Microstructural Changes by Annealing in Ultrafine-Grained Electrodeposited Pure Iron

2013 ◽  
Vol 45 (2) ◽  
pp. 990-1000 ◽  
Author(s):  
Yuhua Su ◽  
Yo Tomota ◽  
Stefanus Harjo
2011 ◽  
Vol 51 (9) ◽  
pp. 1534-1538 ◽  
Author(s):  
Yuhua Su ◽  
Yo Tomota ◽  
Junichi Suzuki ◽  
Masato Ohnuma
Keyword(s):  

1990 ◽  
Vol 196 ◽  
Author(s):  
Yasunori Saotome ◽  
Nobuhiro Iguchi

ABSTRACTThe microstructural changes associated with phase transformation and the straining behavior in polycrystalline structures during transformational superplastic deformation have betransformatonal superplasticen investigated. In-situ observations have been carried out with specially designed hot-stage microscopes. The strain distribution has been examined by microscopic strain analyses using a micro-grid pattern with 12.7 and 6 μm intervals in pure iron, 0.1%C steel and eutectoid steel. The results are as follows: (1) In the initial stage of Ac3 transformation in pure iron, superplastic strain is induced by the sliding at o/y interface along the prior ferrite grain boundaries and by the grain rotation. In the intermediate stage, the sliding deformation is generated at the migrating tranformation interface associated with the growth of austenite grains. (2) Accumulated strain by sliding has been observed within the previously transformed region during Ac3 transformation in 0.1%C steel. (3) The characteristic straining behavior in the eutectoid steel is due to the behavior at the transformation interface in the microstructure including secondary phase Fe3C particles. These observations suggest that a sliding mechanism at the migrating interface is a principal mechanism of transformation superplasticity.


2020 ◽  
Vol 22 (7) ◽  
pp. 2000183
Author(s):  
Beatriz Araújo Batista ◽  
Renata Braga Soares ◽  
Vanessa de Freitas Cunha Lins ◽  
Roberto Braga Figueiredo ◽  
Anton Hohenwarter ◽  
...  

2020 ◽  
Vol 20 (7) ◽  
pp. 4419-4422
Author(s):  
Seong-Hee Lee

Microstructural changes with annealing of a nanostructured complex aluminum alloy fabricated by 3 cycles of four-layer stack ARB process using different Al alloys were investigated in detail. The four-layer stack ARB process using AA1050, AA5052 and AA6061 alloy sheets was performed up to 3 cycles without a lubricant at room temperature. The sample fabricated by the ARB is a multi-layer aluminum alloy sheet in which the AA1050, AA5052 and AA6061 aluminum alloys are alternately stacked to each other. The layer thickness of each alloy became thinner and elongated to the rolling direction with the number of ARB cycles. The grain size decreased with increasing of the number of ARB cycles, and became about 160 nm in thickness after 3 cycles. The complex Al alloy still showed ultrafine grained microstructure to annealing temperature of 300 °C, but it had a heterogeneous structure containing both the ultrafine grains and the coarse grains due to an occurrence of discontinuous recrystallization after 350 °C.


2013 ◽  
Vol 581 ◽  
pp. 8-15 ◽  
Author(s):  
Jiang-li Ning ◽  
Eglantine Courtois-Manara ◽  
Lilia Kurmanaeva ◽  
Artur V. Ganeev ◽  
Ruslan Z. Valiev ◽  
...  

Metals ◽  
2020 ◽  
Vol 10 (10) ◽  
pp. 1320
Author(s):  
Fumihisa Nagashima ◽  
Yuki Nakagawa ◽  
Masahiko Yoshino

In recent years, ultrafine-grained steel has been gaining increasing attention as a high-performance material. Accordingly, it is necessary to develop an efficient production method for ultrafine-grained steel. Severe plastic deformation is a critical factor that causes grain subdivision into ultrafine grains less than 1 µm in diameter. In this study, the effects of plastic deformation on the microstructure and static recrystallization of pure iron were studied by comparing orthogonal cutting and rolling. Orthogonal cutting yielded ultrafine grains with a diameter of 0.2 µm. It was found that a high strain rate in the thin shear plane generated during the cutting process caused a uniform subdivision of grains, and this uniform plastic deformation resulted in the uniform recrystallization of grains. In addition, a theoretical model was developed, and it was revealed that the number of recrystallized grains depended on the fraction of a large-misorientation area constructed with geometrically necessary boundaries (GNBs). It was suggested that the cutting process was more advantageous than rolling in producing ultrafine recrystallized grains because cutting could apply severe plastic strain uniformly on a work material, effectively generating GNBs.


Author(s):  
Matthias Hockauf ◽  
Lothar W. Meyer ◽  
Thorsten Halle ◽  
Corinna Kuprin ◽  
Michael Hietschold ◽  
...  

2013 ◽  
Vol 48 (13) ◽  
pp. 4620-4625 ◽  
Author(s):  
Zbigniew Oksiuta ◽  
Pawel Kozikowski ◽  
Malgorzata Lewandowska ◽  
Masato Ohnuma ◽  
Koppoju Suresh ◽  
...  

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