Determination of 2,3,7,8-tetrachlorodibenzo--dioxin (TCDD) in human adipose tissue on whole-weight and lipid bases

Chemosphere ◽  
1987 ◽  
Vol 16 (5) ◽  
pp. 935-936 ◽  
Author(s):  
D.G. Patterson ◽  
J.S. Holler ◽  
W.T. Belser ◽  
E.L. Boozer ◽  
C.R. Lapeza ◽  
...  
1986 ◽  
Vol 69 (3) ◽  
pp. 451-458
Author(s):  
Guy L Lebel ◽  
David T Williams

Abstract <A method has been developed for determination of organochlorine contaminants in human adipose tissue. After fat extraction from the tissue with acetone-hexane (15 + 85, v/v), organochlorines were fractionated from fat by gel permeation chromatography with methylene chloride-cyclohexane (1 + 1, v/v) as solvent. After Florisil column cleanup, the GPC extract was analyzed by capillary column gas chromatography using 2 columns of different polarity. Compound identity was confirmed by gas chromatography-mass spectrometry using selected ion monitoring. Recoveries for fortification levels of 10-500 ng/g were greater than 80 % except for trichlorobenzene and hexachlorobutadiene (ca 60%).


2010 ◽  
Vol 85 (1) ◽  
pp. 97-102 ◽  
Author(s):  
Nebile Daglioglu ◽  
Mete K. Gulmen ◽  
Ramazan Akcan ◽  
Pınar Efeoglu ◽  
Fadile Yener ◽  
...  

1977 ◽  
Vol 11 (4) ◽  
pp. 435-435
Author(s):  
Fredda V Ginsberg-Fellner ◽  
Andrew Davis ◽  
Gary J Bergman ◽  
Jacqueline S Schenkein-Stern ◽  
Jerome L Knittle

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