Complete columnar-to-equiaxed transition and significant grain refinement in an aluminium alloy by adding Nb particles through laser powder bed fusion

2022 ◽  
pp. 102615
Author(s):  
Zhichao Wang ◽  
Xintian Wang ◽  
Xu Chen ◽  
Chunlei Qiu
2021 ◽  
Vol 1016 ◽  
pp. 580-586
Author(s):  
Hideaki Ikehata ◽  
Eric Jägle

Grain refinement tendency of pure Fe and Fe-X (X=5~10at%Al, 2~10at%Ti) alloys produced by laser powder bed fusion (LPBF) process was investigated. Pure Fe, Al, and Ti powders were dry mixed and cubic samples were built from the mixtures. The microstructure analysis revealed that (1) the microstructure of pure Fe consisted of equiaxed grains having an average diameter of 1.7 μm with fine iron oxide particles. (2) Fe-5 and 10at%Al alloys showed coarse columnar grains. (3) Fe-2at%Ti shows a mixture of fine equiaxed and columnar shape grains. (4) the microstructures of Fe-5at%Ti and 10at%Ti alloys are fully equiaxed, and grain refinement tendency was confirmed with increasing Ti content. Ti(N,O) oxi-nitrides are efficient in reducing the grain size because of the low lattice misfit with the ferrite matrix. Additionally, the effectiveness of Ti(N,O) particles as grain refiners was confirmed by building samples using TiN powder mixed with Fe-10at%Al and Fe-2at%Ti. While these alloys alone are coarse grained, a dispersion of Ti(N,O) particles achieved a fine-grained microstructure.


2020 ◽  
Vol 196 ◽  
pp. 109181
Author(s):  
Hossein Eskandari Sabzi ◽  
Nesma T. Aboulkhair ◽  
Xingzhong Liang ◽  
Xiao-Hui Li ◽  
Marco Simonelli ◽  
...  

Materialia ◽  
2021 ◽  
pp. 101160
Author(s):  
Maxence BUTTARD ◽  
Béchir CHEHAB ◽  
Ravi SHAHANI ◽  
Florence ROBAUT ◽  
Gilles RENOU ◽  
...  

2019 ◽  
Vol 116 ◽  
pp. 83-91 ◽  
Author(s):  
Ali Keshavarzkermani ◽  
Ehsan Marzbanrad ◽  
Reza Esmaeilizadeh ◽  
Yahya Mahmoodkhani ◽  
Usman Ali ◽  
...  

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
P. Van Cauwenbergh ◽  
V. Samaee ◽  
L. Thijs ◽  
J. Nejezchlebová ◽  
P. Sedlák ◽  
...  

AbstractTailoring heat treatments for Laser Powder Bed Fusion (LPBF) processed materials is critical to ensure superior and repeatable material properties for high-end applications. This tailoring requires in-depth understanding of the LPBF-processed material. Therefore, the current study aims at unravelling the threefold interrelationship between the process (LPBF and heat treatment), the microstructure at different scales (macro-, meso-, micro-, and nano-scale), and the macroscopic material properties of AlSi10Mg. A similar solidification trajectory applies at different length scales when comparing the solidification of AlSi10Mg, ranging from mould-casting to rapid solidification (LPBF). The similarity in solidification trajectories triggers the reason why the Brody-Flemings cellular microsegregation solidification model could predict the cellular morphology of the LPBF as-printed microstructure. Where rapid solidification occurs at a much finer scale, the LPBF microstructure exhibits a significant grain refinement and a high degree of silicon (Si) supersaturation. This study has identified the grain refinement and Si supersaturation as critical assets of the as-printed microstructure, playing a vital role in achieving superior mechanical and thermal properties during heat treatment. Next, an electrical conductivity model could accurately predict the Si solute concentration in LPBF-processed and heat-treated AlSi10Mg and allows understanding the microstructural evolution during heat treatment. The LPBF-processed and heat-treated AlSi10Mg conditions (as-built (AB), direct-aged (DA), stress-relieved (SR), preheated (PH)) show an interesting range of superior mechanical properties (tensile strength: 300–450 MPa, elongation: 4–13%) compared to the mould-cast T6 reference condition.


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