Segmented flow synthesis of Ag nanoparticles in spiral microreactor: Role of continuous and dispersed phase

2012 ◽  
Vol 192 ◽  
pp. 357-368 ◽  
Author(s):  
D.V. Ravi Kumar ◽  
B.L.V. Prasad ◽  
A.A. Kulkarni
RSC Advances ◽  
2015 ◽  
Vol 5 (61) ◽  
pp. 49671-49679 ◽  
Author(s):  
Prem. C. Pandey ◽  
Richa Singh ◽  
Yashashwa Pandey

A facile method for the synthesis of functional AgNPs and bimetallic Ag–Au/Au–Ag are reported, enabling the formation of nanocomposite with prussian blue in a crystalline framework for bioanalytical applications, showing the active role of organic reducing agents and 3-aminopropyltrimethoxysilane.


2016 ◽  
Vol 6 (1) ◽  
Author(s):  
Kaijun Zhou ◽  
Yi Hu ◽  
Luqing Zhang ◽  
Kun Yang ◽  
Daohui Lin

Polymer ◽  
1997 ◽  
Vol 38 (1) ◽  
pp. 21-30 ◽  
Author(s):  
Julie Y. Qian ◽  
Raymond A. Pearson ◽  
Victoria L. Dimonie ◽  
Olga L. Shaffer ◽  
Mohamed S. El-Aasser

2017 ◽  
Vol 13 ◽  
pp. 960-987 ◽  
Author(s):  
Chinmay A Shukla ◽  
Amol A Kulkarni

The implementation of automation in the multistep flow synthesis is essential for transforming laboratory-scale chemistry into a reliable industrial process. In this review, we briefly introduce the role of automation based on its application in synthesis viz. auto sampling and inline monitoring, optimization and process control. Subsequently, we have critically reviewed a few multistep flow synthesis and suggested a possible control strategy to be implemented so that it helps to reliably transfer the laboratory-scale synthesis strategy to a pilot scale at its optimum conditions. Due to the vast literature in multistep synthesis, we have classified the literature and have identified the case studies based on few criteria viz. type of reaction, heating methods, processes involving in-line separation units, telescopic synthesis, processes involving in-line quenching and process with the smallest time scale of operation. This classification will cover the broader range in the multistep synthesis literature.


Soft Matter ◽  
2021 ◽  
Author(s):  
Junsu Chae ◽  
Siyoung Choi ◽  
KyuHan Kim

A high internal phase emulsion (HIPE), which has a volume fraction of dispersed phase of over 74%, shows a solid like property because of concentrated polyhedral droplets. Although many studies...


2020 ◽  
Vol 4 (3) ◽  
pp. 38
Author(s):  
Giuseppe Cinelli ◽  
Martina Cofelice ◽  
Francesco Venditti

This review traces the current knowledge on the effects of various factors and phenomena that occur at interface, and the role of dispersed phase on the physicochemical, sensorial and nutritional characteristics of veiled extra virgin olive oil (VVOO). Since 1994 there have been numerous articles in the literature regarding the peculiar characteristic of unfiltered olive oil, so-called veiled or cloud virgin olive oil. It is a colloidal system (emulsion–sol), where the continuous lipidic phase dispreads mini droplets of milling water, fragments of cells and biotic fraction obtained from oil processing. During storage, the dispersed phase collapses and determines the quality of the virgin olive oil (VOO). The observed phenomena lead to worsening the quality of the product by causing defects such as oxidation of phenols, triacylglycerols hydrolysis and off-flavor formation. The addition of bioactive compounds, such as vitamins, on product based on VVOO, must take into account the eventual synergistic effect of individual substances. The role of the interphase is crucial to the synergic activity of bioactive molecules in improving oxidative stability, sensorial and health characteristics of VVOO.


2021 ◽  
Vol 50 (1) ◽  
pp. 208-216
Author(s):  
Mengnan Yang ◽  
Zhaoli Yan ◽  
Tiantian Li ◽  
Bing Liu ◽  
Qiangshan Jing ◽  
...  

Negatively charged surface hydroxyls and micropores of Janus silica nanosheets play a particular role in the highly efficient and dispersed assembly of ultra-small Ag nanoparticles with high catalytic activity.


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