Optimization on Tribological Behaviour of Milled Nano-B4C Particles Reinforced with AZ91 Alloy Through Powder Metallurgy Method

2019 ◽  
Vol 72 (5) ◽  
pp. 1255-1275 ◽  
Author(s):  
C. Sankar ◽  
K. Gangatharan ◽  
S. Christopher Ezhil Singh ◽  
R. Krishna Sharma ◽  
K. Mayandi
2020 ◽  
Vol 26 (4) ◽  
pp. 392-400
Author(s):  
Sankar CHINTHAMANI ◽  
Gangatharan KANNAN ◽  
Glan Devadhas GEORGE ◽  
Christopher Ezhil Singh SREEDHARAN ◽  
Krishna Sharma RAJAGOPAL

In this present study, the particle size of as received magnesium alloy (AZ91) and B4C powders was reduced through high energy ball mills. The combination of AZ91 (both 10 µm and 60 µm) reinforced with nano B4C particles were fabricated by powder metallurgy technique. The incorporation of nano B4C particles to the Mg matrix was done at various weight % such as 5, 10, 15 and 20. The AZ91 composites were fabricated in a suitable die set assembly and the green compacts were sintered in an electric muffle furnace at 500 °C with argon atmosphere for a dwell time of 1 h. The density of the composites was estimated using Archimedes principle. Micro hardness test was carried out for the prepared specimens and dry sliding wear test was conducted by using pin-on-disc apparatus at room temperature with varying loads and sliding velocities by keeping a constant Sliding Distance (SD). Among the various specimens, the composite with 10 µm size attained a higher Vickers hardness value as well as better wear resistant property. Worn surface analysis of the prepared composites was studied using Scanning Electron Microscope (SEM).


Author(s):  
J. Alias

Much research on magnesium (Mg) emphasises creating good corrosion resistance of magnesium, due to its high reactivity in most environments. In this study, powder metallurgy (PM) technique is used to produce Mg samples with a variation of aluminium (Al) composition. The effect of aluminium composition on the microstructure development, including the phase analysis was characterised by optical microscope (OM), scanning electron microscopy (SEM) and x-ray diffraction (XRD). The mechanical property of Mg sample was performed through Vickers microhardness. The results showed that the addition of aluminium in the synthesised Mg sample formed distribution of Al-rich phases of Mg17Al12, with 50 wt.% of aluminium content in the Mg sample exhibited larger fraction and distribution of Al-rich phases as compared to the 20 wt.% and 10 wt.% of aluminium content. The microhardness values were also increased at 20 wt.% and 50 wt.% of aluminium content, comparable to the standard microhardness value of the annealed Mg. A similar trend in corrosion resistance of the Mg immersed in 3.5 wt.% NaCl solution was observed. The corrosion behaviour was evaluated based on potentiodynamic polarisation behaviour. The corrosion current density, icorr, is observed to decrease with the increase of Al composition in the Mg sample, corresponding to the increase in corrosion resistance due to the formation of aluminium oxide layer on the Al-rich surface that acted as the corrosion barrier. Overall, the inclusion of aluminium in this study demonstrates the promising development of high corrosion resistant Mg alloys.


2018 ◽  
Vol 280 ◽  
pp. 221-225
Author(s):  
C.D. Zuraidawani ◽  
F.W. Norhadira ◽  
Mochd Nazree B. Derman

The Mg-1wt.%Ca alloy was fabricated using powder metallurgy method. The anodizing process were done by using different voltage (5V, 15V, 25V) and concentration of KOH (0.1M, 0.5M, 1.0M). The surface changes on PM Mg/1wt.%Ca resulted by anodizing was analyzed using SEM-EDX and XRD pattern. Meanwhile, surface hardness was measured by micro-Vickers hardness machine. The experiment found different XRD pattern between all non-anodized and anodized samples. The study found that increasing the voltage will increase the hardness while increasing KOH concentration reduced the hardness. The relation of the hardness and oxide film formation can be analyzed using SEM-EDX and XRD pattern. The optimum value for voltage, KOH concentration and hardness are 25V, 0.1M and 27.2 HV. The XRD detect the changes in PM Mg/1wt.% Ca indicates the oxide film formation.


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