Room temperature solution-phase synthesis of flower-like nanostructures of [Ni3(BTC)2·12H2O] and their conversion to porous NiO

2013 ◽  
Vol 24 (8) ◽  
pp. 663-667 ◽  
Author(s):  
Li-Na Jin ◽  
Qing Liu ◽  
Wei-Yin Sun
Keyword(s):  
Room Temperature ◽  
Solution Phase ◽  
Phase Synthesis ◽  
Solution Phase Synthesis ◽  
Temperature Solution

Facile room-temperature solution-phase synthesis of a spherical covalent organic framework for high-resolution chromatographic separation

2015 ◽  
Vol 51 (61) ◽  
pp. 12254-12257 ◽  
Author(s):  
Cheng-Xiong Yang ◽  
Chang Liu ◽  
Yi-Meng Cao ◽  
Xiu-Ping Yan
Keyword(s):  
High Resolution ◽  
Surface Area ◽  
Chromatographic Separation ◽  
Room Temperature ◽  
Solution Phase ◽  
Phase Synthesis ◽  
Covalent Organic Framework ◽  
Solution Phase Synthesis ◽  
Temperature Solution ◽  
Organic Framework

Facile room-temperature solution-phase synthesis of a spherical covalent organic framework with large surface area and good stability for high-resolution chromatographic separation.

Template-free room temperature solution phase synthesis of Cu2O hollow spheres

CrystEngComm ◽  
2010 ◽  
Vol 12 (3) ◽  
pp. 700-701 ◽  
Author(s):  
Wenzhong Wang ◽  
Pengcheng Zhang ◽  
Lei Peng ◽  
Wenjuan Xie ◽  
Guling Zhang ◽  
...  
Keyword(s):  
Room Temperature ◽  
Hollow Spheres ◽  
Solution Phase ◽  
Phase Synthesis ◽  
Solution Phase Synthesis ◽  
Temperature Solution ◽  
Template Free

Solution-phase synthesis of monodispersed SnTe nanocrystallites at room temperature

2003 ◽  
Vol 6 (2) ◽  
pp. 181-184 ◽  
Author(s):  
Changhua An ◽  
Kaibin Tang ◽  
Bin Hai ◽  
Guozhen Shen ◽  
Chunrui Wang ◽  
...  
Keyword(s):  
Room Temperature ◽  
Solution Phase ◽  
Phase Synthesis ◽  
Solution Phase Synthesis

A general and rapid room-temperature synthesis approach for metal sulphide nanocrystals with tunable properties

Nanoscale ◽  
2019 ◽  
Vol 11 (1) ◽  
pp. 136-144 ◽  
Author(s):  
Yang Liu ◽  
Maixian Liu ◽  
Deqiang Yin ◽  
Dewei Zhu ◽  
Mark T. Swihart
Keyword(s):  
Room Temperature ◽  
Solution Phase ◽  
High Quality ◽  
Temperature Synthesis ◽  
Phase Synthesis ◽  
Metal Sulphide ◽  
Room Temperature Synthesis ◽  
Tunable Properties ◽  
Solution Phase Synthesis ◽  
Synthesis Approach

A rapid, room-temperature, and solution-phase synthesis produces high-quality, monodisperse metal sulphide nanocrystals with tunable properties.

Advances in nanoscale alloys and intermetallics: low temperature solution chemistry synthesis and application in catalysis

2015 ◽  
Vol 44 (43) ◽  
pp. 18692-18717 ◽  
Author(s):  
Subhra Jana
Keyword(s):  
Low Temperature ◽  
Solution Chemistry ◽  
Solution Phase ◽  
Phase Synthesis ◽  
Size And Shape ◽  
Solution Phase Synthesis ◽  
Temperature Solution ◽  
Made In

Advances made in the synthesis of size and shape-tunable nanoscale alloys and intermetallics using the low-temperature solution-phase synthesis approaches have been discussed in this perspective, keeping a focus on the utility of these nanomaterials in understanding the catalysis.

A Low Temperature, Solution Phase Synthesis of III-V Semiconductor Nanocrystals

1994 ◽  
Vol 351 ◽  
Author(s):  
Shreyas S. Kher ◽  
Richard L. Wells
Keyword(s):  
Semiconductor Nanocrystals ◽  
Solution Phase ◽  
High Yield ◽  
Group V ◽  
Phase Synthesis ◽  
Group Iii ◽  
Wide Range ◽  
Solution Phase Synthesis ◽  
Temperature Solution ◽  
High Yields

ABSTRACTNanocrystalline materials have been intensely investigated in the recent past due to the novel properties associated with size-quantized particles. We have developed a new method for high yield, solution phase synthesis of nanocrystalline III-V semiconductors which eliminates the use of substituted or unsubstituted Group V hydrides and Group III alkyls. Our approach consists of in situ syntheses of (Na/K)3E (E = P, As, Sb) in aromatic solvents and subsequent reactions of these pnictides with Group III halide solutions in coordinating solvents. The nanocrystalline III-V semiconductors GaP, GaAs, GaSb, InP, InAs and InSb are readily prepared in a wide range of particle sizes (4–36 nm) and in high yields. The resultant Ill-V materials have been characterized by XRD, EDXA, TEM and elemental analyses.

Solvent-Dependent, Low-Temperature Solution Phase Synthesis of FePt Nanowires

2008 ◽  
Vol 8 (7) ◽  
pp. 3379-3385 ◽  
Author(s):  
Kai-Ming Chi ◽  
Pei-Yu Chen
Keyword(s):  
Thermal Decomposition ◽  
Low Temperature ◽  
Reaction Temperature ◽  
Average Diameter ◽  
Solution Phase ◽  
Synthetic Approach ◽  
Phase Synthesis ◽  
Solution Phase Synthesis ◽  
Temperature Solution

Preparation of FePt nanowires by thermal decomposition of the solution mixture of equimolar Fe(CO)5 and Pt(acac)2 in n-octylamine will be presented in this account. The nanowires with the average diameter about 2 nm and the length of several hundred nanometers were characterized by TEM, EDS, XRD. It is believed that FePt nanowires were generated via the catalytic solution-liquid-solid (S-L-S) synthetic approach. This process is strongly dependent on the solvent and barely on the reaction temperature and the concentrations of precursors.

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