A study of the compositional homogeneity of an NdFe master alloy, ingot

1992 ◽  
Vol 180 (1-2) ◽  
pp. 77-82
Author(s):  
Zuoshun Li ◽  
Zongan Li ◽  
Guanglu Yang
Metals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 960 ◽  
Author(s):  
Junhui Xiao ◽  
Wei Ding ◽  
Yang Peng ◽  
Tao Chen ◽  
Kai Zou

In this study, preparation of Al–Mg–Sc master alloy tests were carried out by Al–Mg thermoreduction method. Stirring by blowing argon and pressing with molten salt jar were adopted to reduce scandium segregation and upgrading scandium recovery of scandium-bearing master alloy. The results show that the Al–Mg–Sc master alloy ingot contained 2.90% Sc, 5.73% Mg, 0.0058% Cu, 0.29%, 0.029% Ti, 0.13% Fe, 0.075% Zn, 0.025% Na, and 96.72% recovered scandium obtained under the comprehensive conditions used: m(Al): m(Mg): m(ScCl3) = 10:1:1.5, stirring speed of eight rpm, reduction temperature of 1223 K, reduction time of 40 min. The experimental results are in agreement with the thermodynamic predictions, and Al–Mg–Sc master alloy indicator was ideal.


2009 ◽  
Vol 24 (12) ◽  
pp. 3590-3595 ◽  
Author(s):  
Yong Hu ◽  
Jinfu Li ◽  
Tao Lin ◽  
Yaohe Zhou

The effect of repeated melting of master alloy ingots on the bending properties of Zr55Al10Ni5Cu30 bulk metallic glass (BMG) was investigated. The bending plasticity of Zr55Al10Ni5Cu30 BMG was found to be improved with the increased remelting times. When remelted 10 times, the BMG sample cast from the master alloy ingot undergoes bending, but it does not fracture even though the bending angle increases to 100°; the maximum bending stress and elastic strain remain almost constant. The bending plasticity improvement may be attributed to the fact that the increased remelting times result in more free volume and more disorder and homogeneous microstructure in the BMG, which favors the initial nucleation of profuse shear bands and reduces the probability of catastrophic fracture.


Author(s):  
Edgar S. Etz ◽  
Thomas D. Schroeder ◽  
Winnie Wong-Ng

We are investigating by Raman microprobe measurements the superconducting and related phases in the LnBa2Cu3O7-x (for x=0 to 1) system where yttrium has been replaced by several of the lanthanide (Ln = Nd,Sm,Eu,Ho,Er) elements. The aim is to relate the observed optical spectra (Raman and fluorescence) to the compositional and structural properties of these solids as part of comprehensive materials characterization. The results are correlated with the methods of synthesis, the processing techniques of these materials, and their superconducting properties. Of relevance is the substitutional chemistry of these isostructural systems, the differences in the spectra, and their microanalytical usefulness for the detection of impurity phases, and the assessment of compositional homogeneity. The Raman spectra of most of these compounds are well understood from accounts in the literature.The materials examined here are mostly ceramic powders prepared by conventional solid state reaction techniques. The bulk samples are of nominally single-phase composition as determined by x-ray diffraction.


Alloy Digest ◽  
1959 ◽  
Vol 8 (1) ◽  

Abstract APEX 39 is an aluminum die casting alloy ingot containing copper and silicon. It has excellent castability and improved machinability. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties as well as fracture toughness. It also includes information on high temperature performance and corrosion resistance as well as casting and machining. Filing Code: Al-75. Producer or source: Apex Smelting Company.


Author(s):  
Wenxue Fan ◽  
Hai Hao

Abstract Grain refinement has a significant influence on the improvement of mechanical properties of magnesium alloys. In this study, a series of Al–Ti–C-xGd (x = 0, 1, 2, 3) master alloys as grain refiners were prepared by self-propagating high-temperature synthesis. The synthesis mechanism of the Al–Ti–C-xGd master alloy was analyzed. The effects of Al–Ti–C-xGd master alloys on the grain refinement and mechanical properties of AZ31 (Mg-3Al-1Zn-0.4Mn) magnesium alloys were investigated. The results show that the microstructure of the Al–Ti–C-xGd alloy contains α-Al, TiAl3, TiC and the core–shell structure TiAl3/Ti2Al20Gd. The refining effect of the prepared Al–Ti–C–Gd master alloy is obviously better than that of Al–Ti–C master alloy. The grain size of AZ31 magnesium alloy was reduced from 323 μm to 72 μm when adding 1 wt.% Al–Ti–C-2Gd master alloy. In the same condition, the ultimate tensile strength and elongation of as-cast alloy were increased from 130 MPa, 7.9% to 207 MPa, 16.6% respectively.


Author(s):  
Jiawei Yang ◽  
Sarina Bao ◽  
Shahid Akhtar ◽  
Yanjun Li

AbstractIn this work, a systematic study on the interactions between aluminum oxide films and TiB2 grain refiner particles and their effect on grain refinement behavior have been conducted. Oxide films were introduced into a commercial purity aluminum melt by adding AA 6061 alloy chips while the grain refiner particles were introduced by adding Al-3T-1B master alloy. Strong sedimentation of TiB2 grain refiner particles was observed in aluminum melt without chip addition during long-time settling. Most of the TiB2 particles were settled and accumulated at the bottom of crucible. In contrast, the sedimentation of TiB2 particles is much less in the melt with the addition of oxide films. A large fraction of TiB2 particles were found to be adhered to the oxide films located at the top part of the crucible, which inhibited the sedimentation of grain refiner particles. TP-1 type tests were also done to study the grain refinement efficiency of Al-3Ti-1B master alloy under different melt cleanliness and settling time. It is found that sedimentation of TiB2 particles greatly reduces the grain refinement efficiency. The introduction of oxide films seems to slightly alleviate the fading effect. This is owing to the strong adherence between the oxide films and TiB2 particles, which leads to a retardation of particle sedimentation.


2020 ◽  
Vol 29 (10) ◽  
pp. 6840-6848 ◽  
Author(s):  
Xudong Liu ◽  
Qingfeng Zhu ◽  
Tao Jia ◽  
Zhihao Zhao ◽  
Jianzhong Cui ◽  
...  

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