of pencil glide across grain boundaries is discussed. The residual stresses observed by the optical method in polycrystalline sheets may be divided into three groups: (1) A system of stresses set up between the glide zones of each grain and alternating with a period equal to the spacing of the glide zones. A detailed analysis of these is given in the second paper (part II). (2) Alternating stresses produced when a system of glide zones meets a grain boundary. (3) ‘Heyn stresses’ produced by the nonuniformity of plastic deformation from grain to grain.


Sign in / Sign up

Export Citation Format

Share Document