The influence of large second phase grains on microstructural evolution during diffusion creep

2021 ◽  
pp. 104371
Author(s):  
Joe Gardner ◽  
John Wheeler
2020 ◽  
Vol 24 ◽  
pp. 100956
Author(s):  
Fan Zhang ◽  
Yafei Wang ◽  
Yunbiao Duan ◽  
Kaijun Wang ◽  
Yutian Wang ◽  
...  

2013 ◽  
Vol 54 (1) ◽  
pp. 57-62 ◽  
Author(s):  
F. Xu ◽  
Y Niu ◽  
X.-F. Hu ◽  
Y.-C. Li ◽  
H.-Y. Qu ◽  
...  

2011 ◽  
Vol 217-218 ◽  
pp. 1123-1128
Author(s):  
Jun Wei Liu ◽  
Shi Qiang Lu ◽  
Xian Juan Dong ◽  
Xuan Xiao

The microstructural evolution and mechanical properties of as cast AZ91 Mg alloy enduring different homogenization conditions were researched. The results show that the peak stress and plasticity obtain improvement with the increase of heat treated time and temperature until 693K. When the temperature is higher than 743K, the sample will occur the over-burned and directly lead to the decrease of mechanical properties. Otherwise, with the increase of heat treated time and temperatures, the second phase gradually precipitate from the solution, while the grain evolution is not obvious. In the compression process for the samples after heat treatment, some twins could be found in the grains.


2016 ◽  
Vol 853 ◽  
pp. 153-157
Author(s):  
Zhi Gang Xie ◽  
Yan Ming He ◽  
Jian Guo Yang ◽  
Zeng Liang Gao

The A508-III steel is widely used to manufacture the lower heads of commercial reactor pressure vessels (RPV). In severe accident, the reactor core in the RPV begins to melt and meanwhile the technology of in-vessel retention (IVR) exerts its role. In this case the inner surface of RPV will expose to temperatures over a phase transition temperature. However, the significant nonlinear feature of creep curve of A508-III steel suffered heterogeneous damage was not studied. In this work, the creep tests were performed for the steel at the phase transition temperature of 800°C. The microstructural evolution at different creep stages was characterized by scanning electron microscopy and transmission electron microscopy. The results show that, at the second creep stage, more coarsening second phase particles occur in the steel. With the creep processing, the grain size and diameter of second phase particles increase. At the tertiary creep stage, the grain size increases significantly, and the second phase particles coarsen during the process of atom migration. In addition, Micro-cracks and voids also come into being in the situation and they can become larger by combing each other during the creep process. At this stage, the growth of cavities and second phase particles coarsening become the main mechanism of creep damage. The trend of microstructural evolution is consistent with the creep constitutive equation obtained for the A508-III steel at the phase transition temperature of 800°C. The results obtained provide indispensable foundation to establish the relationship between the macroscopic creep and microscopic damage.


2011 ◽  
Vol 409 ◽  
pp. 362-367 ◽  
Author(s):  
M. Paliwal ◽  
Dae H. Kang ◽  
Elhachmi Essadiqi ◽  
In Ho Jung

Although numerous solidification experiments have been conducted for Al, Cu and Si alloys to investigate microstructural features like primary and secondary dendrite arm spacing, solute distribution with in secondary arms and second phase fraction, no systematic solidification study on Mg alloys has been performed to understand the evolution of microstructural features as a function of cooling rate and solute content. The present study focuses on the experimental microstructural evolution of Mg-3, 6 and 9 wt. % Al alloys in the cooling rate range of 1 K/sec to 1000 K/sec. The results suggest that secondary dendrite arm spacing and amount of second phase formation are strongly dependent on both solute content and cooling rate.


Author(s):  
I. Dutta ◽  
C. Park ◽  
S. Choi

Microelectronic solder joints are typically exposed to aggressive thermo-mechanical cycling (TMC) conditions, resulting in significant strain-enhanced microstructural coarsening during service. This microstructural evolution produces continuously evolving mechanical properties during extended use. Since solder joint life is dictated largely by the creep strain range, it is necessary to develop microstructurally adaptive creep models for solders to enable accurate prediction of joint life. In this paper, we present (1) a new closed-form creep model incorporating microstructural coarsening in lead-free solders, which can be easily incorporated into life-prediction models; and (2) a methodology for impression creep testing of Sn-3.5Ag solders which can potentially enable creep testing of individual flip chip or BGA balls in a package. The proposed creep model incorporates the effects of both static and strain-enhanced coarsening of second phase intermetallic particles which are present in lead-free solders, and shows that as a joint undergoes TMC, the creep rate increases continuously, adversely impacting life. This inference is supported by the impression creep experiments, which are shown to capture the essential features of creep in Sn-Ag alloys, in accordance with the available literature. It is also shown that the creep resistance of a given alloy composition is strongly dependent on the microstructure, making it important that creep data used for joint life prediction be based on testing of actual joints or very tightly controlled microstructures.


2012 ◽  
Vol 735 ◽  
pp. 3-8
Author(s):  
John Wheeler

The Earth deforms dominantly by solid-state creep. Diffusion creep is known to be important. It is less clear whether mechanisms in which grain boundary sliding is accompanied by other processes (dislocation activity), and/or are associated with stress exponents closer to 2 than to 1 are important. Since the mechanisms of superplasticity are themselves not fully resolved, we cannot say for sure whether the Earth deforms superplastically. Models for diffusion creep are relevant for the Earth and possibly for superplastic materials. Modelling shows that large strains may not necessarily obliterate initial textures because grain rotations, although they occur, slow down as microstructures evolve. Modelling also predicts major strength anisotropy induced by grain shape alignment. Models for two-phase diffusion creep can be constructed for when the second phase is inert (insoluble). If both phases are soluble and can participate in diffusion, the basic theory for single phase diffusion creep cannot be applied and new insight is required.


Author(s):  
B. Hidalgo-Prada ◽  
J.J. Guilarte ◽  
S.Y. Paredes

An investigation was carried out to determine the effect of a thermomechanical process (TMP) in the precipitation of dispersed second phase particles, and to assess the recrystallization behavior of a deformed ALCANVEN-7475 commercial aluminum alloy. The TMP included solution anneal treatment at Ts = 482°C for 3 hours, overaging at temperatures (To) in the range from 160 - 400°c for 1 to 30 hours, cold and warm deformation up to 90% reduction of thickness (RA) and recrystallization at Tr = 482 °C for 15 to 60 minutes.A Hitachi H-600 TEM operated at 100 KV was utilized to examine the microstructural evolution of the alloy leading to the nucleation of recrystallization as a consecuence of the previously described four steps TMP.It was determined that the nucleation of recrystallized grains is promoted by the presence of second phase particles with critical sizes between 0.5 and 1.0 μm.


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