Reassessment of mercury intrusion porosimetry for characterizing the pore structure of cement-based porous materials by monitoring the mercury entrapments with X-ray computed tomography

2020 ◽  
Vol 113 ◽  
pp. 103726
Author(s):  
Qiang Zeng ◽  
Shan Chen ◽  
Pengcheng Yang ◽  
Yu Peng ◽  
Jiyang Wang ◽  
...  
Materials ◽  
2019 ◽  
Vol 12 (14) ◽  
pp. 2220 ◽  
Author(s):  
Xiaohu Wang ◽  
Yu Peng ◽  
Jiyang Wang ◽  
Qiang Zeng

Mercury intrusion porosimetry (MIP) is questioned for possibly damaging the micro structure of cement-based materials (CBMs), but this theme still has a lack of quantitative evidence. By using X-ray computed tomography (XCT), this study reported an experimental investigation on probing the pore structure damages in paste and mortar samples after a standard MIP test. XCT scans were performed on the samples before and after mercury intrusion. Because of its very high mass attenuation coefficient, mercury can greatly enhance the contrast of XCT images, paving a path to probe the same pores with and without mercury fillings. The paste and mortar showed the different MIP pore size distributions but similar intrusion processes. A grey value inverse for the pores and material skeletons before and after MIP was found. With the features of excellent data reliability and robustness verified by a threshold analysis, the XCT results characterized the surface structure of voids, and diagnosed the pore structure damages in terms of pore volume and size of the paste and mortar samples. The findings of this study deepen the understandings in pore structure damages in CBMs by mercury intrusion, and provide methodological insights in the microstructure characterization of CBMs by XCT.


2015 ◽  
Vol 52 (10) ◽  
pp. 1448-1456 ◽  
Author(s):  
Akira Sato ◽  
Koichi Ikeda

The migration of water and contamination materials in rock structures is a significant issue in projects that utilize deep underground locations such as “carbon-dioxide capture and storage” (CCS) and disposal of high-level nuclear waste. These phenomena are also important in the area of preservation of stone structures of cultural heritage signficance, as such stone structures are usually located outside, exposed to wind and rain. The migration of contamination materials in the underground environment, especially in porous rock mass, is governed mainly by water permeation and diffusion. In this study, one-dimensional diffusion testing was conducted and the process in the porous materials was visualized by X-ray computed tomography (CT) scanning. Diffusion is the process caused by the concentrate or density gradient, and is a suitable phenomenon for X-ray CT analysis. In this paper, information related to diffusion is extracted from X-ray CT image data and the distribution of concentration is estimated. From the obtained density distribution, diffusion coefficients are evaluated. One-dimensional permeation tests were also conducted and intrinsic permeabilities of porous materials are evaluated, then the relation between diffusion coefficients and intrinsic permeability is discussed.


◽  
2016 ◽  
Author(s):  
Katsufumi Hashimoto ◽  
◽  
Hiroshi Yokota ◽  
Takafumi Sugiyama ◽  
◽  
...  

BioResources ◽  
2020 ◽  
Vol 15 (2) ◽  
pp. 3053-3063
Author(s):  
Liangyan Guo ◽  
Hongchao Cheng ◽  
Junfeng Chen ◽  
Wentao Chen ◽  
Jingyao Zhao

The microscopic pore structure of wood is an important factor that affects its macroscopic properties. In this study, an oak sample was used for pore structure characterization. X-ray computed tomography imaging was carried out, and the scanning results (a multi-layer two-dimensional planar image) were rendered using Avizo software (a three-dimensional stereo image). A digital image processing method was used to identify the characteristics of the three-dimensional pore structure features and to calculate the characteristic parameters, i.e., the porosity (volume/surface), pore area and volume, pore size distribution, and the connectivity. The 27 mm3 oak sample had the following characteristics: a pore size which ranged from 8.56 µm to 1262.84 µm; a pore volume of 1.01 × 1010 µm3; a pore area and volume porosity of 1.12 × 109 µm2 and 37.6%, respectively; a surface porosity range of approximately 36.1% to 39.1%; a pore diameter for axial connection ranging from approximately 164.57 µm to 1262.84 µm; and had corresponding proportions of the pore area and volume of approximately 74.4% and 67.3%, respectively. This information provided useful structural data for the construction of future models.


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