High efficiency adsorption of uranium in solution with magnesium oxide embedded horse manure-derived biochar

2021 ◽  
Vol 9 (6) ◽  
pp. 106897
Author(s):  
Bowen Zheng ◽  
Jun Liao ◽  
Ling Ding ◽  
Yong Zhang ◽  
Wenkun Zhu
2020 ◽  
Vol 27 (13) ◽  
pp. 15463-15474
Author(s):  
Shuaishuai Li ◽  
Wei Zeng ◽  
Huanhuan Xu ◽  
Ziyue Jia ◽  
Yongzhen Peng

2014 ◽  
Vol 878 ◽  
pp. 185-193 ◽  
Author(s):  
Huai Li ◽  
Jian Zheng Li ◽  
Zi Fang Chi

Leather processing is an important industry in China, and the discharge of chromium waste has been severely circumscribed. Though traditional processes for treating chromium waste have been widely used in tannery plants, technology adopting high efficiency and economic simultaneously is deficient. In order to develop an economic treatment for tannery waste, a mixed alkali of sodium hydroxide and magnesium oxide and diluted mineral acids were tested to improve the sedimentation effect of trivalent chromium from tannery wastewater. The results showed that the most feasible alkali was a mixture of sodium hydroxide and magnesium oxide with a mass ratio of 5:1 to balance the cost performance. The high chromium removal as 99.1% was obtained with a mixed alkali dosage only 0.2 g/L at pH 9.5, with a very low Cr-sludge yield. The effects of various factors on the extraction of trivalent chromium from Cr-sludge using mineral acids were investigated further more, and the results indicated that the feasible condition for chromium recovery from wet chromium sludge was as follows: 4% sulfuric acid as the leaching acid, chromium sludge (dry weight) load 23.55 g/L, extraction time 60 min, and reaction temperature 30°C. A chromium recovery of 20.86 mg/g was obtained under the feasible condition with a recovery rate of 91.8%. The method developed in the present study provided an effective solution to balance the cost performance for tannery waste treatment.


Author(s):  
Yuqing Lei ◽  
Keding Li ◽  
Jun Liao ◽  
Yong Zhang ◽  
Lin Zhang ◽  
...  

3D alumina-doped magnesium oxide (Al2O3/MgO) aerogels with remarkable adsorption properties for U(vi) were prepared via a simple lyophilization–calcination method.


1988 ◽  
Vol 102 ◽  
pp. 41
Author(s):  
E. Silver ◽  
C. Hailey ◽  
S. Labov ◽  
N. Madden ◽  
D. Landis ◽  
...  

The merits of microcalorimetry below 1°K for high resolution spectroscopy has become widely recognized on theoretical grounds. By combining the high efficiency, broadband spectral sensitivity of traditional photoelectric detectors with the high resolution capabilities characteristic of dispersive spectrometers, the microcalorimeter could potentially revolutionize spectroscopic measurements of astrophysical and laboratory plasmas. In actuality, however, the performance of prototype instruments has fallen short of theoretical predictions and practical detectors are still unavailable for use as laboratory and space-based instruments. These issues are currently being addressed by the new collaborative initiative between LLNL, LBL, U.C.I., U.C.B., and U.C.D.. Microcalorimeters of various types are being developed and tested at temperatures of 1.4, 0.3, and 0.1°K. These include monolithic devices made from NTD Germanium and composite configurations using sapphire substrates with temperature sensors fabricated from NTD Germanium, evaporative films of Germanium-Gold alloy, or material with superconducting transition edges. A new approache to low noise pulse counting electronics has been developed that allows the ultimate speed of the device to be determined solely by the detector thermal response and geometry. Our laboratory studies of the thermal and resistive properties of these and other candidate materials should enable us to characterize the pulse shape and subsequently predict the ultimate performance. We are building a compact adiabatic demagnetization refrigerator for conveniently reaching 0.1°K in the laboratory and for use in future satellite-borne missions. A description of this instrument together with results from our most recent experiments will be presented.


Author(s):  
P. L. Burnett ◽  
W. R. Mitchell ◽  
C. L. Houck

Natural Brucite (Mg(OH)2) decomposes on heating to form magnesium oxide (MgO) having its cubic ﹛110﹜ and ﹛111﹜ planes respectively parallel to the prism and basal planes of the hexagonal brucite lattice. Although the crystal-lographic relation between the parent brucite crystal and the resulting mag-nesium oxide crystallites is well known, the exact mechanism by which the reaction proceeds is still a matter of controversy. Goodman described the decomposition as an initial shrinkage in the brucite basal plane allowing magnesium ions to shift their original sites to the required magnesium oxide positions followed by a collapse of the planes along the original <0001> direction of the brucite crystal. He noted that the (110) diffraction spots of brucite immediately shifted to the positions required for the (220) reflections of magnesium oxide. Gordon observed separate diffraction spots for the (110) brucite and (220) magnesium oxide planes. The positions of the (110) and (100) brucite never changed but only diminished in intensity while the (220) planes of magnesium shifted from a value larger than the listed ASTM d spacing to the predicted value as the decomposition progressed.


Author(s):  
J. M. Cowley ◽  
R. Glaisher ◽  
J. A. Lin ◽  
H.-J. Ou

Some of the most important applications of STEM depend on the variety of imaging and diffraction made possible by the versatility of the detector system and the serial nature, of the image acquisition. A special detector system, previously described, has been added to our STEM instrument to allow us to take full advantage of this versatility. In this, the diffraction pattern in the detector plane may be formed on either of two phosphor screens, one with P47 (very fast) phosphor and the other with P20 (high efficiency) phosphor. The light from the phosphor is conveyed through a fiber-optic rod to an image intensifier and TV system and may be photographed, recorded on videotape, or stored digitally on a frame store. The P47 screen has a hole through it to allow electrons to enter a Gatan EELS spectrometer. Recently a modified SEM detector has been added so that high resolution (10Å) imaging with secondary electrons may be used in conjunction with other modes.


Author(s):  
K.M. Hones ◽  
P. Sheldon ◽  
B.G. Yacobi ◽  
A. Mason

There is increasing interest in growing epitaxial GaAs on Si substrates. Such a device structure would allow low-cost substrates to be used for high-efficiency cascade- junction solar cells. However, high-defect densities may result from the large lattice mismatch (∼4%) between the GaAs epilayer and the silicon substrate. These defects can act as nonradiative recombination centers that can degrade the optical and electrical properties of the epitaxially grown GaAs. For this reason, it is important to optimize epilayer growth conditions in order to minimize resulting dislocation densities. The purpose of this paper is to provide an indication of the quality of the epitaxially grown GaAs layers by using transmission electron microscopy (TEM) to examine dislocation type and density as a function of various growth conditions. In this study an intermediate Ge layer was used to avoid nucleation difficulties observed for GaAs growth directly on Si substrates. GaAs/Ge epilayers were grown by molecular beam epitaxy (MBE) on Si substrates in a manner similar to that described previously.


Author(s):  
T. Kizuka ◽  
N. Tanaka

Structure and stability of atomic clusters have been studied by time-resolved high-resolution electron microscopy (TRHREM). Typical examples are observations of structural fluctuation in gold (Au) clusters supported on silicon oxide films, graphtized carbon films and magnesium oxide (MgO) films. All the observations have been performed on the clusters consisted of single metal element. Structural stability of ceramics clusters, such as metal-oxide, metal-nitride and metal-carbide clusters, has not been observed by TRHREM although the clusters show anomalous structural and functional properties concerning to solid state physics and materials science.In the present study, the behavior of ceramic, magnesium oxide (MgO) clusters is for the first time observed by TRHREM at 1/60 s time resolution and at atomic resolution down to 0.2 nm.MgO and gold were subsequently deposited on sodium chloride (001) substrates. The specimens, single crystalline MgO films on which Au particles were dispersed were separated in distilled water and observed by using a 200-kV high-resolution electron microscope (JEOL, JEM2010) equipped with a high sensitive TV camera and a video tape recorder system.


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