Nanocrystalline structure of non-equilibrium FeCu alloys obtained by severe plastic deformation under pressure

1995 ◽  
Vol 6 (1-4) ◽  
pp. 437-440 ◽  
Author(s):  
V.A. Teplov ◽  
V.P. Pilugin ◽  
V.S. Gaviko ◽  
E.G. Chernyshov
2011 ◽  
Vol 312-315 ◽  
pp. 1116-1125
Author(s):  
Vladimir V. Popov

Recent models of grain-boundary diffusion are briefly reviewed. Models of diffusion along equilibrium boundaries of recrystallization origin in coarse-grained materials and along non-equilibrium boundaries in nanocrystalline materials obtained by gas condensation and compacting or by severe plastic deformation are considered separately.


2006 ◽  
Vol 977 ◽  
Author(s):  
Xavier Sauvage ◽  
Xavier Quelennec ◽  
Peter Jessner ◽  
Florian Wetscher ◽  
Reinhard Pippan

AbstractGrain size reduction induced by severe plastic deformation (SPD) and the resulting mechanical properties have been widely investigated for pure metals but less is known and reported about multi-phase materials. To study the grain size reduction mechanisms in multiphase structure subjected to SPD, two copper based composites (Cu-10%Fe and Cu-43%Cr) were severely deformed by torsion under high pressure. The grain size achieved with these composite materials is much smaller than in pure metals. It is for example in a range of 10 to 20 nm for the Cu-43%Cr composite, e.g. one order of magnitude lower than in pure Cu processed by SPD. Three dimensional atom probe data show also the formation of non equilibrium supersaturated solid solutions. The mechanisms of the deformation induced intermixing are discussed together with its influence on the mechanical properties.


2007 ◽  
Vol 539-543 ◽  
pp. 2787-2792 ◽  
Author(s):  
Minoru Umemoto ◽  
Yoshikazu Todaka ◽  
Jin Guo Li ◽  
Koichi Tsuchiya

Formation of nanocrystalline structure by severe plastic deformation has studied extensively. Although ultra fine grained structure (grain size larger than 100 nm) had been obtained in many processes such as heavy cold rolling, equal channel angular pressing (ECAP) or accumulative roll bonding (ARB), the formation of nano grained structure (< 100 nm) is limited to processes such as ball milling, shot peening or drilling. In the present study, high pressure torsion (HPT) deformation and drilling were carried out to understand the conditions necessary to obtain nano grained structure in steels. The results of HPT experiments in pure Fe showed that HPT has superior ability of strengthening and grain refinement probably due to a strain gradient but the saturation of grain refinement occurs before reaching nano grained structure. Drilling experiments in high carbon martensitic steel revelaed that nano grained ferrite forms at the drilled hole surface only when the transformation from ferrite to austenite takes place during drilling. Considering various other processes by which nano grained ferrite was produced, it is proposed that heavy strains with large strain gradients together with dynamic transformation are necessary to reach nano grained ferrite structure.


2006 ◽  
Vol 2006 (6) ◽  
pp. 533-540 ◽  
Author(s):  
S. V. Dobatkin ◽  
V. V. Zakharov ◽  
A. Yu. Vinogradov ◽  
K. Kitagawa ◽  
N. A. Krasil’nikov ◽  
...  

2010 ◽  
Vol 297-301 ◽  
pp. 1312-1321 ◽  
Author(s):  
Vladimir V. Popov ◽  
A.V. Stolbovkiy ◽  
E.N. Popova ◽  
V.P. Pilyugin

Evolution of structure of high-purity and commercially pure copper at severe plastic deformation (SPD) by high pressure torsion (HPT) at room temperature and in liquid nitrogen has been studied by transmission electron microscopy (TEM) and measurements of microhardness. Thermal stability of structure obtained by HPT has been investigated. Factors preventing from obtaining nanocrystalline structure in Cu are analyzed and possible ways of their overcoming are discussed.


2019 ◽  
Vol 11 (11) ◽  
pp. 1489-1501
Author(s):  
Wenjing He ◽  
Caihe Fan ◽  
Shu Wang ◽  
Junhong Wang ◽  
Su Chen ◽  
...  

The evolution of nanoprecipitated phases in Al–Cu alloys under severe plastic deformation (SPD) is summarized in this study. SPD at room temperature induces the precipitation of Al–Cu alloys to dissolve, leading to the reformation of supersaturated solid solution in the aluminum matrix. In the process of SPD or aging treatment after the SPD, the reprecipitated phases are precipitated from the aluminum matrix and the mechanical properties of the alloys are remarkably improved. The mechanism and system of the redissolution of the precipitation phases and the effects of redissolution and reprecipitation on the microstructure and properties of Al–Cu alloys are comprehensively analyzed. The development and future of redissolution and reprecipitation of nanoprecipitated phases in Al–Cu alloys are also described.


2016 ◽  
Vol 367 ◽  
pp. 130-139 ◽  
Author(s):  
Vladimir V. Popov ◽  
A.V. Sergeev

The grain-boundary diffusion of Co in ultra-fine grained Mo processed by high-pressure torsion has been studied by emission Mössbauer spectroscopy and radio-tracer analysis. It is demonstrated that under the severe plastic deformation by high-pressure torsion the non-equilibrium grain boundaries are formed which are the ultra-fast diffusion paths. At annealing in the temperature range of 623-823 K the relaxation of the non-equilibrium boundaries proceeds and their properties approach to those of equilibrium boundaries of recrystallization origin.


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